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公开(公告)号：US5268102A
公开(公告)日：1993-12-07
申请号：US27077
申请日：1993-03-05
申请人： Dale L. Clay , Robert W. Allington , Phillip B. Liescheski, III , Robin R. Winter , Daniel G. Jameson
发明人： Dale L. Clay , Robert W. Allington , Phillip B. Liescheski, III , Robin R. Winter , Daniel G. Jameson
IPC分类号： B01D11/00 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： F04B9/042 , B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： To supply supercritical fluid to an automatic supercritical fluid extractor and collect extract from the extractor, sample holding cartridges are lifted one by one in series by an elevator plug into a pressure chamber. An inlet at the top of the cartridge engages a pressure vessel inlet for the extractant so that extractant flows into the cartridge and into the space between the cartridge and inner walls of the pressure chamber. The outlets from the cartridge and pressure vessel communicate with the collector and exhaust through passageways in the plug. The plug has cleaning ports for cleaning seals and the outlet from the cartridge flows past the seals. The collector lifts vials into place and can precool the collection solvent, and later as part of the collection procedure, heat and pressurize the collector.
摘要翻译： 为了将超临界流体提供给自动超临界流体提取器并从提取器收集提取物，样品保持盒由电梯塞一个接一个地提升到压力室中。 药筒顶部的入口接合用于提取剂的压力容器入口，使得萃取剂流入药筒并进入药筒和压力室的内壁之间的空间。 墨盒和压力容器的出口与收集器连通，并通过插头中的通道排出。 插头具有用于清洁密封件的清洁端口，并且墨盒的出口流过密封件。 收集器将小瓶提升到适当位置，并可预先收集溶剂，然后作为收集过程的一部分，对收集器进行加热和加压。
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公开(公告)号：US5173188A
公开(公告)日：1992-12-22
申请号：US847652
申请日：1992-03-05
IPC分类号： B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： B01D11/0407 , B01D11/0203 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. In one embodiment, the extractor includes a fraction collector for extractants, an automatic sample changer and an automatic cartridge transfer mechanism which provide completely automated extractions. To automatically perform extraction, valves for the fluids are automatically opened and closed in synchronism with the insertion and removal of the cartridges. These valves force a hard valve element into a softer valve seat with a valve stem that does not rotate significantly under the control of a rotary motor.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 在一个实施方案中，提取器包括用于萃取剂的馏分收集器，自动取样器和提供完全自动提取的自动送料机构。 为了自动执行萃取，流体的阀门将与插入和拆卸墨盒同步自动打开和关闭。 这些阀将硬阀元件压入较软的阀座，阀杆在旋转电机的控制下不会显着转动。
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公开(公告)号：US5094753A
公开(公告)日：1992-03-10
申请号：US553119
申请日：1990-07-13
IPC分类号： F16J12/00 , B01D11/00 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： B01D11/0407 , B01D11/0203 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior.
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公开(公告)号：US5296145A
公开(公告)日：1994-03-22
申请号：US75314
申请日：1993-06-11
IPC分类号： B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015 , B01D11/00
CPC分类号： B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. In one embodiment, the extractor includes a fraction collector for extractants, an automatic sample changer and an automatic cartridge transfer mechanism which provide completely automated extractions. To automatically perform extraction, valves for the fluids are automatically opened and closed in synchronism with the insertion and removal of the cartridges. These valves force a hard valve element into a softer valve seat with a valve stem that does not rotate significantly under the control of a rotary motor.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 在一个实施方案中，提取器包括用于萃取剂的馏分收集器，自动取样器和提供完全自动提取的自动送料机构。 为了自动执行萃取，流体的阀门将与插入和拆卸墨盒同步自动打开和关闭。 这些阀将硬阀元件压入较软的阀座，阀杆在旋转电机的控制下不会显着转动。
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公开(公告)号：US5160624A
公开(公告)日：1992-11-03
申请号：US795987
申请日：1991-11-22
IPC分类号： B01D11/00 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/10 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： B01D11/0407 , B01D11/0203 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and/or machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior. In one embodiment, the extractor includes a fraction collector fr extractants, an automatic sample changer and an automatic cartridge transfer mechanism which provide completely automated extractions.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 由于低压差，提取筒不需要具有承受显着压力的强度，并且可以由用于一次性使用的模制塑料以及用于可重复使用的不锈钢和/或加工塑料制成。 提取盒可以拆卸和打开，无需使用工具进行样品通道。 在将其安装在加热的高压容器中以清除其外部的污染物之后，可将其清除。 在一个实施方案中，提取器包括馏分收集器fr萃取剂，自动样品更换器和提供完全自动提取的自动转移机构。
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6.发明授权Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography 失效超临界流体萃取或超临界流体色谱仪的设备和方法
公开(公告)号：US5601707A
公开(公告)日：1997-02-11
申请号：US501536
申请日：1995-07-12
IPC分类号： B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/32 , G01N30/60 , G01N30/82 , G01N35/04 , G21F5/015 , B01D11/00 , B01D15/08
