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    Sucralose production method
    1.
    发明申请
    Sucralose production method 审中-公开
    三氯蔗糖生产方法

    公开(公告)号：US20080234472A1

    公开(公告)日：2008-09-25

    申请号：US12009455

    申请日：2008-01-18

    申请人： Duane Leinhos ,  John Kerr ,  Bob Jansen ,  Sebastien Camborieux ,  Peter Lloyd-Jones ,  Anthony Baiada

    发明人： Duane Leinhos ,  John Kerr ,  Bob Jansen ,  Sebastien Camborieux ,  Peter Lloyd-Jones ,  Anthony Baiada

    IPC分类号： C07H1/00

    CPC分类号： C07H5/02

    摘要： There is provided a method for the production of sucralose from a feed stream resulting from the chlorination of a sucrose-6-acylate in a reaction vehicle, said feed stream comprising a sucralose-6-acylate, the reaction vehicle, and by-products including high molecular weight coloured material, said method comprising: deacylation of the sucralose-6-acylate by treatment with a base to afford sucralose, and, before or after said deacylation, removal of the reaction vehicle and isolation of the sucralose characterised in that immediately before the removal of the reaction vehicle, the reaction stream is subjected to a precipitation step comprising treatment with a metal or ammonium hydroxide and carbon dioxide to form a precipitate of the corresponding metal or ammonium carbonate in which at least a portion of said high molecular weight coloured material is trapped, followed by separation of said precipitate.

    摘要翻译： 提供了从反应载体中的蔗糖-6-酰化物氯化得到的进料流中生产三氯蔗糖的方法，所述进料流包含三氯半乳蔗糖-6-酰化物，反应载体和副产物，包括 所述方法包括：用碱处理三氯半乳蔗糖-6-酰化物脱酰基，得到三氯半乳蔗糖，并且在所述脱酰化之前或之后，除去反应载体和分离三氯半乳蔗糖，其特征在于，紧接在之前 去除反应载体，将反应物流进行沉淀步骤，包括用金属或氢氧化铵和二氧化碳处理以形成相应的金属或碳酸铵的沉淀物，其中至少部分所述高分子量着色 材料被捕获，然后分离所述沉淀物。

    Corn Wet Milling Process
    3.
    发明申请
    Corn Wet Milling Process 审中-公开
    玉米湿磨工艺

    公开(公告)号：US20090238918A1

    公开(公告)日：2009-09-24

    申请号：US12357555

    申请日：2009-01-22

    申请人： Robert Jansen ,  John Kerr ,  Peter Lloyd-Jones ,  Richard Tanner

    发明人： Robert Jansen ,  John Kerr ,  Peter Lloyd-Jones ,  Richard Tanner

    IPC分类号： C12C11/07 ,  C12C1/16

    CPC分类号： C13K1/06 ,  C08B30/044 ,  C12P7/06 ,  C12P19/14 ,  Y02E50/17

    摘要： A corn wet-milling process comprises steeping corn kernels in an aqueous liquid, which produces softened corn; milling the softened corn in a first mill, which produces a first milled corn; separating germ from the first milled corn, thereby producing a germ-depleted first milled corn; milling the germ-depleted first milled corn in a second mill, producing a second milled corn; separating the second milled corn into a first starch/protein portion that comprises starch and protein and a first fiber portion that comprises fiber, starch, and protein; milling the first fiber portion in a third mill, which produces a milled fiber material that comprises fiber, starch, and protein; separating at least some of the starch and protein in the milled fiber material from the fiber therein, producing a second fiber portion that comprises fiber and starch and a second starch/protein portion that comprises starch and protein; and contacting the second fiber portion with at least one enzyme to convert at least some of the starch therein to dextrose. The converted material is screened using one or more screens to separate the fiber from the liquor. The liquor can be fermented to ethanol, or refined to dextrose. The fiber can be pressed and dried as an animal feed.

