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    Composition and Article Including Fluoropolymer and Branched Silsesquioxane Polymer
    1.
    发明申请
    Composition and Article Including Fluoropolymer and Branched Silsesquioxane Polymer 有权

    公开(公告)号：US20220282079A1

    公开(公告)日：2022-09-08

    申请号：US17632253

    申请日：2020-09-03

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Michael H. Mitchell ,  Chetan P. Jariwala ,  Jitendra S. Rathore ,  Tho Q. Nguyen

    IPC: C08L27/24 ,  C08L27/18 ,  C08L27/20 ,  C08L27/16 ,  C08L29/10

    Abstract: The composition can include a fluoropolymer and a branched silsesquioxane polymer having terminal —Si(R3)3 groups and units having formula, in which * represents a bond to another silicon atom in the branched silsesquioxane polymer, R is an organic group comprising an aliphatic carbon-carbon double bond, and R3 is a non-hydrolyzable group or hydrogen. The fluoropolymer can be crosslinked with the branched silsesquioxane polymer. An article can include a first composition including a fluoropolymer in contact with a second composition including a silicone, wherein at least one of the first composition or second composition includes the branched silsesquioxane polymer. At least one of the fluoropolymer or the silicone can be crosslinked with a branched silsesquioxane polymer including terminal —Si(R3)3 groups and units having formula, in which R* is an organic group comprising a carbon-carbon bond between the branched silsesquioxane polymer and the fluoropolymer, the silicone, or another R* group.

    Compositions including a silsesquioxane polymer and a free siloxane, and articles
    3.
    发明授权
    Compositions including a silsesquioxane polymer and a free siloxane, and articles 有权

    公开(公告)号：US10988578B2

    公开(公告)日：2021-04-27

    申请号：US16641053

    申请日：2018-09-13

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Jitendra S. Rathore ,  Ramesh C. Kumar ,  Chetan P. Jariwala

    IPC: C08G77/24 ,  C08G77/04 ,  C09J7/40 ,  C09J7/38

    Abstract: A composition, and article including such composition, wherein the composition includes a silsesquioxane polymer and a free siloxane; wherein the silsesquioxane polymer includes a three-dimensional network of Formula (I): wherein: each R1 and R2 is independently a (C1-C4)alkyl; each L1 and L2 is independently a single bond, an alkylene, or an alkylene bonded to a group selected from oxy, thio, carbonyl, —NH—, and combinations thereof; each R3 is independently a linear (C14-C100)alkyl; each R5 is independently a (C1-C30)alkyl, a (C1-C30)fluorinated alkyl, or a (C2-C30)heteroalkyl having at least one oxygen, sulfur, or —NH— group; with the proviso that L1, L2, and R5 are selected such that each Si atom is directly bonded to an alkylene or an alkyl; m is an integer of at least 2; n is an integer of 0 or above; m+n is an integer of at least 10; each oxygen atom at an asterisk (*) is bonded to another Si atom within the three-dimensional network; and the silsesquioxane polymer is a solid at 25° C.

    COMPOUND, ADHESIVE ARTICLE, AND METHODS OF MAKING THE SAME
    6.
    发明申请
    COMPOUND, ADHESIVE ARTICLE, AND METHODS OF MAKING THE SAME 审中-公开

    公开(公告)号：US20190382625A1

    公开(公告)日：2019-12-19

    申请号：US16349667

    申请日：2017-11-08

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Maria A. Appeaning ,  Marie A. Boulos ,  David J. Kinning ,  Georgiy Teverovskiy ,  Chetan P. Jariwala ,  Michael L. Steiner ,  Sai Vang

    IPC: C09J7/40 ,  C09J7/20

    Abstract: A method of making an adhesive article comprises three steps. First, a backing is provided having first and second opposed major surfaces with respective first and second silicone release layers disposed thereon. The second silicone release layer further comprises organic solvent and a compound represented by the formula: R1 represents a monovalent, divalent, or trivalent hydrocarbon radical having from 2 to 40 carbon atoms or covalent bond. Rf represents a perfluorinated group having from 3 to 5 carbon atoms. X1 represents —NH— or a covalent bond. Second, an adhesive layer is disposed onto the first silicone release layer. Third, the adhesive layer is exposed to E-beam radiation within a process chamber containing oxygen to provide a crosslinked adhesive layer. An adhesive article made by the method and the compound are also disclosed.

    Fluid control films with hydrophilic surfaces, methods of making same, and processes for cleaning structured surfaces
    7.
    发明授权
    Fluid control films with hydrophilic surfaces, methods of making same, and processes for cleaning structured surfaces 有权

    公开(公告)号：US10378813B2

    公开(公告)日：2019-08-13

    申请号：US15305524

    申请日：2015-04-22

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Adam J. Meuler ,  Susannah C. Clear ,  Steven P. Swanson ,  Kurt J. Halverson ,  Justin A. Riddle ,  Paul B. Armstrong ,  Caleb T. Nelson ,  Chetan P. Jariwala

    IPC: F25D21/14 ,  C08J5/18 ,  B32B7/06 ,  B32B7/12 ,  B08B1/00 ,  B08B3/10 ,  F15D1/00 ,  B32B3/30

    Abstract: A fluid control film is provided that includes fluid control channels extending along a channel longitudinal axis. Each of the fluid control channels has a surface and is configured to allow capillary movement of liquid in the channels. The fluid control film further includes a hydrophilic surface treatment covalently bonded to at least a portion of the surface of the fluid control channels. The fluid control film exhibits a capillary rise percent recovery of at least ten percent. Typically, the hydrophilic surface treatment includes functional groups selected from a non-zwitterionic sulfonate, a non-zwitterionic carboxylate, a zwitterionic sulfonate, a zwitterionic carboxylate, a zwitterionic phosphate, a zwitterionic phosphonic acid, and/or a zwitterionic phosphonate. A process for forming a fluid control film is also provided. Further, a process for cleaning a structured surface is provided, including providing a structured surface and a hydrophilic surface treatment covalently bonded to at least a portion of the structured surface, and soiling the structured surface with a material. The process also includes removing the material by at least one of submerging the structured surface in an aqueous fluid, rinsing the structured surface with an aqueous fluid, condensing an aqueous fluid on the structure surface, or wiping the structured surface with a cleaning implement.

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