Process for the preparation of polyacetylene
    1.
    发明授权
    Process for the preparation of polyacetylene 失效
    聚乙炔的制备方法

    公开(公告)号:US4771115A

    公开(公告)日:1988-09-13

    申请号:US921145

    申请日:1986-10-21

    CPC分类号: C08F38/02

    摘要: Polyacetylene having an apparent density at 20.degree. C. greater than 0.6 g/ccm and a surface area below 60 m.sup.2 /g is prepared by polymerizing gaseous acetylene in the presence of a catalytic system consisting of:(a) an oxygenized compound of Ti or V, containing at least one metal-oxygen bond;(b) an organometallic compound of aluminum containing at least one hetero-atom, of the formula: ##STR1## wherein: ##STR2## while R=a hydrocarbon radical with 1-18 carbon atoms, and where R'.dbd.R, or halogen or alcoxyl.

    摘要翻译: 通过在催化体系存在下聚合气态乙炔来制备表观密度大于0.6g / cm 2,表面积低于60m 2 / g的聚乙炔,所述催化体系由以下组成:(a)Ti的氧化化合物或 V,含有至少一个金属 - 氧键; (b)含有至少一个杂原子的铝的有机金属化合物,其具有下式:其中:当R =具有1-18个碳原子的烃基,并且其中R'= R或卤素 或醇酸。

    Article based on a metal alloy of nickel, chromium and metalloid elements including microcrystalline precipitates, metal alloy and preparation method
    7.
    发明授权
    Article based on a metal alloy of nickel, chromium and metalloid elements including microcrystalline precipitates, metal alloy and preparation method 失效
    基于镍,铬和金属合金的元素,包括微晶沉淀物,金属合金及其制备方法

    公开(公告)号:US06461744B1

    公开(公告)日:2002-10-08

    申请号:US09736142

    申请日:2000-12-15

    IPC分类号: B21C3700

    摘要: A description follows of an article based on a nickel-chromium-silicon metal alloy, including microcrystalline borides, obtained by the rapid solidification and subsequent thermal treatment of a nickel-chromium-boron-silicon metal alloy comprising from 39.0 to 69.4 atom % of nickel, from 11.8 to 33.9 atom % of chromium, from 7.6 to 27.4 atom % of boron and from 7.6 to 17.5 atom % of silicon. The above article is preferably a tape or a sheet or a fiber having high mechanical properties and is particularly resistant to oxidation.

    摘要翻译: 以下描述的是基于包含微晶硼化物的镍 - 铬 - 硅金属合金制品,其通过快速凝固和随后的镍铬 - 硼 - 硅金属合金的热处理获得,所述镍 - 铬 - 硼 - 硅金属合金包含39.0-69.4原子%的镍 ,11.8至33.9原子%的铬,7.6至27.4原子%的硼和7.6至17.5原子%的硅。 上述制品优选是具有高机械性能的带或片或纤维,并且特别耐氧化。

    Method for the production of superconductive wires based on hollow filaments made of MgB2
    9.
    发明申请
    Method for the production of superconductive wires based on hollow filaments made of MgB2 审中-公开
    基于由MgB2制成的中空丝的超导丝的生产方法

    公开(公告)号:US20050159318A1

    公开(公告)日:2005-07-21

    申请号:US11074092

    申请日:2005-03-07

    摘要: A method is described for the production of superconductive wires based on hollow filaments made of MgB2, which comprises: a) the formation of a composite billet by means of the coaxial insertion in a tubular metallic container of a cylindrical bar made of metallic magnesium and amorphous boron powder in the interspace between the container and bar, said powder being pressed between the metallic container and the magnesium bar, in such a quantity that the weight ratio magnesium/boron is higher than 1.2; b) at least one plastic deformation treatment of the composite billet thus obtained until a wire with a prefixed diameter is obtained, with the subsequent winding of the wire onto a support; c) a thermal treatment of the filament product thus obtained, at a temperature ranging from 700° C. to 950° C. for a time ranging from 15 minutes to three hours.

    摘要翻译: 描述了一种用于生产基于由MgB 2 N 2制成的中空丝的超导丝的方法,其包括:a)通过同轴插入在管状金属容器中形成复合坯料 在金属容器和镁棒之间的间隙中将金属镁和无定形硼粉制成的圆柱形棒在金属容器和镁棒之间的间隙中,镁/硼的重量比高于1.2; b)对由此获得的复合钢坯进行至少一次塑性变形处理,直到获得具有预定直径的钢丝,随后将钢丝卷绕到支撑件上; c)将由此获得的长丝产品在700℃至950℃的温度范围内热处理15分钟至3小时。