Distillation of titanium tetrachloride in solution with selected amines
    1.
    发明授权
    Distillation of titanium tetrachloride in solution with selected amines 失效
    在选择的胺溶液中蒸馏四氯化钛

    公开(公告)号:US3963585A

    公开(公告)日:1976-06-15

    申请号:US465954

    申请日:1974-05-01

    IPC分类号: C01G23/02 B01D3/34

    CPC分类号: C01G23/024

    摘要: In the purification of impure titanium tetrachloride comprising adding an agent to said titanium tetrachloride and thereafter distilling off purified titanium tetrachloride while leaving the impurity in the distillation residue, the improvement which comprises employing as said agent at least one amine of the formula ##EQU1## in which R.sub.1 and R.sub.2 each independently is hydrogen, alkyl or alkenyl of up to 6 carbon atoms, cycloalkyl of 5 to 7 carbon atoms, or aryl, andR.sub.3 is cycloalkyl of 5 to 7 ring carbon atoms, or aryl, orR.sub.2 together with R.sub.3 is butylene, pentylene or hexylene, in which eventR.sub.1 is hydrogen, alkyl of up to 6 carbon atoms or aryl.The preferred agents are aniline, cyclohexylamine, N,N-dimethyl-aniline, diphenylamine, 2,3-dimethyl-aniline and 2,6-dimethyl-aniline. The process serves to remove vanadium impurities.

    摘要翻译: 在不纯的四氯化钛的纯化中,包括在所述四氯化钛中加入试剂,然后蒸馏出纯化的四氯化钛,同时留下蒸馏残余物中的杂质,其改进包括使用至少一种式R 2 R 1 -N 其中R 1和R 2各自独立地为氢,至多6个碳原子的烷基或烯基,5至7个碳原子的环烷基或芳基,R 3为5至7个环碳原子的环烷基,或芳基或R 2 与R 3一起是亚丁基,亚戊基或亚己基,其中R1是氢,高达6个碳原子的烷基或芳基。

    Production of zinc and alkaline earth metal titanates
    3.
    发明授权
    Production of zinc and alkaline earth metal titanates 失效
    生产锌和碱土金属钛酸盐

    公开(公告)号:US4173485A

    公开(公告)日:1979-11-06

    申请号:US873995

    申请日:1978-01-31

    摘要: Titanates of zinc and/or alkaline earth metals are produced by simultaneously adding to a suspension of finely divided TiO.sub.2, maintained at a substantially constant pH above about 8, a solution of a salt of zinc and/or alkaline earth metal and alkali to form a hydroxide precipitate. Filtration produces a filter cake mixture of TiO.sub.2 and hydroxide and calcination at above 500.degree. C. produces the desired titanate of narrow particle size distribution and desirable optical properties. Non-simultaneous addition results in a non-filterable material. Zinc, magnesium and/or calcium are preferred and doping elements such as aluminum, phosphorus, boron and/or silicon may also be present.

    摘要翻译: 锌和/或碱土金属的钛酸盐通过同时加入到细分散的TiO 2的悬浮液中,将其保持在高于约8的基本上恒定的pH,锌和/或碱土金属和碱的盐溶液形成 氢氧化物沉淀。 过滤产生TiO 2和氢氧化物的滤饼混合物并在500℃以上煅烧,产生窄粒度分布的所需钛酸盐和所需的光学性质。 非同时加入导致不可过滤的材料。 优选锌,镁和/或钙,也可以存在诸如铝,磷,硼和/或硅的掺杂元素。

    Method and preparations for stabilizing biological materials by drying methods without freezing
    7.
    发明授权
    Method and preparations for stabilizing biological materials by drying methods without freezing 失效
    通过干燥方法稳定生物材料而不冻结的方法和制剂

    公开(公告)号:US07172999B2

    公开(公告)日:2007-02-06

    申请号:US09051918

    申请日:1996-10-24

    IPC分类号: A61K38/18 C07K14/505

    摘要: The present invention concerns processes for the production of dry, partially amorphous products containing biologically active and in particular therapeutically active material which are macroscopically homogeneous substance mixtures, the substance mixtures being selected from at least one substance of each of the groups (i) carbohydrate or zwitterion with a polar residue and derivatives thereof, and (ii) zwitterion with an apolar residue and derivatives thereof, wherein a solution is prepared of the biologically or therapeutically active material and of substances (i) and (ii) and the solution is dried at a product temperature above the freezing point of the solution. In addition the invention concerns new substance mixtures which are obtained by the said process as well as the use thereof in diagnostic or therapeutic methods.

