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公开(公告)号：US10228617B2
公开(公告)日：2019-03-12
申请号：US15891771
申请日：2018-02-08
摘要： A semi-submersible microscope objective includes a microscope objective having a protective barrel with an optical inlet and optical outlet, and a protective element affixed to the microscope objective, sealing the optical exit but not the optical inlet. A transparent portion of the protective element is aligned with the optical exit. The protective element is separable from the microscope objective without damaging the microscope objective. Use of the semi-submersible microscope objective in a multiphoton imaging method is also disclosed.
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公开(公告)号：US11248117B2
公开(公告)日：2022-02-15
申请号：US16629429
申请日：2018-07-17
发明人： Xuan Jiang , Jeffrey N. Bartow , Robert J. DeVoe , Tatsuo Fukushi , Klaus Hintzer , Tho Q. Nguyen , Sheng Ye , Fee Zentis
IPC分类号： C08L27/20 , B29C35/08 , C08F214/22 , C08K5/14 , C08K5/357
摘要： Described herein is a curable composition comprising an amorphous fluoropolymer having an iodine, bromine and/or nitrile cure site; a peroxide cure system comprising a peroxide and a Type II coagent; and a photoinitiator, wherein the curable composition is substantially free of a binder material. Also described herein, are methods of curing the curable composition using actinic radiation and articles thereof.
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公开(公告)号：US20160306277A1
公开(公告)日：2016-10-20
申请号：US15100577
申请日：2014-12-01
发明人： Tzu-Chen Lee , Robert J. DeVoe , Brian K. Nelson , Brian J. Gates
CPC分类号： G03F7/0037 , C08F2/50 , C08F2222/1026 , G03F7/027 , G03F7/031 , G03F7/038 , G03F7/039 , G03F7/16 , G03F7/20 , G03F7/2012 , G03F7/2053 , G03F7/30
摘要： A method of fabricating a structure includes disposing a liquid photoreactive composition on a substrate, exposing a portion of the liquid photoreactive composition to laser light of sufficient intensity and wavelength to cause polymerization via two-photon excitation of the two-photon sensitizer and polymerization of a portion of the liquid photoreactive composition thereby providing an exposed composition; and developing the exposed composition to provide the structure. The liquid composition includes: at least one cationically polymerizable polyepoxide; at least one compound comprising free-radically polymerizable groups; an effective amount of a two-photon photoinitiator system, wherein the weight ratio of component (a) to component (b) is from 25:75 to 75:25, inclusive. The two-photon photoinitiator system includes a two-photon sensitizer and an aromatic onium salt. The liquid photoreactive composition may contain less than about one percent by weight of organic solvent.
摘要翻译： 制造结构的方法包括将液体光反应性组合物设置在基材上，将一部分液体光反应性组合物暴露于具有足够强度和波长的激光以通过双光子敏化剂的双光子激发引发聚合， 液体光反应性组合物的一部分由此提供暴露的组合物; 并显影曝光的组合物以提供结构。 液体组合物包括：至少一种可阳离子聚合的聚环氧化物; 至少一种包含可自由基聚合的基团的化合物; 有效量的双光子光引发剂体系，其中组分（a）与组分（b）的重量比为25:75至75:25，包括端值。 双光子光引发剂体系包括双光子敏化剂和芳族鎓盐。 液体光反应性组合物可以含有小于约1重量％的有机溶剂。
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公开(公告)号：US09096503B2
公开(公告)日：2015-08-04
申请号：US13764291
申请日：2013-02-11
发明人： Ilya Gorodisher , Robert J. Webb , Robert J. DeVoe
IPC分类号： C08F12/30 , C07C321/00 , C08G63/06 , C09B11/02 , C07C323/25 , C07C323/52 , C08G73/06 , C08G75/04 , C08G75/02
CPC分类号： C07C323/25 , C07C323/52 , C08G73/06 , C08G75/02 , C08G75/0236 , C08G75/04
摘要： Novel benzoxazine-thiol adducts are described, which may be may be cured to produce compositions useful in coating, sealants, adhesive and many other applications.
摘要翻译： 描述了新的苯并恶嗪 - 硫醇加合物，其可以固化以产生可用于涂料，密封剂，粘合剂和许多其它应用的组合物。
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公开(公告)号：US20150030985A1
公开(公告)日：2015-01-29
申请号：US14378577
申请日：2013-02-18
发明人： Robert J. DeVoe , Tzu-Chen Lee , Brian J. Gates
IPC分类号： G03F7/20
CPC分类号： G03F7/2053
摘要： The present disclosure relates to multiphoton absorption methods for curing a photocurable composition under conditions wherein negative contrast occurs. The photocurable composition includes a free-radically polymerizable compound. The method is applicable to fabrication of structures with micron-scale dimensions or less.
