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    Microgels and process for their preparation
    1.
    发明授权
    Microgels and process for their preparation 有权
    微凝胶及其制备方法

    公开(公告)号：US06462114B2

    公开(公告)日：2002-10-08

    申请号：US09969710

    申请日：2001-10-03

    申请人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    发明人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    IPC分类号： C08K310

    CPC分类号： C08F265/04 ,  C08F290/04 ,  C08F290/061 ,  C08F293/00 ,  C08F293/005 ,  Y10S514/944

    摘要： A process for forming a microgel which comprises a crosslinked core and a multiplicity of linear polymeric arms attached to the core, wherein the process comprises (a) first forming a halogen atom terminated prepolymer with a weight average molecular weight from 1,000 to 25,000 by polymerizing monoethylenically unsaturated monomers in the presence of an organic sulfonyl halide, an organic complexing agent and a transition metal (i.e., Cu, Ru, Ni, Re, Pd, Fe, or Rh); and (b) subsequently polymerizing the prepolymer with a mixture of monoethylenically unsaturated monomers and 0.5 to 60 mole percent, based on the total moles of monomer and prepolymer, of multi-olefinic polymerizable monomers to form a microgel with a weight average molecular weight of 10,000 to 100,000,000 and crosslinked core.

    摘要翻译： 一种形成微凝胶的方法，其包括交联核心和连接到核心上的多个线性聚合物臂，其中所述方法包括（a）首先通过聚合单烯属化合物形成重均分子量为1,000至25,000的卤素原子封端的预聚物 在有机磺酰卤，有机络合剂和过渡金属（即Cu，Ru，Ni，Re，Pd，Fe或Rh）存在下的不饱和单体; 和（b）随后将单体烯属不饱和单体的混合物和基于单体和预聚物的总摩尔数为0.5至60摩尔％的多烯属可聚合单体聚合预聚物以形成重均分子量为10,000的微凝胶 至100,000,000和交联核心。

    Microgels and process for their preparation
    2.
    发明授权
    Microgels and process for their preparation 有权
    微凝胶及其制备方法

    公开(公告)号：US06822056B2

    公开(公告)日：2004-11-23

    申请号：US09969704

    申请日：2001-10-03

    申请人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    发明人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    IPC分类号： C08F400

    CPC分类号： C08F265/04 ,  C08F290/04 ,  C08F290/061 ,  C08F293/00 ,  C08F293/005 ,  Y10S514/944

    摘要： A process for preparing microgel(s) that uses a wide range of activatable prepolymers; in the process, a polymer composition of crosslinked component A and soluble components B and C is formed from mono-olefinic and multi-olefinic monomers in the presence of catalyst and initiator; the process comprises: I) introducing mono-olefinic monomer, catalyst, and initiator into a reactor in the absence of multi-olefinic monomer and producing an activatable prepolymer, component B; II) contacting the product of I) with multi-olefinic monomer to produce components A and C, optionally in the presence of additional initiator; also optionally in the presence of additional mono-olefinic monomer and initiator; the ratio of components A/(B+C) can be controlled by varying the mole ratio of Component B/multi-olefinic monomer from 0.05/1 up to 5/1, by decreasing the mole ratio to increase the ratio of A/(B+C), and increasing the mole ratio to decrease the ratio of A/(B+C).

    摘要翻译： 一种制备使用广泛可活化预聚物的微凝胶的方法; 在该方法中，交联组分A和可溶组分B和C的聚合物组合物在催化剂和引发剂存在下由单烯烃和多烯属单体形成; 该方法包括：I）在不存在多烯属单体的情况下将单烯烃单体，催化剂和引发剂引入反应器，并产生可活化的预聚物组分B; II）使I）的产物与多烯属单体接触， 产生组分A和C，任选地在另外的引发剂的存在下; 也可任选在另外的单烯烃单体和引发剂的存在下进行; 可以通过将组分B /多烯烃单体的摩尔比从0.05 / 1增加到5/1来控制组分A /（B + C）的比例，通过降低摩尔比以增加A /（ B + C），并增加摩尔比以降低A /（B + C）的比例。

    Microgels and process for their preparation
    3.
    发明授权
    Microgels and process for their preparation 有权
    微凝胶及其制备方法

