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    Bio-based Surfactants
    1.
    发明申请
    Bio-based Surfactants 有权

    公开(公告)号：US20220089983A1

    公开(公告)日：2022-03-24

    申请号：US17482344

    申请日：2021-09-22

    Applicant: Battelle Memorial Institute

    Inventor： Daniel B. Garbark ,  Jeffrey T. Cafmeyer ,  Manoj Kumar Valluri ,  Phillip Denen ,  Albert J. Darling

    IPC: C11D11/00 ,  C11D1/90 ,  C11D1/92 ,  C11D1/66 ,  C11D1/52 ,  C07C231/14

    Abstract: Bio-based surfactants have great opportunity for use in a variety of applications such as laundry detergents, industrial cleaners, adjuvants, and oil & gas. Surfactants in these applications can be nonionic, anionic, cationic, or amphoteric. Utilizing high oleic soybean oil as a platform chemical, a variety of surfactants and properties can be produced. While early work focused solely on surfactant use in laundry cleaning and fracking, recent work has expanded functional groups and application evaluations in hard surface cleaning.
    The current invention expands on Battelle's high oleic soybean oil (HOSO) surfactant technology. Use of HOSO overcomes the limitations of regular soybean oil and significantly reduces or eliminates undesirable byproducts in most chemistries. However, with use of select reagents, a few candidates were achievable with regular epoxidized soybean oil (ESO). The HOSO surfactant platform offers several key advantages including: a highly water miscible (not typical of C18 surfactants) and water stable surfactant; ability to adjust and vary hydrophilic-lipophilic (HLB) values for stain removal performance; and increased biodegradability without toxic or persistent by-products.

    METHODS OF MAKING LEVULINIC ACID AND ALKYL LEVULINATES FROM SACCHARIDES
    3.
    发明申请
    METHODS OF MAKING LEVULINIC ACID AND ALKYL LEVULINATES FROM SACCHARIDES 审中-公开

    公开(公告)号：US20180194711A1

    公开(公告)日：2018-07-12

    申请号：US15403751

    申请日：2017-01-11

    Applicant: Battelle Memorial Institute

    Inventor： Herman P. Benecke ,  Daniel B. Garbark

    IPC: C07C67/00 ,  C07C51/00

    CPC classification number: C07C67/00 ,  C07C51/00 ,  C07C59/185 ,  C07C69/716

    Abstract: Unique methods have been developed to convert polysaccharides into value-added products, such as levulinic acid and alkyl levulinates. The polysaccharides are heated in the presence of water, an alcohol, and an acid to cleave the polysaccharide, and the resulting monosacchrides or monosaccharide acetals or both are contacted with an acid in the presence of an alcohol at a higher temperature. Useful acids include Brønsted acid catalysts and Lewis acid catalysts including mineral acids, metal halides, immobilized heterogeneous catalysts functionalized with a Brønsted acid group or a Lewis acid group, or combinations thereof.

    Process of producing liquid fuels from coal using biomass-derived solvents
    6.
    发明授权
    Process of producing liquid fuels from coal using biomass-derived solvents 有权

    公开(公告)号：US11466217B2

    公开(公告)日：2022-10-11

    申请号：US15760064

    申请日：2016-09-19

    Applicant: Battelle Memorial Institute

    Inventor： Satya P. Chauhan ,  Daniel B. Garbark ,  Herman P. Benecke ,  H. Nicholas Conkle

    IPC: C10G65/12 ,  C10G1/06 ,  C10G65/10

    Abstract: A process of producing a distillate fuel from coal includes: preparing a biomass-derived coal solvent; dissolving the coal in the biomass-derived solvent; and separating undissolved coal and mineral matter to produce a syncrude. In certain embodiments, the process further includes subjecting the syncrude to a hydrotreatment/hydrogenation process to produce a distillate fuel. In certain embodiments, the biomass-derived solvent is a hydrogen-donor solvent. A method to improve direct coal liquefaction includes: using a non-hydrogenated lipid in a direct coal liquefaction process to facilitate coal depolymerization. In certain embodiments, the lipid is a polyunsaturated biobased oil. A method for using a biomass-derived feedstock as a hydrogen donor includes: providing a biomass-derived feedstock; modifying the feedstock to improve its usefulness as a hydrogen donor; and conducting a transfer hydrogenation process using the modified feedstock as a hydrogen donor. In certain embodiments, the transfer hydrogenation process is a direct coal liquefaction process.

    POWDER COATING RESINS FROM C12-C23 DIACIDS
    7.
    发明申请
    POWDER COATING RESINS FROM C12-C23 DIACIDS 有权

    公开(公告)号：US20210054230A1

    公开(公告)日：2021-02-25

    申请号：US16965003

    申请日：2019-01-25

    Applicant: Battelle Memorial Institute

    Inventor： Jeffrey T. Cafmeyer ,  Daniel B. Garbark

    IPC: C09D177/12 ,  C08G69/44 ,  C09D5/03

    Abstract: Powder coating resins and coatings made using the powder coating resins are described. The powder coating resins are based on the use of C12 to C23 diacids. The C12 to C23 diacids are reacted with a reactant having an alcohol functionality and an amine functionality to form a carboxylic acid terminated polymer having ester and amide functionality. Alternatively, the C12 to C23 diacids are reacted with a reactant having an alcohol functionality and an amine functionality to form an intermediate polyol, which is then reacted with acetoacetic acid or an ester thereof to form an acetoacetate-terminated polymer.

    Lignin to liquid fuels and polyols using biomass-derived solvents
    10.
    发明授权
    Lignin to liquid fuels and polyols using biomass-derived solvents 有权

    公开(公告)号：US11268034B2

    公开(公告)日：2022-03-08

    申请号：US16631116

    申请日：2018-07-13

    Applicant: Battelle Memorial Institute

    Inventor： Satya P. Chauhan ,  Daniel B. Garbark

    IPC: C10G1/06 ,  C10G1/04 ,  C10G1/02 ,  C10G69/06 ,  C10G45/32 ,  C10G45/44 ,  C10G1/00

    Abstract: A process of producing a distillate fuel from lignin includes: preparing a biomass-derived lignin solvent; dissolving the lignin in the biomass-derived solvent; and separating undissolved lignin and mineral matter to produce a syncrude. In certain embodiments, the process further includes subjecting the syncrude to a hydrotreatment/hydrogenation process to produce a distillate fuel. A process to improve direct lignin liquefaction includes: using a non-hydrogenated lipid in a direct lignin liquefaction process to facilitate lignin depolymerization. A process for using a biomass-derived feedstock as a hydrogen donor includes: providing a biomass-derived feedstock; modifying the feedstock to improve its usefulness as a hydrogen donor; and conducting a transfer hydrogenation process using the modified feedstock as a hydrogen donor.

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