摘要翻译： 本发明涉及在发生负对比度的条件下固化可光固化组合物的多光子吸收方法。 光固化性组合物包含可自由基聚合的化合物。 该方法适用于具有微米级尺寸或更小尺寸的结构的制造。
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公开(公告)号：US20180363613A1
公开(公告)日：2018-12-20
申请号：US16101775
申请日：2018-08-13
摘要： Nozzle and a method of making the same are disclosed. The method includes forming a material into a nozzle forming microstructured pattern comprising a plurality of nozzle hole forming features and planar control cavity forming features; forming at least one different material into a nozzle pre-form using the nozzle forming microstructured pattern, with the nozzle pre-form comprising a plurality of nozzle pre-form holes and sacrificial planar control cavities; and forming a nozzle from the nozzle pre-form, said forming the nozzle comprising removing enough of the at least one different material to remove the sacrificial planar control cavities so as to form a top surface of the nozzle pre-form into a top surface of the nozzle, and to form each of the nozzle pre-form holes into a nozzle through hole.
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7.发明申请公开(公告)号：US20180231888A1
公开(公告)日：2018-08-16
申请号：US15891771
申请日：2018-02-08
CPC分类号： G03F7/0005 , G02B1/04 , G02B1/14 , G02B7/02 , G02B21/02 , G02B21/33 , G02B2207/114 , G03F7/2053 , G03F7/32 , G03F7/70983
摘要： A semi-submersible microscope objective includes a microscope objective having a protective barrel with an optical inlet and optical outlet, and a protective element affixed to the microscope objective, sealing the optical exit but not the optical inlet. A transparent portion of the protective element is aligned with the optical exit. The protective element is separable from the microscope objective without damaging the microscope objective. Use of the semi-submersible microscope objective in a multiphoton imaging method is also disclosed.
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公开(公告)号：US09927702B2
公开(公告)日：2018-03-27
申请号：US15100552
申请日：2014-12-01
CPC分类号： G03F7/0005 , G02B1/04 , G02B1/14 , G02B7/02 , G02B21/02 , G02B21/33 , G02B2207/114 , G03F7/2053 , G03F7/32 , G03F7/70983
摘要： A semi-submersible microscope objective (100) includes a microscope objective having a protective barrel (120) with an optical inlet (122) and optical outlet (124), and a protective element (130) affixed to the microscope objective, sealing the optical outlet (124) but not the optical inlet (122). A transparent portion (132) of the protective element is aligned with the optical exit (124). The protective element is separable from the microscope objective without damaging the microscope objective. Use of the semi-submersible microscope objective in a multiphoton imaging method is also disclosed.
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9.发明申请SEMI-SUBMERSIBLE MICROSCOPE OBJECTIVE WITH PROTECTIVE ELEMENT AND USE OF THE SAME IN MULTIPHOTON IMAGING METHOD 有权具有保护元件的半不可见微观显微镜及其在多光子成像方法中的应用公开(公告)号：US20160299426A1
公开(公告)日：2016-10-13
申请号：US15100552
申请日：2014-12-01
CPC分类号： G03F7/0005 , G02B1/04 , G02B1/14 , G02B7/02 , G02B21/02 , G02B21/33 , G02B2207/114 , G03F7/2053 , G03F7/32 , G03F7/70983
摘要： A semi-submersible microscope objective (100) includes a microscope objective having a protective barrel (120) with an optical inlet (122) and optical outlet (124), and a protective element (130) affixed to the microscope objective, sealing the optical outlet (124) but not the optical inlet (122). A transparent portion (132) of the protective element is aligned with the optical exit (124). The protective element is separable from the microscope objective without damaging the microscope objective. Use of the semi-submersible microscope objective in a multiphoton imaging method is also disclosed.
摘要翻译： 半潜式显微镜物镜（100）包括具有带有光学入口（122）和光学出口（124）的保护筒（120）的显微镜物镜和固定到显微物镜的保护元件（130），密封光学 出口（124）而不是光学入口（122）。 保护元件的透明部分（132）与光学出口（124）对齐。 保护元件可与显微镜物镜分离，而不会损坏显微镜物镜。 还公开了在多光子成像方法中使用半潜式显微镜物镜。
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公开(公告)号：US08885146B2
公开(公告)日：2014-11-11
申请号：US14100127
申请日：2013-12-09
发明人： Robert J. DeVoe , Brian J. Gates , Dean Faklis , Robert T. Krasa , Przemyslaw P. Markowicz , Craig R. Sykora
CPC分类号： G03F7/20 , B29C64/135 , B33Y10/00 , B33Y30/00 , B33Y40/00 , G03F7/2053 , G03F7/70375 , G03F7/70525 , G03F7/7085
摘要： An exposure system includes a light source emitting a beam along an optical axis that is capable of inducing a multi-photon reaction in a resin. The exposure system further includes a resin undergoing multiphoton reaction, as well as an automated system including a monitor that measures at least one property of the beam selected from power, pulse length, shape, divergence, or position in a plane normal to the optical axis. The monitor generates at least one signal indicative of the property of the beam, and a sub-system adjusts the beam in response to the signal from the monitor.
摘要翻译： 曝光系统包括沿着光轴发射能够在树脂中引起多光子反应的光束的光源。 曝光系统还包括进行多光子反应的树脂，以及包括监测器的自动化系统，该监视器测量从垂直于光轴的平面中的功率，脉冲长度，形状，发散度或位置中选择的光束的至少一个性质 。 监视器产生指示光束的属性的至少一个信号，并且子系统响应于来自监视器的信号来调整光束。
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