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公开(公告)号：US20180258249A1
公开(公告)日：2018-09-13
申请号：US15978647
申请日：2018-05-14
Applicant: BASF SE
Inventor： Marc FRICKE , Dirk WEINRICH , Wibke LOELSBERG , Raman SUBRAHMANYAM , Irina SMIRNOVA , Pavel GURIKOV
CPC classification number: C08J9/28 , C08J9/0066 , C08J9/122 , C08J9/35 , C08J2201/026 , C08J2201/05 , C08J2201/0502 , C08J2203/06 , C08J2205/022 , C08J2205/024 , C08J2205/026 , C08J2205/028 , C08J2205/042 , C08J2305/04 , C08J2483/00 , C09K5/14
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a water soluble polysaccharide, at least one compound suitable to react as cross-linker for the polysaccharide or to release a cross-linker for the polysaccharide, and water, and preparing a gel (A) comprising exposing mixture (I) to carbon dioxide at a pressure in the range of from 20 to 100 bar for a time sufficient to form a gel (A), and depressurizing the gel (A). Gel (A) subsequently is exposed to a water miscible solvent (L) to obtain a gel (B), which is dried. The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material, for cosmetic applications, for biomedical applications or for pharmaceutical applications.
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公开(公告)号：US20180057654A1
公开(公告)日：2018-03-01
申请号：US15557925
申请日：2016-03-07
Applicant: BASF SE
Inventor： Marc FRICKE , Dirk WEINRICH , Wibke LOELSBERG
CPC classification number: C08J9/28 , C08G18/092 , C08G18/1875 , C08G18/225 , C08G18/7664 , C08G2101/0091 , C08G2105/02 , C08J9/0023 , C08J9/0052 , C08J2201/0502 , C08J2205/024 , C08J2205/026 , C08J2205/028 , C08J2375/02 , C08J2375/04
Abstract: The present invention relates to a process for preparing a porous material, at least providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises a catalyst system (CS) comprising a catalyst component (C1) selected from the group consisting of alkali metal and earth alkali metal, ammonium, ionic liquid salts of a saturated or unsaturated monocarboxylic acid and a carboxylic acid as catalyst component (C2). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels, in particular in interior or exterior thermal insulation systems as well as in water tank or ice maker insulation systems.
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公开(公告)号：US20210139633A1
公开(公告)日：2021-05-13
申请号：US16622620
申请日：2018-07-17
Applicant: BASF SE
Inventor： Marc FRICKE , Wibke LOELSBERG , Sohajl MOVAHHED , Dirk WEINRICH
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises a catalyst system (CS) at least comprising a catalyst component (C1) selected from the group consisting of ammonium salts and a carboxylic acid as catalyst component (C2). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels and vacuum insulation systems, in particular in interior or exterior thermal insulation systems as well as for the insulation of refrigerators and freezers and in water tank or ice maker insulation systems.
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公开(公告)号：US20190023864A1
公开(公告)日：2019-01-24
申请号：US16069666
申请日：2017-01-18
Applicant: BASF SE
Inventor： Wibke LOELSBERG , Marc FRICKE , Dirk WEINRICH
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b). According to the present invention, the composition (A) comprises a catalyst system (CS) comprising a component (C1) selected from the group consisting of alkali metal and earth alkali metal salts of a saturated or unsaturated carboxylic acid and a component (C2) selected from the group consisting of ammonium salts of a saturated or unsaturated carboxylic acid and no carboxylic acid is used as a component of the catalyst system. The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels, in particular in interior or exterior thermal insulation systems as well as in water tank or ice maker insulation systems.
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公开(公告)号：US20190023865A1
公开(公告)日：2019-01-24
申请号：US16070413
申请日：2017-01-18
Applicant: BASF SE
Inventor： Marc FRICKE , Dirk WEINRICH , Wibke LOELSBERG , Marcel NOBIS
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises at least one compound (af) comprising phosphorous and at least one functional group which is reactive towards isocyanates. The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels, in particular in interior or exterior thermal insulation systems as well as in water tank or ice maker insulation systems.
