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    Process for producing organotin compounds
    1.
    发明授权
    Process for producing organotin compounds 失效
    生产有机锡化合物的方法

    公开(公告)号：US4195029A

    公开(公告)日：1980-03-25

    申请号：US958761

    申请日：1978-11-08

    申请人： Eberhard Otto ,  Wolfgang Wehner ,  Hermann O. Wirth

    发明人： Eberhard Otto ,  Wolfgang Wehner ,  Hermann O. Wirth

    IPC分类号： A01N55/04 ,  C07F7/22 ,  C08G18/24

    CPC分类号： C08G18/242 ,  A01N55/04 ,  C07F7/2216

    摘要： A process for producing organotin compounds of the formula I ##STR1## in which X is a chlorine, bromine or iodine atom, theR's independently of one another are each a hydrogen atom or alkyl, andY is OH, NH.sub.2 or OR', whereinR' is a hydrocarbon group which optionally contains a functional group and which is of aliphatic, cycloaliphatic or aromatic character,by the direct reaction of a tin dihalide with an unsaturated nitrile of the formula II ##STR2## in which R has the aforesaid meaning, and with hydrogen chloride, hydrogen bromide or hydrogen iodide, in which process the reaction is performed in the presence of water, of a carboxylic acid, or of water and alcohol, or of at least 3 mols of alcohol per mol of nitrile.

    摘要翻译： 制备式I的有机锡化合物（I）其中X是氯，溴或碘原子，R相互独立地是氢原子或烷基，Y是OH，NH2或OR '，其中R'是任选地含有官能团并且具有脂肪族，脂环族或芳族性质的烃基，其通过二卤化二锡与式II（II）的不饱和腈的直接反应，在 其中R具有上述含义，并与氯化氢，溴化氢或碘化氢反应，其中反应在水，羧酸或水和醇或至少3摩尔醇的存在下进行 每摩尔腈。

    .beta.-keto esters as stabilizers for chlorinated polymers
    2.
    发明授权
    .beta.-keto esters as stabilizers for chlorinated polymers 失效
    （BETA） - 作为氯化聚合物的稳定剂的麦芽糖

    公开(公告)号：US5177135A

    公开(公告)日：1993-01-05

    申请号：US621497

    申请日：1990-12-03

    申请人： Wolfgang Wehner ,  Hermann O. Wirth

    发明人： Wolfgang Wehner ,  Hermann O. Wirth

    IPC分类号： C08K5/09 ,  C08K5/098 ,  C08K5/101 ,  C08K5/103 ,  C08K5/13 ,  C08K5/138 ,  C08K5/37 ,  C08K5/372 ,  C08L101/04

    CPC分类号： C08K5/138 ,  C08K5/098 ,  C08K5/101 ,  C08K5/103 ,  C08K5/372

    摘要： A composition comprisinga) a chlorinated polymer,b) at least one Me(II) carboxylate and/or Me(II) phenolate and/or Me(II) alkylphenolate, wherein Me(II) is Ba, Ca, Mg, Cd, Sr or Zn, andc) at least one compound of formula (I) ##STR1## wherein n is 1, 2, 3, 4 or 6 and, when n=1, R is phenyl and X is an alkyl group of 10 to 20 carbon atoms, when n=2, R is alkyl of 1 to 4 carbon atoms or phenyl, and X is alkylene of 4 to 12 carbon atoms, alkylene of 2 to 12 carbon atoms which is substituted by at least one C.sub.1 -C.sub.8 alkyl group, or is --CH.sub.2 --CH.sub.2 --S--CH.sub.2 --CH.sub.2 --S--CH.sub.2 --CH.sub.2 -- or --CH.sub.2 --CH.sub.2 --S--CH.sub.2 --CH.sub.2 --, when n=3, R is alkyl of 1 to 4 carbon atoms of phenyl and X is CH.sub.3 CH.sub.2 C(CH.sub.2 --).sub.3, when n=4, R is alkyl of 1 to 4 carbon atoms or phenyl and X is a group ##STR2## wherein m is 0 or 1, and, when n=6, R is alkyl of 1 to 4 carbon atoms or phenyl and X is the group ##STR3##

