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1.发明申请公开(公告)号：US20150170783A1
公开(公告)日：2015-06-18
申请号：US14109008
申请日：2013-12-17
CPC分类号： H01B1/127 , C08G2261/1412 , C08G2261/212 , C08G2261/3223 , C08G2261/51 , C08G2261/512 , C08G2261/92 , C08K5/56 , C09D165/00 , H01L31/00 , H01L51/0037 , H01L51/0083 , H01L51/0566 , C08L65/00
摘要： Disclosed herein is a composition comprising a regioregular polyalkylthiophene and/or a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene]; and a metallocene; where the metallocene is present in an amount of greater than 50 wt %, based on the total weight of the composition. Disclosed herein too is a method of manufacturing a thin film comprising dissolving a regioregular polyalkylthiophene or a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] in a solvent to form a solution; dissolving a metallocene in the solution; disposing the solution on a substrate; and annealing the substrate.
摘要翻译： 本文公开了包含区域性多烷基噻吩和/或区域性聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]的组合物。 和茂金属; 其中基于组合物的总重量，金属茂以大于50重量％的量存在。 本文也公开了一种制造薄膜的方法，其包括将溶解有约数量的聚烷基噻吩或区域性聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]溶解在溶剂中形成 一个办法; 将金属茂溶解在溶液中; 将溶液置于基材上; 并退火衬底。
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2.发明授权公开(公告)号：US09336921B2
公开(公告)日：2016-05-10
申请号：US14109008
申请日：2013-12-17
CPC分类号： H01B1/127 , C08G2261/1412 , C08G2261/212 , C08G2261/3223 , C08G2261/51 , C08G2261/512 , C08G2261/92 , C08K5/56 , C09D165/00 , H01L31/00 , H01L51/0037 , H01L51/0083 , H01L51/0566 , C08L65/00
摘要： Disclosed herein is a composition comprising a regioregular polyalkylthiophene and/or a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene]; and a metallocene; where the metallocene is present in an amount of greater than 50 wt %, based on the total weight of the composition. Disclosed herein too is a method of manufacturing a thin film comprising dissolving a regioregular polyalkylthiophene or a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] in a solvent to form a solution; dissolving a metallocene in the solution; disposing the solution on a substrate; and annealing the substrate.
摘要翻译： 本文公开了包含区域性多烷基噻吩和/或区域性聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]的组合物。 和茂金属; 其中基于组合物的总重量，金属茂以大于50重量％的量存在。 本文也公开了一种制造薄膜的方法，其包括将溶解有约数量的聚烷基噻吩或区域性聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]溶解在溶剂中形成 一个办法; 将金属茂溶解在溶液中; 将溶液置于基材上; 并退火衬底。
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公开(公告)号：US10600964B2
公开(公告)日：2020-03-24
申请号：US14109032
申请日：2013-12-17
摘要： Disclosed herein is a composition comprising a regioregular oligothiophene, a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] and/or a benzothiophene; where the regioregular oligothiophene, the regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] and the benzothiophene each have a number average molecular weight of less than or equal to 475 grams per mole; where the composition is melted and then annealed at a temperature between a melting point and a glass transition temperature of the composition; the composition having a charge mobility that is greater than a comparative composition that is either not annealed or annealed at the same temperature between the melting point and the glass transition temperature but without being subjected to prior melting.
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4.发明申请公开(公告)号：US20150171331A1
公开(公告)日：2015-06-18
申请号：US14109032
申请日：2013-12-17
CPC分类号： H01L51/0036 , H01L51/0558
摘要： Disclosed herein is a composition comprising a regioregular oligothiophene, a regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] and/or a benzothiophene; where the regioregular oligothiophene, the regioregular poly[2,5-bis(3-alkylthiophen-2-yl)thieno(3,2-b)thiophene] and the benzothiophene each have a number average molecular weight of less than or equal to 475 grams per mole; where the composition is melted and then annealed at a temperature between a melting point and a glass transition temperature of the composition; the composition having a charge mobility that is greater than a comparative composition that is either not annealed or annealed at the same temperature between the melting point and the glass transition temperature but without being subjected to prior melting.