    公开(公告)号：US06355718B1

    公开(公告)日：2002-03-12

    申请号：US09350243

    申请日：1999-07-09

    申请人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    发明人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    IPC分类号： C08F29300

    CPC分类号： C08F265/04 ,  C08F290/04 ,  C08F290/061 ,  C08F293/00 ,  C08F293/005 ,  Y10S514/944

    摘要： A process for preparing microgel(s) that uses a wide range of activatable prepolymers; in the process, a polymer composition of crosslinked component A and soluble components B and C is formed from mono-olefinic and multi-olefinic monomers in the presence of catalyst and initiator; the process comprises: I) introducing mono-olefinic monomer, catalyst, and initiator into a reactor in the absence of multi-olefinic monomer and producing an activatable prepolymer, component B; II) contacting the product of I) with multi-olefinic monomer to produce components A and C, optionally in the presence of additional initiator; also optionally in the presence of additional mono-olefinic monomer and initiator; the ratio of components A/(B+C) can be controlled by varying the mole ratio of Component B/ multi-olefinic monomer from 0.05/1 up to 5/1, by decreasing the mole ratio to increase the ratio of A/(B+C), and increasing the mole ratio to decrease the ratio of A/(B+C).

    摘要翻译： 一种制备使用广泛可活化预聚物的微凝胶的方法; 在该方法中，交联组分A和可溶组分B和C的聚合物组合物在催化剂和引发剂存在下由单烯烃和多烯属单体形成; 该方法包括：I）在不存在多烯属单体的情况下将单烯烃单体，催化剂和引发剂引入反应器，并产生可活化的预聚物，组分B; II）使I）的产物与多烯属单体接触以产生组分A和C，任选地在另外的引发剂的存在下; 也可任选在另外的单烯烃单体和引发剂的存在下进行; 可以通过将组分B /多烯烃单体的摩尔比从0.05 / 1增加到5/1来控制组分A /（B + C）的比例，通过降低摩尔比以增加A /（ B + C），并且增加摩尔比以降低A /（B + C）的比例。

    Microgels and process for their preparation
    6.
    发明授权
    Microgels and process for their preparation 有权
    微凝胶及其制备方法

    公开(公告)号：US06646055B2

    公开(公告)日：2003-11-11

    申请号：US09969706

    申请日：2001-10-03

    申请人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    发明人： Charles T. Berge ,  Michael Fryd ,  Jeffrey W. Johnson ,  Graeme Moad ,  Ezio Rizzardo ,  Christopher Scopazzi ,  San Hoa Thang

    IPC分类号： C08F238

    CPC分类号： C08F265/04 ,  C08F290/04 ,  C08F290/061 ,  C08F293/00 ,  C08F293/005 ,  Y10S514/944

    摘要： A process for preparing microgel(s) that uses a wide range of activatable prepolymers. In the process, a polymer composition of crosslinked component A and soluble components B and C is formed from mono-olefinic and multi-olefinic monomers in the presence of catalyst and initiator. The process comprises: I) introducing mono-olefinic monomer, catalyst, and initiator into a reactor in the absence of multi-olefinic monomer and producing an activatable prepolymer, component B; II) contacting the product of I) with multi-olefinic monomer to produce components A and C, optionally in the presence of additional initiator; also optionally in the presence of additional mono-olefinic monomer and initiator. The ratio of components A/(B+C) can be controlled by varying the mole ratio of The Component B/multi-olefinic monomer from 0.05/1 up to 5/1, by decreasing the mole ratio to increase the ratio of A/(B+C), and increasing the mole ratio to decrease the ratio of A/(B+C).

    摘要翻译： 一种制备使用多种可活化预聚物的微凝胶的方法。 在该方法中，交联组分A和可溶组分B和C的聚合物组合物在催化剂和引发剂存在下由单烯烃和多烯属单体形成。 该方法包括：I）在不存在多烯属单体的情况下将单烯烃单体，催化剂和引发剂引入反应器，并产生可活化的预聚物组分B; II）使I）的产物与多烯属单体接触， 产生组分A和C，任选地在另外的引发剂的存在下; 也可任选在另外的单烯属单体和引发剂的存在下进行。 组分A /（B + C）的比例可以通过将组分B /多烯烃单体的摩尔比从0.05 / 1增加到5/1来控制，通过降低摩尔比以增加A / （B + C），并且增加摩尔比以降低A /（B + C）的比例。

