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33 条记录 (耗时 0.04 秒)

    High throughput property testing of olefin copolymers using rheological determinations
    1.
    发明授权
    High throughput property testing of olefin copolymers using rheological determinations 失效
    使用流变学测定的烯烃共聚物的高通量性能测试

    公开(公告)号：US07427506B2

    公开(公告)日：2008-09-23

    申请号：US10823460

    申请日：2004-04-13

    申请人： Cesar A. Garcia-Franco ,  David J. Lohse ,  Bruce A. Harrington ,  Robert Jay Wittenbrink

    发明人： Cesar A. Garcia-Franco ,  David J. Lohse ,  Bruce A. Harrington ,  Robert Jay Wittenbrink

    IPC分类号： G01N37/00 ,  G01N1/00 ,  B01L9/00

    CPC分类号： G01N33/445 ,  Y10T436/13 ,  Y10T436/25

    摘要： A high throughput method to determine an amount of a comonomer in a copolymer sample of a copolymer system comprises the steps of providing a plurality of copolymer samples; creating an array of the copolymer samples; measuring a sample complex modulus of each of the copolymer samples at a comparison phase angle; and determining the amount of a comonomer in the copolymer sample by comparing the sample complex modulus to a calibration curve, wherein the calibration curve relates a concentration of the comonomer in the copolymer sample to a complex moduli of the copolymer sample determined at the comparison phase angle. A method of determining the amount of a comonomer in both a single copolymer sample, and in a high throughput scheme using the crossover modulus is also disclosed.

    摘要翻译： 用于确定共聚物体系的共聚物样品中共聚单体的量的高通量方法包括提供多个共聚物样品的步骤; 产生共聚物样品阵列; 以比较相位角测量每个共聚物样品的样品复数模量; 并且通过将样品复合物模量与校准曲线进行比较来确定共聚物样品中的共聚单体的量，其中校准曲线将共聚物样品中的共聚单体的浓度与在比较相位角处确定的共聚物样品的复数模量相关 。 还公开了在单一共聚物样品中以及使用交叉模量的高通量方案中测定共聚单体的量的方法。

    Slurry hydrocarbon synthesis with liquid hydroisomerization in the synthesis reactor
    7.
    发明授权
    Slurry hydrocarbon synthesis with liquid hydroisomerization in the synthesis reactor 失效
    在合成反应器中进行液体加氢异构化的淤浆烃合成

    公开(公告)号：US06717024B2

    公开(公告)日：2004-04-06

    申请号：US09992141

    申请日：2001-11-06

    申请人： Robert Jay Wittenbrink ,  Charles John Mart ,  Janet Renee Clark ,  Jennifer Schaefer Feeley

    发明人： Robert Jay Wittenbrink ,  Charles John Mart ,  Janet Renee Clark ,  Jennifer Schaefer Feeley

    IPC分类号： C07C522

    CPC分类号： C10G2/32 ,  B01J8/006 ,  B01J8/226 ,  B01J19/2485 ,  B01J2208/0084 ,  B01J2208/025 ,  C10G2/342 ,  C10G45/58 ,  Y10S208/95

    摘要： A slurry Fischer-Tropsch hydrocarbon synthesis process for synthesizing liquid hydrocarbons from synthesis gas in a synthesis reactor also hydroisomerizes the synthesized hydrocarbon liquid, which comprises the slurry liquid, in one or more lift reactors immersed in the slurry body in the synthesis reactor. A monolithic catalyst is preferably used for the hydroisomerization, and slurry circulation up through the lift reactors from the surrounding slurry body, is achieved at least in part by the lift action of the hydroisomerization treat gas. Preferably, catalyst particles are also removed before the slurry contacts the catalyst. Hydroisomerization occurs while the synthesis reactor is producing hydrocarbons, without interfering with the synthesis reaction. A gas bubble reducing downcomer may be used to produce and feed the gas bubble reduced slurry into the lift reactor, thereby providing a hydraulic head assist in the slurry circulation up through and out of the lift reactor.

    摘要翻译： 用于在合成反应器中从合成气中合成液态烃的浆料费 - 托烃合成方法还将合成的包含浆料液体的烃液体在浸入合成反应器中的浆料体的一个或多个提升反应器中进行加氢异构化。 优选使用整体式催化剂用于加氢异构化，并且至少部分地通过加氢异构化处理气体的提升作用实现通过来自周围淤浆体的提升反应器的浆料循环。 优选地，催化剂颗粒在浆料接触催化剂之前也被除去。 在合成反应器生产碳氢化合物的同时发生加氢异构化，而不会干扰合成反应。 气泡减少降液管可以用于产生并将气泡减少的浆料进料到提升反应器中，从而在通过和离开提升反应器的浆料循环中提供液压头辅助。

    Biodegradable high performance hydrocarbon base oils
    10.
    发明授权
    Biodegradable high performance hydrocarbon base oils 失效
    可生物降解的高性能烃基油

    公开(公告)号：US06506297B1

    公开(公告)日：2003-01-14

    申请号：US09547809

    申请日：2000-04-11

    申请人： Robert Jay Wittenbrink ,  Richard Frank Bauman ,  Daniel Francis Ryan

    发明人： Robert Jay Wittenbrink ,  Richard Frank Bauman ,  Daniel Francis Ryan

    IPC分类号： C10G7100

    CPC分类号： C10G45/58 ,  C10G67/04 ,  C10G2400/10 ,  C10G2400/12 ,  C10G2400/14 ,  C10M107/02 ,  C10M2205/173 ,  C10N2220/028 ,  C10N2270/00

    摘要： Discloses novel biodegradable high performance hydrocarbon base oils useful as lubricants in engine oil and industrial compositions, and process for their manufacture. A waxy, or paraffinic feed, particularly a Fischer-Tropsch wax, is reacted over a dual function catalyst to produce hydroisomerization and hydrocracking reactions, at 700° F.+ conversion levels ranging from about 20 to 50 wt. %, preferably about 25-40 wt. %, sufficient to produce a crude fraction, e.g., a C5-1050° F.+ crude fraction, containing 700° F.+ isoparaffins having from about 6.0 to about 7.5 methyl branches per 100 carbon atoms in the molecule. The methyl paraffins containing crude fraction is topped via atmospheric distillation to produce a bottoms fraction having an initial boiling point between about 650° F. and 750° F. which is then solvent dewaxed, and the dewaxed oil is then fractionated under high vacuum to produce biodegradable high performance hydrocarbon base oils.

    摘要翻译： 公开了可用作发动机油和工业组合物中的润滑剂的新型可生物降解的高性能烃基油及其制造方法。 蜡状或石蜡原料，特别是费 - 托蜡在双功能催化剂上反应，产生加氢异构化和加氢裂化反应，在700°F +转化率范围为约20至50wt。 ％，优选约25-40wt。 ％，足以产生含有分子中每100个碳原子具有约6.0至约7.5个甲基支链的含有700°F +的异构烷烃的粗馏分，例如C5-1050°F +粗馏分。 含有粗制部分的甲基链烷烃通过常压蒸馏来顶部，产生沸点在约650°F至750°F之间的塔底馏分，然后进行溶剂脱蜡，然后将脱蜡油在高真空下分馏， 可生物降解的高性能烃基油。