摘要翻译： 本文公开了一种组合物，其包含区域性低聚噻吩，区域规模聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]和/或苯并噻吩; 其中区域性低聚噻吩，区域规模聚[2,5-双（3-烷基噻吩-2-基）噻吩并（3,2-b）噻吩]和苯并噻吩各自的数均分子量小于或等于475 克/摩尔 其中组合物熔融，然后在组合物的熔点和玻璃化转变温度之间的温度下退火; 所述组合物的电荷迁移率大于在熔点和玻璃化转变温度之间的相同温度下未进行退火或退火但不进行先前熔融的比较组合物。
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公开(公告)号：US08808807B2
公开(公告)日：2014-08-19
申请号：US11566104
申请日：2006-12-01
IPC分类号： B01D69/00
CPC分类号： C08J5/22 , B01D67/0048 , B01D67/0088 , B01D67/0093 , B01D69/10 , B01D69/105 , B01D71/027 , B01D2323/38 , B01D2325/14 , C08J2383/02 , H01B1/06 , H01M8/1016 , H01M2300/0068
摘要： Novel membranes based on functionalized porous inorganic materials for ion exchange and conduction have been synthesized and characterized. The preparation procedure of these new membranes involves the synthesis of porous inorganic films, into which hydrophilic moieties are incorporated along the interior pore surfaces of the inorganic framework. Ion-conducting species are grafted into the pores via reactions with surface groups of the inorganic framework to allow for ion transport through the pore network.
摘要翻译： 基于用于离子交换和传导的官能化多孔无机材料的新型膜已被合成和表征。 这些新膜的制备方法涉及多孔无机膜的合成，其中亲水部分沿着无机骨架的内孔表面并入其中。 离子传导物质通过与无机骨架的表面基团的反应接枝到孔中，以允许离子通过孔网络传递。
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公开(公告)号：US20090162616A1
公开(公告)日：2009-06-25
申请号：US12335225
申请日：2008-12-15
CPC分类号： B81C1/00031 , B81C2201/0149 , B82Y20/00 , B82Y30/00 , H01L51/0012 , H01L51/005 , H01L51/5012 , Y10T428/2457 , Y10T428/2913
摘要： Methods of controlling orientational ordering in self-assembled materials are described. These methods include controlling the nucleation rate and growth of block-copolymer-templated silica domains to yield macroscopically aligned mesostructured materials, and forming patterned mesostructured films or monoliths with control over the direction of alignment of a hexagonally-packed, block-copolymer-directed mesostructure across macroscopic lengths scales are described. Self-assembled materials with controlled orientational ordering are described, including those that contain a surfactant or block-copolymer species, and materials that include an organic (e.g., resin) or inorganic (e.g., silica or titania) network-forming component.
摘要翻译： 描述了在自组装材料中控制取向排序的方法。 这些方法包括控制嵌段共聚物 - 模板二氧化硅域的成核速率和生长以产生宏观取向的介观结构材料，以及形成图案化的介孔结构化膜或整料，其对六边形填充的嵌段共聚物指向的介孔结构的取向方向进行控制 描述了宏观长度尺度。 描述了具有受控定向排列的自组装材料，包括含有表面活性剂或嵌段共聚物物质的材料，以及包括有机（例如树脂）或无机（例如二氧化硅或二氧化钛）网络形成组分的材料。
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公开(公告)号：US08563124B2
公开(公告)日：2013-10-22
申请号：US12367471
申请日：2009-02-06
申请人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
发明人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
CPC分类号： C01B32/00 , Y10T428/249953 , Y10T428/249956
摘要： Methods of forming an electrically-conductive mesoporous carbon structure with interconnected pores or highly interconnected pores, and the resulting structures are described. The structure is formed by providing a mesoporous template, filling the mesopores with an organic precursor, polymerizing the organic precursor, pyrolyzing the polymerized organic precursor, and etching away the template.
