Production of halogen-containing polyaryl esters
    1.
    发明授权
    Production of halogen-containing polyaryl esters 失效
    含卤素多糖酯的生产

    公开(公告)号:US3704279A

    公开(公告)日:1972-11-28

    申请号:US3704279D

    申请日:1971-07-28

    Inventor: ISMAIL ROSHDY

    CPC classification number: H01B3/423 C08G63/68 C08G63/682

    Abstract: IN THE PRODUCTION OF HAOGEN-CONTAINING POLYARYL ESTERS BY THE POLYCONDENSATION OF HALOGEN-CONTAINING DISPHENOLS AND AROMATIC ACID DICHLORIDES IN THE PRESENCE OF A CATALYST COMPRISING A TETIARY AMINE, AN AID AMIDE OR MIXTURES THEREOF, THE IMPROVEMENT WHICH COMPRISES EFFECTING THE CONDESATION IN THE PRESENCE OF ABOUT 0.001 TO 50 MOLEPERCENT BASED ON THE ACID DICHLORIDE, OF AT LEAST ONE ACTIVATOR SELECTED FROM THE GROUP CONSISTING OF MAGNESIUM COMPOUNDS, AND OXIDES, CHLORIDES OR HYDROCHLORIDES OF CU, ZR, SN, TN, V, PB AND FE. THE CONDENSATION IS PREFERABLY EFFECTED IN SOLUTION USING AS ACTIVATED CUO, CUCI, ZRCI4, SNCL2, TICL4, COCI3, PBO, FE2O3 OR AN ALLOY OF MG, CU, ZR, SN, TI, V, PB OR FE. IN THIS MANNER HIGH MOLECULAR WEIGHT CAN BE ATTAINED IN SHORT REACTION TIMES.

    Method of producing halogenated phenoxy-s-triazines
    3.
    发明授权
    Method of producing halogenated phenoxy-s-triazines 失效
    生产羟基苯酚-S-三唑的方法

    公开(公告)号:US3682908A

    公开(公告)日:1972-08-08

    申请号:US3682908D

    申请日:1970-05-05

    Inventor: ISMAIL ROSHDY

    CPC classification number: C07D251/26 C07D251/46

    Abstract: Production of halogenated phenoxy-s-triazines by the reaction of halogenated phenols and C-chlorides of s-triazines in the presence of catalytic quantities of tertiary amine or carbonamide compounds or quaternary ammonium salts thereof.

    Abstract translation: 在催化量的叔胺或碳酰胺化合物或其季铵盐的存在下,通过卤代苯酚和s-三嗪的C-氯化物的反应制备卤代苯氧基-s-三嗪。

    Process for the manufacture of titanic esters
    5.
    发明授权
    Process for the manufacture of titanic esters 失效
    钛铁矿制造工艺

    公开(公告)号:US3641079A

    公开(公告)日:1972-02-08

    申请号:US3641079D

    申请日:1969-03-25

    CPC classification number: C07F7/006

    Abstract: MANUFACTURE OF TATANIC ESTERS FROM TITANIC HALIDES AND UNSUBSITUTED OR ARYL-SUBSITUTED ALIPHATIC BYDROXY COMPOUNDS, CYCLOALIPHARIC HYDROXY COMPOUNDS, OR UNSUBSTITUTED OR ALKYL-SUBSTITUTED AROMATIC HYDROXY COMPOUNDS PERFORMED IN THE PRESENCE OF CATALYTIC QUANTITIES OF TERTIARY AMINES, WHOSE AMINO GROUP MAY OR MAY NOT BE A COMPONENT OF AN AROMATIC RING SYSTEM, AND OR IN THE PRESENCE OF UNSUBSITUTED OR N-MONOSUBSTITUTED OR NDISUBSTITUTED ACID AMIDES, WITH THE USE OF SOLVENTS IF DESIRED, AT TEMPERATURES OF 50 TO 250*C., PREFERABLY 50 TO 200*C.

    Process for the preparation of phosphorus-containing compounds
    7.
    发明授权
    Process for the preparation of phosphorus-containing compounds 失效
    含磷化合物的制备方法

    公开(公告)号:US3927151A

    公开(公告)日:1975-12-16

    申请号:US32879973

    申请日:1973-02-01

    Abstract: Phosphorus-containing compounds, especially alkyl phosphates, of the formula
    wherein A is oxygen or sulfur, g and n are 0 or 1, and R1, R2 and R3, which may be the same or different, are alkyl, cycloalkyl or aryl wherein R1 may be substituted with one or more halogen atoms; are formed from the corresponding halo- or halo-alkoxyphosphorus compounds and a hydroxy-containing organic compound by reaction therebetween under gradual increase of temperature and simultaneous decrease in pressure, over an organo oxy compound catalyst comprising an element of Group II, IV or V of the Periodic System having an atomic number of between 12 and 83, in amounts of from 0.001 to 2 per cent by weight, based on the amount of starting phosphorus compound reactant.

    Abstract translation: 含有磷的化合物,特别是烷基磷酸酯,其通式为R 1 - (O)n | R2-O-P =(A)q | R3-O其中A为氧或硫,g和n为0或 1,R 1,R 2和R 3可以相同或不同,为烷基,环烷基或芳基,其中R 1可被一个或多个卤素原子取代; 由相应的卤代或卤代 - 烷氧基 - 磷化合物和含羟基的有机化合物通过在逐渐升高的温度下同时降低压力而相对于包含II,IV族元素的有机氧化合物催化剂而形成, 基于起始磷化合物反应物的量,周期性体系的V为原子序数为12至83,其量为0.001至2重量%。

    HALOGENPHENOXY-s-TRIAZINE DERIVATIVES HAVING IMPROVED SOLUBILITY
    8.
    发明授权
    HALOGENPHENOXY-s-TRIAZINE DERIVATIVES HAVING IMPROVED SOLUBILITY 失效
    具有改善溶解性的二氢苯并噻吩衍生物

    公开(公告)号:US3687952A

    公开(公告)日:1972-08-29

    申请号:US3687952D

    申请日:1969-02-19

    Inventor: ISMAIL ROSHDY

    Abstract: Novel halophenoxy-s-triazine derivatives and salts thereof characterized by improved solubilities having the formula:-

    WHEREIN X represents from one to five halogen atoms and R1 is either of

    WHEREIN R2 is alkyl having one to five carbon atoms, halogenated alkyl having one to five carbon atoms, alkali metal or ammonium, R3 is hydrogen, alkyl having two to 18 carbon atoms, halogenated alkyl having two to 18 carbon atoms or cycloalkyl, and R4 is alkyl, cycloalkyl, aryl, halogenated alkyl, halogenated cycloalkyl or halogenated aryl, and wherein R3 and R4 taken together with the nitrogen atom to which they are attached form a heterocyclic ring. The novel triazine derivatives and their salts are suitable for use as water repellants, parting agents, textile adjuvants, as fire retardants, fungicidal, phytotoxic, bactericidal and insecticidal agents.

    Abstract translation: 新型卤代苯氧基-s-三嗪衍生物及其盐的特征在于具有下列通式的改进的溶解度:

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