    摘要翻译： 一种组合物，其包含a）氯化聚合物，b）至少一种羧酸Me（II）和/或Me（I​​I）酚盐和/或Me（I​​I）烷基酚盐，其中Me（II）是Ba，Ca，Mg，Cd， Sr或Zn，和c）至少一种式（I）化合物其中n为1,2,3,4或6，当n = 1时，R为苯基，X为烷基 当n = 2时，R为1至4个碳原子的烷基或苯基，X为4至12个碳原子的亚烷基，2至12个碳原子的亚烷基，被至少一个C1 -C 8烷基或-CH 2 -CH 2 -S-CH 2 -CH 2 -S-CH 2 -CH 2 - 或-CH 2 -CH 2 -S-CH 2 -CH 2 - ，当n = 3时，R是1至4个碳原子的烷基 的苯基，X为CH 3 CH 2 C（CH 2 - ）3，当n = 4时，R为1〜4个碳原子的烷基或苯基，X为基团，其中m为0或1，当n = 6时， R为1至4个碳原子的烷基或苯基，X为基团

    Organotin compounds
    3.
    发明授权
    Organotin compounds 失效
    有机锡化合物

    公开(公告)号：US4188334A

    公开(公告)日：1980-02-12

    申请号：US939944

    申请日：1978-09-06

    申请人： Wolfgang Wehner ,  Hermann O. Wirth

    发明人： Wolfgang Wehner ,  Hermann O. Wirth

    IPC分类号： A01N55/04 ,  C07F7/22 ,  C08G18/00 ,  C08G18/22

    CPC分类号： C07F7/2216

    摘要： Organotin compounds of the general formula ##STR1## wherein X is a chlorine, bromine or iodine atom,R is a hydrogen atom and/or an alkyl radical,Z is an oxygen or sulfur atom, andR' is a hydrocarbon group of aliphatic, cycloaliphatic or aromatic character which can contain functional groups,and a process for their production by the direct reaction of a tin dihalide with an unsaturated nitrile.The organotin compounds are used as intermediates for the production of organotin stabilizers for halogen-containing thermoplastics.

    摘要翻译： 有机锡化合物，其通式为：其中X为氯，溴或碘原子，R为氢原子和/或烷基，Z为氧或硫原子，R'为脂族， 可以含有官能团的脂环族或芳族特征，以及通过二卤化锡与不饱和腈的直接反应生产的方法。 有机锡化合物用作生产含卤素热塑性塑料的有机锡稳定剂的中间体。

    Chlorinated thermoplastics stabilized with aminouracils
    4.
    发明授权
    Chlorinated thermoplastics stabilized with aminouracils 失效
    用氨基尿嘧啶稳定的氯化热塑性塑料

    公开(公告)号：US4656209A

    公开(公告)日：1987-04-07

    申请号：US378540

    申请日：1982-05-17

    申请人： Wolfgang Wehner ,  Hermann O. Wirth

    发明人： Wolfgang Wehner ,  Hermann O. Wirth

    IPC分类号： C08K5/3462 ,  C08K5/34

    CPC分类号： C08K5/3462

    摘要： The invention relates to thermoplastic molding compositions based on vinyl chloride polymers and containing, as stabilizer, 0.1 to 5% by weight of an aminouracil of the formula I ##STR1## wherein R.sup.1 is hydrogen, C.sub.1 -C.sub.8 alkyl, C.sub.5 -C.sub.8 cycloalkyl, phenyl, benzyl, C.sub.1 -C.sub.4 hydroxyalkyl, hydroxyphenyl, C.sub.2 -C.sub.8 alkoxyalkyl, C.sub.2 -C.sub.8 alkylthioalkyl, C.sub.6 -C.sub.10 cycloalkoxyalkyl, C.sub.6 -C.sub.10 cycloalkylthioalkyl, C.sub.8 -C.sub.14 aralkoxyalkyl, C.sub.8 -C.sub.14 aralkylthioalkyl, C.sub.7 -C.sub.14 aryloxyalkyl, C.sub.7 -C.sub.14 arylthioalkyl, --NHR.sup.4, in which R.sup.4 is hydrogen, phenyl or chlorine-substituted phenyl, and R.sup.2 and R.sup.3, each independently of the other, are C.sub.2 -C.sub.21 alkyl, C.sub.6 -C.sub.12 aryl or C.sub.7 -C.sub.19 aralkyl, while one of R.sup.2 and R.sup.3 may also be hydrogen.The addition of such aminouracils gives vinyl chloride polymers which are very well protected against heat-induced degradation. The aminouracils cause no haze in the polymer to be protected.