摘要翻译： 描述形成具有互连孔或高度互连的孔的导电介孔碳结构的方法，以及所得结构。 通过提供介孔模板，用有机前体填充介孔，聚合有机前体，热解聚合的有机前体和蚀刻掉模板来形成结构。
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公开(公告)号：US20090258213A1
公开(公告)日：2009-10-15
申请号：US12367471
申请日：2009-02-06
申请人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
发明人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
CPC分类号： C01B32/00 , Y10T428/249953 , Y10T428/249956
摘要： Methods of forming an electrically-conductive mesoporous carbon structure with interconnected pores or highly interconnected pores, and the resulting structures are described. The structure is formed by providing a mesoporous template, filling the mesopores with an organic precursor, polymerizing the organic precursor, pyrolyzing the polymerized organic precursor, and etching away the template.
摘要翻译： 描述形成具有互连孔或高度互连的孔的导电介孔碳结构的方法，以及所得结构。 通过提供介孔模板，用有机前体填充介孔，聚合有机前体，热解聚合的有机前体和蚀刻掉模板来形成结构。
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9.发明授权公开(公告)号：US08758653B2
公开(公告)日：2014-06-24
申请号：US12792590
申请日：2010-06-02
CPC分类号： C01B37/00 , C01B39/026 , C07F7/21
摘要： A material and method for producing mesostructured materials with multiple functionalities that are independently adjustable and collectively optimizable is provided. The method uses a series of discrete synthesis steps under otherwise mutually incompatible conditions, e.g., from acidic, alkaline, and/or non-aqueous solutions, allows different functionalities to be introduced to the materials and optimized. To illustrate the method, cubic mesoporous silica films were prepared from strongly acidic solutions that were separately functionalized under highly alkaline conditions to incorporate hydrophilic aluminosilica moieties and under non-aqueous conditions to introduce perfluorosulfonic-acid surface groups.
摘要翻译： 提供了一种用于生产具有独立可调整和可共同优化的多种功能的介观材料的材料和方法。 该方法在另外相互不相容的条件下使用一系列离散的合成步骤，例如从酸性，碱性和/或非水溶液中，允许将不同的官能团引入材料并进行优化。 为了说明该方法，从强酸性溶液制备立方介孔二氧化硅膜，其在高碱性条件下分别官能化以掺入亲水性铝硅氧烷部分，并在非水条件下引入全氟磺酸表面基团。
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公开(公告)号：US20100311856A1
公开(公告)日：2010-12-09
申请号：US12792590
申请日：2010-06-02
IPC分类号： C08J9/00
CPC分类号： C01B37/00 , C01B39/026 , C07F7/21
摘要： A material and method for producing mesostructured materials with multiple functionalities that are independently adjustable and collectively optimizable is provided. The method uses a series of discrete synthesis steps under otherwise mutually incompatible conditions, e.g., from acidic, alkaline, and/or non-aqueous solutions, allows different functionalities to be introduced to the materials and optimized. To illustrate the method, cubic mesoporous silica films were prepared from strongly acidic solutions that were separately functionalized under highly alkaline conditions to incorporate hydrophilic aluminosilica moieties and under non-aqueous conditions to introduce perfluorosulfonic-acid surface groups.
摘要翻译： 提供了一种用于生产具有独立可调整和可共同优化的多种功能的介观材料的材料和方法。 该方法在另外相互不相容的条件下使用一系列离散的合成步骤，例如从酸性，碱性和/或非水溶液中，允许将不同的官能团引入材料并进行优化。 为了说明该方法，从强酸性溶液制备立方介孔二氧化硅膜，其在高碱性条件下分别官能化以掺入亲水性铝硅氧烷部分，并在非水条件下引入全氟磺酸表面基团。
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