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    Methods of making metal particles
    1.
    发明授权
    Methods of making metal particles 有权

    公开(公告)号：US11273494B2

    公开(公告)日：2022-03-15

    申请号：US16494800

    申请日：2018-03-16

    申请人： BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM

    发明人： Simon M. Humphrey

    IPC分类号： B22F9/24 ,  B01J37/04 ,  B22F1/00 ,  B01J23/46 ,  B01J21/08

    摘要： Disclosed herein are methods of making a plurality of metal particles, the methods comprising: injecting a metal particle precursor, a capping material, and a reducing agent into an inlet of a continuous flow microwave reactor, thereby forming a mixture within the continuous flow microwave reactor, wherein the inlet of the continuous flow microwave reactor is fluidly connected to an outlet of the continuous flow microwave reactor through a reaction vessel; flowing the mixture through the reaction vessel, wherein the metal particle precursor is reduced within the reaction vessel, thereby forming the plurality of metal particles; and collecting the plurality of metal particles from the outlet of the continuous flow microwave reactor.

    Phosphorous-Based Sensors For Detection Of Multiple Solvents
    4.
    发明申请
    Phosphorous-Based Sensors For Detection Of Multiple Solvents 有权

    公开(公告)号：US20220268707A1

    公开(公告)日：2022-08-25

    申请号：US17740135

    申请日：2022-05-09

    申请人： Board of Regents, The University of Texas System

    发明人： Simon M. Humphrey ,  Bradley J. Holliday ,  Matthew D. Moore ,  Samuel G. Dunning

    IPC分类号： G01N21/78 ,  C09K11/06 ,  G01N31/22

    摘要： Embodiments of the present disclosure pertain to methods of monitoring an environment for the presence of a solvent by: (i) exposing the environment to a luminescent compound, where the relative luminescence emission intensity of the luminescent compound changes upon interaction with the solvent; and (ii) monitoring a change in the relative luminescence emission intensity of the luminescent compound, where the absence of the change indicates the absence of the solvent from the environment, and where the presence of the change indicates the presence of the solvent in the environment. The luminescent compounds include a phosphorous atom with one or more carboxyl groups, where the carboxyl groups are coordinated with one or more metallic ions (e.g., lanthanide ions and yttrium ions). The present disclosure also pertains to sensors for monitoring an environment for the presence of a solvent, where the sensors include one or more of the aforementioned luminescent compounds.

    Phosphorous-based sensors for detection of multiple solvents
    5.
    发明授权
    Phosphorous-based sensors for detection of multiple solvents 有权

    公开(公告)号：US10782239B2

    公开(公告)日：2020-09-22

    申请号：US15572411

    申请日：2016-05-10

    申请人： Board of Regents, The University of Texas System

    发明人： Simon M. Humphrey

    IPC分类号： G01N21/00 ,  G01N21/78 ,  C09K11/06 ,  G01N31/22 ,  G01N21/77

    摘要： Embodiments of the present disclosure pertain to methods of monitoring an environment for the presence of a solvent by: (i) exposing the environment to a luminescent compound, where the relative luminescence emission intensity of the luminescent compound changes upon interaction with the solvent; and (ii) monitoring a change in the relative luminescence emission intensity of the luminescent compound, where the absence of the change indicates the absence of the solvent from the environment, and where the presence of the change indicates the presence of the solvent in the environment. The luminescent compounds include a phosphorous atom with one or more carboxyl groups, where the carboxyl groups are coordinated with one or more metallic ions (e.g., lanthanide ions and yttrium ions). The present disclosure also pertains to sensors for monitoring an environment for the presence of a solvent, where the sensors include one or more of the aforementioned luminescent compounds.

    Use of metal organic frameworks for H2O sorption
    6.
    发明授权
    Use of metal organic frameworks for H2O sorption 有权

    公开(公告)号：US11266948B2

    公开(公告)日：2022-03-08

    申请号：US16540728

    申请日：2019-08-14

    申请人： Board of Regents, The University of Texas System ,  Korea Research Institute of Chemical Technology

    发明人： Simon M. Humphrey ,  Jong-San Chang ,  Young Kyu Hwang

    IPC分类号： B01J20/22 ,  B01D53/26 ,  B01D53/04 ,  B01D53/047 ,  B01J20/28

    摘要： Embodiments of the present disclosure pertain to methods of sorption of H2O from an environment by associating the environment with a porous material such that the association results in the sorption of H2O to the porous material. The porous material includes a (M)-2,4-pyridinedicarboxylic acid coordination polymer, where M is a divalent metal ion selected from the group consisting of Mn, Fe, Co, Ni, Mg, and combinations thereof. The coordination polymer has a one-dimensional pore structure and shows reversible soft-crystal behavior. The porous material may be a Mg(II) 2,4-pyridinedicarboxylic acid coordination polymer (i.e., Mg-CUK-1). The methods of the present disclosure may also include one or more steps of releasing the sorbed H2O from the porous material and reusing the porous material after the releasing step for sorption of additional H2O from the environment.

    USE OF METAL ORGANIC FRAMEWORKS FOR H2O SORPTION
    7.
    发明申请
    USE OF METAL ORGANIC FRAMEWORKS FOR H2O SORPTION 审中-公开

    公开(公告)号：US20200054991A1

    公开(公告)日：2020-02-20

    申请号：US16540728

    申请日：2019-08-14

    申请人： Board of Regents, The University of Texas System ,  Korea Research Institute of Chemical Technology

    发明人： Simon M. Humphrey ,  Jong-San Chang ,  Young Kyu Hwang

    IPC分类号： B01D53/26 ,  B01D53/04 ,  B01D53/047 ,  B01J20/22 ,  B01J20/28

    摘要： Embodiments of the present disclosure pertain to methods of sorption of H2O from an environment by associating the environment with a porous material such that the association results in the sorption of H2O to the porous material. The porous material includes a (M)-2,4-pyridinedicarboxylic acid coordination polymer, where M is a divalent metal ion selected from the group consisting of Mn, Fe, Co, Ni, Mg, and combinations thereof. The coordination polymer has a one-dimensional pore structure and shows reversible soft-crystal behavior. The porous material may be a Mg(II) 2,4-pyridinedicarboxylic acid coordination polymer (i.e., Mg-CUK-1). The methods of the present disclosure may also include one or more steps of releasing the sorbed H2O from the porous material and reusing the porous material after the releasing step for sorption of additional H2O from the environment.