    Ink jet ink, ink set and method of printing
    8.
    发明申请
    Ink jet ink, ink set and method of printing 审中-公开
    喷墨墨水，墨水组合和印刷方法

    公开(公告)号：US20070259989A1

    公开(公告)日：2007-11-08

    申请号：US11799221

    申请日：2007-05-01

    申请人： Charles T. Berge ,  Xiaoqing Li

    发明人： Charles T. Berge ,  Xiaoqing Li

    IPC分类号： C09D11/00

    CPC分类号： C09D11/38 ,  C09D11/40

    摘要： This invention pertains to an inkjet ink comprising a β-hydroxyalkyl amidyl-containing compound, a binder and, optionally, acidic or anhydric ink components as part of the ink or as part of an additional ink in an ink set, and a method of printing with the ink and/or the ink set.

    摘要翻译： 本发明涉及包含含有β-羟基烷基酰氨基化合物，粘合剂和任选的作为油墨的一部分的酸性或非金属油墨组分或作为油墨组中的附加油墨的一部分的喷墨油墨，以及印刷方法 与墨水和/或墨水组合。

    Phosphonic acid reaction products and use in coating compositions
    9.
    发明授权
    Phosphonic acid reaction products and use in coating compositions 失效
    膦酸反应产物和用于涂料组合物

    公开(公告)号：US06624227B1

    公开(公告)日：2003-09-23

    申请号：US09462966

    申请日：2000-07-12

    申请人： Paul Peter Bruylants ,  Josef Huybrechts ,  Kenneth S. Kirshenbaum ,  Charles T. Berge

    发明人： Paul Peter Bruylants ,  Josef Huybrechts ,  Kenneth S. Kirshenbaum ,  Charles T. Berge

    IPC分类号： C08K308

    CPC分类号： C09C1/644 ,  C01P2004/20 ,  C08F8/40 ,  C09C1/622 ,  C09D5/38

    摘要： The invention provides an aqueous coating composition comprising nonionically and/or anionically stabilized film-forming polymers and metallic pigments and a compound which is the reaction product of a phosphonic acid derivative, a hydroxy-functional addition polymers and, optionally a compound having a hydroxy group, in which the phosphonic acid derivative is selected from one or both of wherein R and R′ are selected from the group consisting of an aliphatic and an aromatic substituent having 1 to 25 carbon atoms optionally including heteroatoms of at least one of oxygen, phosphorus and silicon.

    摘要翻译： 本发明提供一种水性涂料组合物，其包含非离子和/或阴离子稳定的成膜聚合物和金属颜料，以及作为膦酸衍生物，羟基官能加成聚合物和任选具有羟基的化合物的反应产物的化合物 其中膦酸衍生物选自其中一个或两个，其中R和R'选自具有1至25个碳原子的脂族和芳族取代基，任选地包括氧，磷和硅中的至少一个的杂原子 。

    Process of polymerization in an aqueous system
    10.
    发明授权
    Process of polymerization in an aqueous system 失效
    在水性体系中的聚合方法

    公开(公告)号：US5264530A

    公开(公告)日：1993-11-23

    申请号：US876764

    申请日：1992-05-01

    申请人： Michael J. Darmon ,  Charles T. Berge ,  Joseph A. Antonelli

    发明人： Michael J. Darmon ,  Charles T. Berge ,  Joseph A. Antonelli

    IPC分类号： C08F2/16 ,  C08F2/18 ,  C08F2/38 ,  C08F2/42 ,  C08F20/18 ,  C08F220/10 ,  C09D157/00

    CPC分类号： C08F2/38

    摘要： A improved method of free radical polymerization in an aqueous system, such as an emulsion or suspension process. The polymerization is conducted in the presence of a relatively low molecular weight macromonomer such as can be made with a metal chelate chain transfer catalyst. This method is useful for reducing the molecular weight of a variety of polymers and copolymers, including acrylic and olefinic polymers.

    摘要翻译： 在水性体系中的改进的自由基聚合方法，例如乳液或悬浮方法。 聚合在相对低分子量的大分子单体的存在下进行，例如可以用金属螯合链转移催化剂制备。 该方法可用于降低各种聚合物和共聚物（包括丙烯酸和烯烃聚合物）的分子量。