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    Deodorized pesticidal organothiophosphorus compounds
    3.
    发明授权
    Deodorized pesticidal organothiophosphorus compounds 失效
    除臭农药有机硫代磷化合物

    公开(公告)号：US3961043A

    公开(公告)日：1976-06-01

    申请号：US63293

    申请日：1970-08-12

    申请人： Arthur J. Huvar

    发明人： Arthur J. Huvar

    IPC分类号： C07F9/16 ,  A01N9/36

    CPC分类号： C07F9/16

    摘要： Deodorization of organothiophosphorus compounds is achieved by mixing said organothiophosphorus compounds with appropriate amounts of linoleic acid and/or linolenic acid, or drying oils containing linoleic acid and linolenic acid. Said mixtures are useful as pesticidal compositions having an acceptable or pleasant odor.

    摘要翻译： 通过将所述有机硫代磷化合物与适量的亚油酸和/或亚麻酸或含有亚油酸和亚麻酸的干性油混合来实现有机硫代磷化合物的除臭。 所述混合物可用作具有可接受或愉快气味的杀虫组合物。

    Process for the preparation of phosphorus-containing compounds
    4.
    发明授权
    Process for the preparation of phosphorus-containing compounds 失效
    含磷化合物的制备方法

    公开(公告)号：US3927151A

    公开(公告)日：1975-12-16

    申请号：US32879973

    申请日：1973-02-01

    申请人： DYNAMIT NOBEL AG

    发明人： ISMAIL ROSHDY ,  LENZ ARNOLD ,  TERMIN ERICH

    IPC分类号： C07F9/02 ,  C07F9/09 ,  C07F9/16 ,  C07F9/32 ,  C07F9/40 ,  C07F9/46 ,  C07F9/48 ,  C07F9/08

    CPC分类号： C07F9/48 ,  C07F9/02 ,  C07F9/09 ,  C07F9/16 ,  C07F9/32 ,  C07F9/40 ,  C07F9/46

    摘要： Phosphorus-containing compounds, especially alkyl phosphates, of the formula
    wherein A is oxygen or sulfur, g and n are 0 or 1, and R1, R2 and R3, which may be the same or different, are alkyl, cycloalkyl or aryl wherein R1 may be substituted with one or more halogen atoms; are formed from the corresponding halo- or halo-alkoxyphosphorus compounds and a hydroxy-containing organic compound by reaction therebetween under gradual increase of temperature and simultaneous decrease in pressure, over an organo oxy compound catalyst comprising an element of Group II, IV or V of the Periodic System having an atomic number of between 12 and 83, in amounts of from 0.001 to 2 per cent by weight, based on the amount of starting phosphorus compound reactant.

    摘要翻译： 含有磷的化合物，特别是烷基磷酸酯，其通式为R 1 - （O）n | R2-O-P =（A）q | R3-O其中A为氧或硫，g和n为0或 1，R 1，R 2和R 3可以相同或不同，为烷基，环烷基或芳基，其中R 1可被一个或多个卤素原子取代; 由相应的卤代或卤代 - 烷氧基 - 磷化合物和含羟基的有机化合物通过在逐渐升高的温度下同时降低压力而相对于包含II，IV族元素的有机氧化合物催化剂而形成， 基于起始磷化合物反应物的量，周期性体系的V为原子序数为12至83，其量为0.001至2重量％。

    0,0-Dialkyl-(3,5-dialkyl-4-hydroxybenzyl)dithiophosphate compositions and process for making same
    5.
    发明授权
    0,0-Dialkyl-(3,5-dialkyl-4-hydroxybenzyl)dithiophosphate compositions and process for making same 失效
    0-二烷基 - （3,5-二烷基-4-羟基苄基）二硫代磷酸酯组合物及其制备方法

    公开(公告)号：US3865906A

    公开(公告)日：1975-02-11

    申请号：US33544673

    申请日：1973-02-26

    申请人： ETHYL CORP

    发明人： SHIN KJU HI ,  ZAWESKI EDWARD F

    IPC分类号： C07F9/16 ,  C07F9/165 ,  C08K5/49 ,  C07F9/12 ,  B01J1/18

    CPC分类号： C07F9/165 ,  C07F9/16 ,  C08K5/49 ,  C08L21/00

    摘要： Organic material such as styrene-butadiene rubber is stabilized against oxidative degradation by the addition of an antioxidant composition made by the process comprising (A) reacting from 1-10 moles of a monohydric alkanol containing from one to about 50 carbon atoms with a mole of P2S5 at a temperature of from about 75* to about 125* C. to form a dithiophosphate reaction mixture; (B) neutralizing said dithiophosphate reaction mixture with aqueous ammonia; and (C) adding from about 1 to 3 moles of a hydroxybenzyl chloride to the neutralized reaction mixture and reacting at a temperature of from about 50* to 150* C. The preferred hydroxybenzyl chloride is 3,5-di-tert-butyl-4hydroxybenzyl chloride, and the preferred alkanol is a mixture of monohydric aliphatic C20-50 alcohols.