    摘要翻译： 本发明涉及基于氯乙烯聚合物的热塑性模塑组合物，其含有0.1至5重量％的式I（I）的氨基脲，其中R 1是氢，C 1 -C 8烷基，C 5 -C 8环烷基， 苯基，苄基，C 1 -C 4羟烷基，羟基苯基，C 2 -C 8烷氧基烷基，C 2 -C 8烷硫基烷基，C 6 -C 10环烷氧基烷基，C 6 -C 10环烷硫基烷基，C 8 -C 14芳烷氧基烷基，C 8 -C 14芳烷硫基烷基，C 7 -C 14芳氧烷基，C 7 -C 14芳硫基烷基，-NHR 4，其中R 4为氢 ，苯基或氯取代的苯基，R 2和R 3各自独立地是C 2 -C 21烷基，C 6 -C 12芳基或C 7 -C 19芳烷基，而R 2和R 3之一也可以是氢。 加入这样的氨基脲可提供非常良好的防止热诱导降解的氯乙烯聚合物。 氨基尿嘧啶在聚合物中不会引起雾霾的保护。

    Stabilized chlorine-containing polymer compositions
    6.
    发明授权
    Stabilized chlorine-containing polymer compositions 失效
    稳定的含氯聚合物组合物

    公开(公告)号：US5350785A

    公开(公告)日：1994-09-27

    申请号：US58853

    申请日：1993-05-06

    申请人： Hans J. Sander ,  Olaf-Rene Hartmann ,  Hermann O. Wirth ,  Wolfgang Wehner

    发明人： Hans J. Sander ,  Olaf-Rene Hartmann ,  Hermann O. Wirth ,  Wolfgang Wehner

    IPC分类号： C08K3/22 ,  C08K3/24 ,  C08K3/26 ,  C08K3/34 ,  C08K3/36 ,  C08K5/00 ,  C08K5/09 ,  C08K5/17 ,  C08K5/34 ,  C08K13/02 ,  C08L23/28 ,  C08L101/04 ,  C08K5/3435

    CPC分类号： C08K5/0008 ,  C08K13/02 ,  C08K3/34

    摘要： Stabilized chlorine-containing polymer compositions comprising a chlorine-containing polymer and a stabilizer mixture comprising:a) at least one cyclic or non-cyclic, sterically hindered amine,b) at least one organic zinc compound and/or inorganic zinc compound from the series consisting of carbonates, chlorides, sulfates, oxides, hydroxides, basic oxides and mixed oxides, andc) at least one compound from the series consisting of the crystalline alkali metal/alkaline earth metal aluminosilicates, and, if desired,d) at least one 1,3-diketone and/ore) at least one organic or inorganic calcium compound.Polymer compositions of this type are preferably employed for slush mould and crash pad applications.

    摘要翻译： 包含含氯聚合物和稳定剂混合物的稳定含氯聚合物组合物，其包含：a）至少一种环状或非环状空间位阻胺，b）至少一种来自该系列的有机锌化合物和/或无机锌化合物 由碳酸盐，氯化物，硫酸盐，氧化物，氢氧化物，碱性氧化物和混合氧化物组成，以及c）至少一种由结晶碱金属/碱土金属铝硅酸盐组成的系列化合物，如果需要，d）至少一种 1,3-二酮和/或e）至少一种有机或无机钙化合物。 这种类型的聚合物组合物优选用于糊模和碰撞垫应用。

    Coordination-polymeric triethanolamineperchlorato(triflato)metal inner complexes as additives for synthetic polymers
    8.
    发明授权
    Coordination-polymeric triethanolamineperchlorato(triflato)metal inner complexes as additives for synthetic polymers 有权
    配位聚合三乙醇胺（triflato）金属内复合物作为合成聚合物的添加剂