    摘要翻译: 本发明涉及生产含有生物活性的,特别是宏观上均匀的物质混合物的治疗活性物质的干燥,部分无定形产物的方法,所述物质混合物选自每个组的至少一种物质(i)碳水化合物或 具有极性残基及其衍生物的两性离子,和(ii)与非极性残基及其衍生物的两性离子,其中制备生物或治疗活性物质和物质(i)和(ii)的溶液,并将溶液在 产品温度高于溶液的冰点。 此外,本发明涉及通过所述方法获得的新物质混合物以及其在诊断或治疗方法中的用途。

    Thermal fuse and method for its activation
    9.
    发明授权
    Thermal fuse and method for its activation 失效
    热熔丝及其激活方法

    公开(公告)号:US5612662A

    公开(公告)日:1997-03-18

    申请号:US384821

    申请日:1995-02-07

    摘要: A thermal fuse includes a leaf spring formed of a narrow sheet metal strip. The leaf spring has ends and at least two contact points at the ends. At least one of the contact points is a soldering point for connection with corresponding circuit contacts of a circuit substrate. The leaf spring has at least one spring arm interconnecting the contact points. The spring arm has a roof-shaped deformation in the vicinity of one contact point. The spring arm has a flat and elongated spring segment with a transition adjoining the deformation and a transition extending to the other contact point. The spring segment is bending resistant in the vicinities of the transitions, for transforming a compressive deformation applied to the roof-shaped deformation into a lateral movement and into an arching of the spring segment, with both ends of the leaf spring attached to the circuit substrate without pretensioning. A method for activation of the thermal fuse includes placing the contact points of the leaf springs free of tension on the circuit contacts, soldering the contact points to the circuit contacts, and compressively deforming the roof-shaped deformation after the soldering for creating an arching of the spring segment and a desired pretensioning.

    摘要翻译: 热熔丝包括由窄金属片条形成的板簧。 板簧在端部具有端部和至少两个接触点。 接触点中的至少一个是用于与电路基板的相应电路触点连接的焊接点。 板簧具有互连接触点的至少一个弹簧臂。 弹簧臂在一个接触点附近具有屋顶形变形。 弹簧臂具有平坦且细长的弹簧段,其具有与变形相邻的过渡以及延伸到另一个接触点的过渡。 弹簧段在过渡附近是抗弯曲的,用于将应用于屋顶形变形的压缩变形转变为横向运动并进入弹簧段的拱形,其中板簧的两端附接到电路基板 没有预张力。 用于激活热熔丝的方法包括将板簧的接触点放置在电路触点上,将接触点焊接到电路触点上,并且在焊接之后对屋顶形变形进行压缩变形,以产生拱形 弹簧段和所需的预张紧。

    Method for the production of a radiographic screen
    10.
    发明授权
    Method for the production of a radiographic screen 失效
    用于生产放射线照相屏幕的方法

    公开(公告)号:US5296117A

    公开(公告)日:1994-03-22

    申请号:US983708

    申请日:1992-12-01

    摘要: A method for the production of a radiographic screen comprising the following steps:1) dispersing phosphor particles in an organic liquid in the presence of a charge controlling agent that charges said phosphor particles with a positive or negative net charge,2) arranging said dispersion between a pair of electrodes, wherein one of said electrodes is or carries a conductive support of said radiographic screen,3) applying and maintaining between said electrodes a sufficiently high direct current voltage to deposit charged phosphor particles onto said conductive support, and4) separating said support carrying electrophoretically deposited phosphor particles from said organic liquid,wherein the dispersing of said phosphor particles proceeds by means of an organic surface active compound acting as dispersing agent for said phosphor particles, and said phosphor particles are electrostatically charged through adsorption thereon of ionic components of said organic surface active compound and/or through adsorption of cations or anions stemming from an ionic inorganic compound incorporated in said liquid.

    摘要翻译: 一种用于生产射线照相屏幕的方法,包括以下步骤:1)在电荷控制剂的存在下,将荧光体颗粒分散在有机液体中,所述电荷控制剂用正或负净电荷对所述荧光体颗粒进行充电,2)将所述分散体布置在 一对电极,其中所述电极之一是或承载所述放射线照相屏幕的导电支撑件,3)在所述电极之间施加和保持足够高的直流电压以将带电荧光粉颗粒沉积到所述导电支撑件上,以及4)将所述 从所述有机液体中携带电泳沉积的荧光体颗粒的载体,其中所述荧光体颗粒的分散通过作为所述荧光体颗粒的分散剂的有机表面活性化合物进行,并且所述荧光体颗粒通过其上的离子组分的吸附静电 所述有机表面活性化合物 和/或通过吸附由所述液体中引入的离子型无机化合物产生的阳离子或阴离子。