    摘要翻译： 苯乙烯 - 丁二烯橡胶等有机材料通过加入由（A）使1-10摩尔含有1-约50个碳原子的一元烷醇与一摩尔 P2S5在约75℃至约125℃的温度下反应形成二硫代磷酸酯反应混合物; （B）用氨水中和所述二硫代磷酸盐反应混合物; 和（C）将约1至3摩尔羟基苄基氯加入到中和的反应混合物中并在约50至150℃的温度下反应。优选的羟基苄基氯是3,5-二叔丁基 - 4-羟基苄基氯，优选的链烷醇是一元脂肪族C20-50醇的混合物。

    Alkoxyimino-phosphorus compounds
    6.
    发明授权
    Alkoxyimino-phosphorus compounds 失效
    碱金属磷酸盐化合物

    公开(公告)号：US3792130A

    公开(公告)日：1974-02-12

    申请号：US3792130D

    申请日：1971-11-29

    申请人： VELSICOL CHEMICAL CORP

    发明人： STACH L

    IPC分类号： C07F9/08 ,  C07F9/16 ,  C07F9/24 ,  C07F9/40 ,  A01N9/36

    CPC分类号： C07F9/40 ,  C07F9/08 ,  C07F9/16 ,  C07F9/24 ,  C07F9/2408

    摘要： THIS INVENTION DISCLOSES NEW COMPOUNDS OF THE FORMULA

    Z1-(X3)M-P(=X1)(-Y)-X2-CH(-(X4)N-Z2)-C(-R1)=N-O-R2

    WHEREIN R1 IS SELECTED FROM THE GROUP CONSISTING OF ALKYL, PHENYL, HALOPHENYL, ALKYLPHENYL AND ALKYL-HALOPHENYL; R2 IS ALKYL; X1, X2, X3 AND X4 ARE INDEPENDENTLY SELECTED FROM THE GROUP CONSISTING OF OXYGEN AND SULFUR; M AND N ARE EACH INTEGERS FROM 0 TO 1; Z1 IS SELECTED FROM THE GROUP CONSISTING OF ALKYL, ALKENYL AND

    ((A)Q,(H)(5-Q)-PHENYL)-(CH2)P-

    WHEREIN A IS SELECTED FROM THE GROUP CONSISTING OF ALKYL, ALKENYL, ALKOXY, ALKYLTHIO, HALOGEN, NITRO, ALKYLSULFOXIDE, ALKYLSULFONE AND DIALKYLAMINO; Q IS AN INTEGER FROM 0 TO 5, AND P IS AN INTEGER FROM 0 TO 3; Z2 IS SELECTED FROM THE GROUP CONSISTING OF HYDROGEN AND Z1, PROVIDED THAT WHEN Z2 IS HYDROGEN THEN N IS ZERO; AND Y IS SELECTED FROM THE GROUP CONSISTING OF ALKYL, ALKENYL, ALKOXY, ALKYLTHIO, AMINO, ALKYLAMINO, DIALKYLAMINO AND

    ((B)R,(H)(5-R)-PHENYL)-(Q)T-

    WHEREIN B IS SELECTED FROM THE GROUP CONSISTING OF ALKYL, ALKENYL, ALKOXY, ALKYLTHIO, HALOGEN, NITRO, ALKYLSULFOXIDE, ALKYLSULFONE AND DIALKYLAMINO; R IS AN INTEGER FROM 0 TO 5; Q IS SELECTED FROM THE GROUP CONSISTING OF OXYGEN, SULFUR, ALKYLENE, ALKYLENEOXY AND ALKYLENETHIO, AND T IS AN INTEGER FROM 0 TO 1. ALSO DISCLOSED ARE INSECTICIDAL AND ACARICIDAL COMPOSITIONS COMPRISING AN INERT CARRIER AND AN ABOVE DESCRIBED COMPOUND.