    摘要翻译： 玉米湿法研磨方法包括在含水液体中浸泡玉米粒，产生软化的玉米; 在第一磨机中研磨软化的玉米，其生产第一研磨的玉米; 将胚芽与第一磨碎的玉米分离，从而产生一种无菌的第一磨碎的玉米; 在第二磨机中研磨灭菌的第一批玉米，生产第二批玉米; 将第二研磨的玉米分离成包含淀粉和蛋白质的第一淀粉/蛋白质部分和包含纤维，淀粉和蛋白质的第一纤维部分; 在第三磨机中研磨第一纤维部分，其产生包含纤维，淀粉和蛋白质的研磨纤维材料; 将磨碎的纤维材料中的至少一些淀粉和蛋白质与其中的纤维分离，产生包含纤维和淀粉的第二纤维部分和包含淀粉和蛋白质的第二淀粉/蛋白质部分; 以及使所述第二纤维部分与至少一种酶接触以将其中的至少一些淀粉转化成葡萄糖。 使用一个或多个筛网筛选转化的材料以将纤维与液体分离。 酒可以发酵成乙醇，或精制成葡萄糖。 纤维可以作为动物饲料被压制和干燥。

    Cereal Refining Process
    4.
    发明申请
    Cereal Refining Process 审中-公开
    谷物精制工艺

    公开(公告)号：US20090095286A1

    公开(公告)日：2009-04-16

    申请号：US12173257

    申请日：2008-07-15

    申请人： John Kerr ,  Robert Jansen ,  Loren Luppes ,  Peter Lloyd-Jones ,  Richard Tanner

    发明人： John Kerr ,  Robert Jansen ,  Loren Luppes ,  Peter Lloyd-Jones ,  Richard Tanner

    IPC分类号： C08B30/00

    CPC分类号： C12M43/04 ,  A23J1/12 ,  A23L7/152 ,  A23L7/197 ,  C12M21/04 ,  C12M21/12 ,  C12P5/023 ,  C12P7/06 ,  F23G2900/50208 ,  Y02E50/17 ,  Y02E50/343

    摘要： A process including steeping cereal kernels in an aqueous liquid, producing softened cereal; milling the softened cereal, producing a milled cereal comprising germ, protein, starch, and fiber; separating at least some of at least one material selected from the group consisting of germ, starch, and protein from the milled cereal, producing at least one of germ, starch, and a first protein portion, and also producing a first fiber portion that comprises fiber and starch, and a light steep water that comprises protein; separating at least some protein from the light steep water, producing a second protein portion and a process water that comprises protein; converting at least some of the starch in the first fiber portion to saccharides; separating at least some of the saccharides from the first fiber portion, producing saccharides and a second fiber portion that comprises fiber; and burning at least some of the fiber from the second fiber portion, producing a flue gas and a first quantity of energy; wherein the process further comprises at least one step selected from the group consisting of least partially powering at least one previous step with the first quantity of energy; and drying at least one separated material selected from the group consisting of the germ, the starch, the first protein portion, the second protein portion, and the saccharides with the flue gas, producing a dried separated material and a dryer exhaust. In one further embodiment, the process further includes digesting anaerobically the biologically available organic residues from the process water, producing a biogas and a final waste water. In a still further embodiment, the process further includes burning the biogas to produce a second quantity of energy and at least partially powering at least one previous step with the second quantity of energy.

    摘要翻译： 一种包括在水性液体中浸泡谷粒的方法，产生软化谷物; 研磨软化谷物，生产包含胚芽，蛋白质，淀粉和纤维的碾磨谷物; 从磨碎的谷物中分离至少一种选自细菌，淀粉和蛋白质的至少一种材料，产生胚芽，淀粉和第一蛋白质部分中的至少一种，并且还产生第一纤维部分，其包含 纤维和淀粉，以及包含蛋白质的轻陡的水; 从轻水中分离出至少一些蛋白质，产生第二蛋白质部分和包含蛋白质的工艺水; 将第一纤维部分中的至少一些淀粉转化为糖; 从第一纤维部分分离出至少一些糖类，生成糖类和包含纤维的第二纤维部分; 并且从第二纤维部分燃烧至少一些纤维，产生烟道气和第一量的能量; 其中所述方法还包括至少一个步骤，所述步骤选自由对所述第一能量的至少一个先前步骤进行的至少部分供电; 并用烟道气干燥选自由胚芽，淀粉，第一蛋白质部分，第二蛋白质部分和糖类组成的组中的至少一种分离的材料，产生干燥的分离的材料和干燥器排气。 在一个另外的实施方案中，该方法还包括厌氧地从工艺水中消化生物可获得的有机残余物，产生沼气和最终的废水。 在又一个实施例中，该方法还包括燃烧沼气以产生第二数量的能量，并且至少部分地为第二数量的能量提供至少一个先前步骤。