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Patent Agency Ranking
公开(公告)号：US20180244888A1
公开(公告)日：2018-08-30
申请号：US15758601
申请日：2016-09-19
Applicant: BASF SE
Inventor： Wibke LOELSBERG , Marc FRICKE , Dirk WEINRICH
CPC classification number: C08J9/286 , C08G18/022 , C08G18/225 , C08G18/7664 , C08G18/7671 , C08G2101/0066 , C08G2101/0091 , C08G2105/02 , C08G2330/50 , C08G2350/00 , C08J2201/0502 , C08J2205/024 , C08J2205/026 , C08J2207/00 , C08J2375/00 , F16L59/00
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) at least comprising an isocyanate composition (A*) comprising a polymeric polyfunctional isocyanate as component (ai), a monomeric polyfunctional isocyanate as component (aii), at least one catalyst as component (ac), wherein composition (A) is substantially free of aromatic amines, and a solvent (B), reacting the components in the composition (A) obtaining an organic gel, and drying of the gel obtained in step b). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels.
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公开(公告)号：US20170341945A1
公开(公告)日：2017-11-30
申请号：US15528308
申请日：2015-11-16
Applicant: BASF SE
Inventor： Wibke LOELSBERG , Marc FRICKE , Mark ELBING , Dirk WEINRICH
IPC: C01B33/158 , A61Q19/00 , A61K8/25 , B01J13/00 , A61K8/02
CPC classification number: C01B33/158 , A61K8/0279 , A61K8/25 , A61K2800/10 , A61K2800/805 , A61Q19/00 , B01J13/0091 , E04B2001/742 , Y02P20/544
Abstract: The present invention is directed to a process for preparing an inorganic aerogel, the process comprising the steps of providing a composition (I) suitable to form an inorganic gel with a gelation time tG, spraying the composition (I) into supercritical carbon dioxide at a spraying time tS to obtain gel particles, and drying the gel particles obtained in step (ii) by supercritical liquid extraction, wherein the ratio tS:tG is in the range of from 0.2 to 0.99. The present invention further is directed to the inorganic aerogel as such as well as the use of the inorganic aerogel according to the invention in particular for medical and pharmaceutical applications or for thermal insulation.
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公开(公告)号：US20220289928A1
公开(公告)日：2022-09-15
申请号：US17753147
申请日：2020-08-25
Applicant: BASF SE
Inventor： Dirk WEINRICH , Volker Vogelsang , Rene Thomas Wiegmann , Sohaji Movahhed , Marc Fricke , Torben Kaminsky , Maria Thomas , Joerg Erbes , Wibke Loelsberg
Abstract: A method can be used for manufacturing one or more bodies made of a porous material derived from precursors of the porous material in a sol-gel process. The method involves filling precursors of the porous material into a mold defining the shape of the body, where the precursors include at least two reactive components and a solvent, and forming a gel body. The step is then repeated so as to form several gel bodies. The gel bodies are then removed from the mold after a predetermined time in which the gel bodies are formed from the precursors of the porous material. The gel bodies are arranged adjacent to one another, a spacer is provided between two adjacent gel bodies so as to provide a clearance therebetween, and the solvent is then removed from the gel bodies.
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公开(公告)号：US20210139662A1
公开(公告)日：2021-05-13
申请号：US16621153
申请日：2018-07-13
Applicant: BASF SE
Inventor： Marc FRICKE , Wibke LOELSBERG , Marcel NOBIS , Dirk WEINRICH
Abstract: A process for preparing a porous material, including the steps of providing a mixture (I) containing a composition (A) containing components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) contains at least one compound (af) containing phosphorous and at least one functional group which is reactive towards isocyanates and at least one component (au) selected from the group consisting of urea, biuret, and derivatives of urea and biuret.
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公开(公告)号：US20210031464A1
公开(公告)日：2021-02-04
申请号：US16969066
申请日：2019-02-28
Applicant: BASF SE
Inventor： Dirk WEINRICH , Marc FRICKE , Volker VOGELSANG , Wibke LOELSBERG , Christian STELLING , Marcel NOBIS , Torben KAMINSKY , Maria THOMAS
Abstract: A method for manufacturing a body made of a porous material derived from precursors of the porous material in a sol-gel process, including (i) providing a mold, containing a lower part defining an interior volume for receiving the precursors of the porous material, wherein the lower part comprises a first opening, and surfaces of the lower part facing the interior volume are at least partially provided with a coating made of a material being electrically dissipative and non-sticky to the precursors of the porous material and/or the body, (ii) filling precursors of the porous material into the lower part in a first inert or ventilated region, wherein the precursors include two reactive components and a solvent, (iii) removing the body from the lower part through the first opening after a predetermined time, (iv) disposing the body onto a support, and (v) removing the solvent from the body.
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