摘要:
A novel process for preparing particles of polymer gel prepared by polymerizing an aqueous solution of water-soluble vinyl monomers which comprises breaking the polymer gel into particles with a breaker device wherein the gel is cut into strips by a pair of rollers having a plurality of annular projections or grooves on their surfaces, the rollers rotating in an opposite direction to each other to engage each other and cut off the gel fed between the rollers, and the strips are then cut into particles by a combination of a fixed cutting blade and a rotating cutting blade. The obtained gel particles are further pulverized into fine round or particles spherical in a vertical type cutter comprising at least one vertically fixed cutting blade and a rotary cutting blade arranged rotatably and vertically, a clearance being provided between an edge of the rotary cutting blade and an edge of the fixed blade.
摘要:
An improved process for preparing a sticky water-soluble polymer, e.g. acrylamide polymers and acrylic acid polymers, which comprises polymerizing an aqueous solution of a monomer in a polymerization vessel of which the surface contacting the aqueous monomer solution is covered with a tetrafluoroethylene-ethylene copolymer film, whereby the stickiness of the produced polymer to the vessel is remarkably decreased, namely the peelability of the polymer from the vessel is remarkably improved, and moreover the polymerization conversion is remarkably improved. Also, the use of a metal deposited tetrafluoroethylene-ethylene copolymer film as a covering material improves the efficiency of a photopolymerization and enables to use a polymerization vessel made of an inexpensive material.
摘要:
An improved process for preparing a water-soluble polymer having an excellent water solubility and a high molecular weight, which comprises subjecting a thin layer of an aqueous solution of a water-soluble vinyl monomer to polymerization on a solid support, covering the thin layer with a substantially water-insoluble organic material, e.g. a paraffin, a silicone oil or a low molecular polyethylene, and/or a slightly water-soluble or substantially water-insoluble alkylene oxide adduct at least at a point of time when the aqueous monomer solution has not freely flowed, and further continuing the polymerization.
摘要:
A process for preparing particulate water-soluble acrylic polymers, e.g. acrylamide or methacrylamide polymers and cationic acrylic polymers, having a high molecular weight, an excellent water solubility and a uniform particle size with a good productivity, which comprises:(a) adding at least one surfactant selected from the group consisting of a non-ionic surfactant and an anionic surfactant to an at least 20% by weight aqueous solution of a vinyl monomer in an amount of 0.001 to 1% by weight based on the monomer.(b) adjusting the dissolved oxygen in the aqueous monomer solution to at most 1 mg/liter,(c) admixing the aqueous monomer solution with at most 0.03% by weight of a photopolymerization initiator based on the monomer,(d) continuously feeding the aqueous monomer solution in the form of a layer having a thickness of 3 to 10 mm onto a moving support located in an atmosphere containing at most 1% by volume of oxygen,(e) irradiating the layer of the aqueous monomer solution on the moving support with ultraviolet rays having a wavelength of 300 to 450 millimicrons at an intensity of at most 50 W/m.sup.2,(f) continuously taking out the produced polymer in the form of a sheet having a thickness of 3 to 10 mm from the moving support,(g) breaking the polymer sheet to cubic pieces of 3 to 10 mm in length of a side by a roller type cutter,(h) pulverizing the cubic pieces to particles having a diameter of 0.3 to 3 mm by a vertical type cutter, and(i) drying the particles with hot air.
摘要:
A slide member is slidable along a slide rail provided at a vehicle-body side portion. When lock pawls provided at the slide member are engaged with the slide rail, the slide member is locked. The slide member is unlocked by operating an operation cable connected to the lock pawls. The operation cable is fitted to a fitting portion of an attachment bracket connected to the slide rail. A portion from a fixed portion fixed to the fitting portion to a movable portion (one end portion) extends through a region where a non-contact portion is disposed, and does not contact the non-contact portion. The movable portion is connected to the slide member and moved integrally with the slide member.
摘要:
A silicon-based thin film depositing apparatus, including a plurality of transparent electrodes disposed to face corresponding counter electrodes with a space therebetween. Subsequently, while injecting a raw material gas from raw material gas injection orifices toward the supporting electrodes and also injecting a barrier gas from barrier gas injection orifices in the same direction as the direction in which the raw material gas is injected, the gases are discharged from a gas outlet, and thereby, the pressure in a chamber is controlled to a pressure of more than 1 kPa. Then, a DC pulse voltage is applied to each counter electrode to deposit a silicon-based thin film. A DC pulse voltage is applied to perform discharge. Therefore, even in a state where the distance between the electrodes is increased, plasma can be generated efficiently, and the in-plane distribution of film thickness can be improved.
摘要:
A pulsed power supply includes a DC power source, and a transformer and a switch which are connected in series with each other across the DC power source. The pulsed power supply operates to produce a plurality of high-voltage pulses in a repetition of cycles in each of which an induced energy is stored in the transformer when the switch is turned on and a high-voltage pulse is generated across a secondary winding of the transformer when the switch is turned off. The current flowing through the primary winding of the transformer is controlled to keep its peak value constant. The pulsed power supply further includes a current detector for detecting the current flowing through the primary winding of the transformer, and a third circuit for turning off the switch when the current detected by the current detector reaches the peak value.
摘要:
A direct current pulse voltage is applied on a treatment gas to generate a discharge plasma. The duty ratio of the direct current pulse voltage is controlled within the range of 0.0001% or more and 8.0% or less. The rise time of the direct current pulse voltage is controlled in the range of not lower than 0.1 V/nsec and not higher than 10000 V/nsec. Alternatively, a positive pulse and a negative pulse are applied from a single power source for performing the discharge plasma and the impurity implantation.
摘要:
A pulse power source comprises a first circuit, a second circuit, a transformer for coupling the first circuit and the second circuit, and a switching controller. The second circuit comprises a third semiconductor switch connected in series with a secondary winding of the transformer. The third semiconductor switch is connected in such a direction that a voltage generated in the second circuit is reverse-biased during a period in which the second semiconductor switch is turned on. A gate amplifier for forming a control signal from the switching controller into a pulse and outputting the pulse as a pulse signal is connected between a gate terminal and a cathode terminal of the third semiconductor switch.
摘要:
Metallic particle layers with metallic domains being arranged therein each at a predetermined space within a horizontal plane are laminated at an appropriate distance in the vertical direction in a dielectric layer. The distance ΔW between each of the metallic domains may be controlled by controlling the growth of metallic particles for the horizontal direction and the distance ΔL between the metallic particle layers may be controlled by controlling the thickness of the dielectric layer to be laminated for the vertical direction, so that the effect of field enhancement by plasmon resonance is improved by satisfactory control for the plasmon resonance in the direction of the thickness and in the direction orthogonal thereto.