CPC分类号： B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G01N30/82 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6008 , G01N2030/6013 , G01N2035/0441 , G01N30/02 , G01N30/32 , G01N30/60
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and/or machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior. In one embodiment, the extractor includes a fraction collector for extractants, an automatic sample changer and an automatic cartridge transfer mechanism which provide completely automated extractions.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 由于低压差，提取筒不需要具有承受显着压力的强度，并且可以由用于一次性使用的模制塑料以及用于可重复使用的不锈钢和/或加工塑料制成。 提取盒可以拆卸和打开，无需使用工具进行样品通道。 在将其安装在加热的高压容器中以清除其外部的污染物之后，可将其清除。 在一个实施方案中，提取器包括用于萃取剂的馏分收集器，自动取样器和提供完全自动提取的自动送料机构。
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公开(公告)号：US5250195A
公开(公告)日：1993-10-05
申请号：US966083
申请日：1992-10-23
IPC分类号： B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. In one embodiment, the extractor includes a fraction collector for extractants, an automatic sample changer and an automatic cartridge transfer mechanism which provide completely automated extractions. To automatically perform extraction, valves for the fluids are automatically opened and closed in synchronism with the insertion and removal of the cartridges. These valves force a hard valve element into a softer valve seat with a valve stem that does not rotate significantly under the control of a rotary motor.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 在一个实施方案中，提取器包括用于萃取剂的馏分收集器，自动取样器和提供完全自动提取的自动送料机构。 为了自动执行萃取，流体的阀门将与插入和拆卸墨盒同步自动打开和关闭。 这些阀将硬阀元件压入较软的阀座，阀杆在旋转电机的控制下不会显着转动。
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公开(公告)号：US5132014A
公开(公告)日：1992-07-21
申请号：US786752
申请日：1991-11-01
IPC分类号： A61B17/32 , A61B18/14 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： G21F5/015 , B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , A61B17/32 , A61B2018/126 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02 , Y10T29/53443
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior.
摘要翻译： 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 由于低压差，提取盒不需要具有承受显着压力的强度，并且可以由用于一次性使用的模制塑料以及用于可重复使用的不锈钢和机加工塑料制成。 提取盒可以拆卸和打开，无需使用工具进行样品通道。 在将其安装在加热的高压容器中以清除其外部的污染物之后，可将其清除。
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公开(公告)号：US5635070A
公开(公告)日：1997-06-03
申请号：US208121
申请日：1994-03-08
申请人： Robert W. Allington , Daniel G. Jameson , Dale A. Davison , Dale Clay , Robin R. Winter , Yoossef Tehrani
发明人： Robert W. Allington , Daniel G. Jameson , Dale A. Davison , Dale Clay , Robin R. Winter , Yoossef Tehrani
IPC分类号： B01D11/00 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F04B53/08 , F04B53/14 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： G01N1/34 , B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B53/08 , F04B53/143 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2201/0209 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： To pump supercritical carbon dioxide into a supercritical extractor without overpressure in the reservoir and to record the volume being delivered, the pumping speed is controlled and the volume pumped is determined from a pressure-related signal used in a feedback circuit. The feedback controls the velocity of pumping in conjunction with programmed values to avoid destructive reverse torque. A cam in the pump controls piston stroke, has a depressurization portion with an initial slope equal to but in the opposite direction of the final slope, rounded transition slopes, increasing linear velocity to the refill portion and constant velocity in the refill portion.
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10.发明授权Apparatus and method for pumping supercritical fluid and measuring flow thereof 失效用于泵送超临界流体并测量其流量的装置和方法
公开(公告)号：US5755559A
公开(公告)日：1998-05-26
申请号：US673177
申请日：1996-06-26
申请人： Robert William Allington , Daniel Gene Jameson , Dale A. Davison , Dale Clay , Robin R. Winter , Yoossef Tehrani
发明人： Robert William Allington , Daniel Gene Jameson , Dale A. Davison , Dale Clay , Robin R. Winter , Yoossef Tehrani
IPC分类号： B01D11/00 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F04B53/08 , F04B53/14 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015 , F04B49/00
CPC分类号： G01N1/34 , B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B53/08 , F04B53/143 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/40 , G01N30/28 , G21F5/015 , F04B2201/0209 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02
摘要： In a piston pump for pumping liquid carbon dioxide at a temperature below 30 degrees Fahrenheit and pressures at least as high as 7500 psi, the volume leaving the pump is determined by measuring only pressure or other parameter related to flow and movement of the plunger. The position of the piston is measured and the resulting displacement is integrated to determine volume of fluid pumped.
摘要翻译： 在用于在低于30华氏度的温度下泵送液体二氧化碳和至少高达7500psi的压力的活塞泵中，通过仅测量与柱塞的流动和运动相关的压力或其它参数来确定离开泵的体积。 测量活塞的位置，并将所得到的位移整合在一起，以确定泵送的流体体积。
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