    公开(公告)号：US07741390B2

    公开(公告)日：2010-06-22

    申请号：US11964671

    申请日：2007-12-26

    申请人： Wolfgang Wehner ,  Trupti Dave ,  Thomas Wannemacher

    发明人： Wolfgang Wehner ,  Trupti Dave ,  Thomas Wannemacher

    IPC分类号： C08K5/34 ,  C08G73/02

    CPC分类号： C08K5/005 ,  C08K5/0091 ,  C08L27/06

    摘要： Stabilizer system for chlorinated polymers, especially PVC, comprising at least one coordination-polymeric triethanolamineperchlorato(triflato)metal inner complex comprising the monomer unit of the formula (A) The stabilizer system may additionally comprise substituted cyanoacetylureas or/and 6-aminouracils or/and 3-aminocrotonic esters or/and hydantoins or/and monomeric or polymeric dihydropyridines or alkaline earth metal hydroxides or/and hydrotalcites or/and dawsonites or/and zeolites or/and glycidyl compounds or/and cyanamides or/and cyanoguanidines or/and melamines. In addition, phosphites or/and sterically hindered amines or/and NOR-HALS compounds may be present.

    摘要翻译： 用于氯化聚合物，特别是PVC的稳定剂体系包含至少一种包含式（A）的单体单元的配位聚合的三乙醇胺三（三氟甲基）金属内复合物。稳定剂体系可以另外包含取代的氰基乙酰脲或/和6-氨基尿嘧啶或/和 3-氨基巴豆酸酯或/和乙内酰脲或/和单体或聚合二氢吡啶或碱土金属氢氧化物或/和水滑石或/和片钠铝石或/和沸石或/和缩水甘油基化合物或/和氰酰胺或/和氰胍胺或/和三聚氰胺。 此外，可能存在亚磷酸酯或/和空间位阻胺或/和NOR-HALS化合物。

    COORDINATION-POLYMERIC TRIETHANOLAMINEPERCHLORATO(TRIFLATO)METAL INNER COMPLEXES AS ADDITIVES FOR SYNTHETIC POLYMERS
    10.
    发明申请
    COORDINATION-POLYMERIC TRIETHANOLAMINEPERCHLORATO(TRIFLATO)METAL INNER COMPLEXES AS ADDITIVES FOR SYNTHETIC POLYMERS 有权
    作为合成聚合物的添加剂的协调 - 聚合三乙醇胺金属（三氟化硫）金属内部复合物

    公开(公告)号：US20090131564A1

    公开(公告)日：2009-05-21

    申请号：US11964671

    申请日：2007-12-26

    申请人： Wolfgang Wehner ,  Trupti Dave ,  Thomas Wannemacher

    发明人： Wolfgang Wehner ,  Trupti Dave ,  Thomas Wannemacher

    IPC分类号： C08L27/06

    CPC分类号： C08K5/005 ,  C08K5/0091 ,  C08L27/06

    摘要： Stabilizer system for chlorinated polymers, especially PVC, comprising at least one coordination-polymeric triethanolamineperchlorato(triflato)metal inner complex comprising the monomer unit of the formula (A) The stabilizer system may additionally comprise substituted cyanoacetylureas or/and 6-aminouracils or/and 3-aminocrotonic esters or/and hydantoins or/and monomeric or polymeric dihydropyridines or alkaline earth metal hydroxides or/and hydrotalcites or/and dawsonites or/and zeolites or/and glycidyl compounds or/and cyanamides or/and cyanoguanidines or/and melamines. In addition, phosphites or/and sterically hindered amines or/and NOR-HALS compounds may be present.

    摘要翻译： 用于氯化聚合物，特别是PVC的稳定剂体系包含至少一种包含式（A）的单体单元的配位聚合的三乙醇胺三（三氟甲基）金属内复合物。稳定剂体系可以另外包含取代的氰基乙酰脲或/和6-氨基尿嘧啶或/和 3-氨基巴豆酸酯或/和乙内酰脲或/和单体或聚合二氢吡啶或碱土金属氢氧化物或/和水滑石或/和片钠铝石或/和沸石或/和缩水甘油基化合物或/和氰酰胺或/和氰胍胺或/和三聚氰胺。 此外，可能存在亚磷酸酯或/和空间位阻胺或/和NOR-HALS化合物。