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    PHOSPHORUS-CONTAINING STABILIZERS FOR FLUOROOLEFINS
    4.
    发明申请
    PHOSPHORUS-CONTAINING STABILIZERS FOR FLUOROOLEFINS 有权
    含氟磷酸的含磷稳定剂

    公开(公告)号：US20100301259A1

    公开(公告)日：2010-12-02

    申请号：US12377474

    申请日：2007-08-31

    申请人： Thomas J. Leck ,  Nandini C. Mouli ,  Barbara Haviland Minor ,  Mario Joseph Nappa ,  Jon Lee Howell

    发明人： Thomas J. Leck ,  Nandini C. Mouli ,  Barbara Haviland Minor ,  Mario Joseph Nappa ,  Jon Lee Howell

    IPC分类号： C09K5/00

    CPC分类号： C09K5/045 ,  C09K2205/126

    摘要： The present disclosure relates to compositions comprising at least one fluoroolefin and an effective amount of a stabilizer comprising at least one phosphorus-containing compound selected from the group consisting of thiophosphates, butylated triphenylphosphorothionates, and organophosphates. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.

    摘要翻译： 本公开涉及包含至少一种氟代烯烃和有效量的稳定剂的组合物，其包含至少一种选自硫代磷酸酯，丁基化三苯基硫代硫酸酯和有机磷酸酯的含磷化合物。 稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。

    Synthesis of carbon-labeled perfluoroalkyl compounds
    7.
    发明授权
    Synthesis of carbon-labeled perfluoroalkyl compounds 有权
    碳标记的全氟烷基化合物的合成

    公开(公告)号：US07351870B2

    公开(公告)日：2008-04-01

    申请号：US10794556

    申请日：2004-03-05

    申请人： Alexander Borisovich Shtarov ,  Jon Lee Howell

    发明人： Alexander Borisovich Shtarov ,  Jon Lee Howell

    IPC分类号： C07C19/08

    CPC分类号： C07B59/001 ,  C07B2200/05 ,  C07C19/16 ,  C07C21/18 ,  C07C41/18 ,  C07C43/123 ,  C07C51/15 ,  C07C51/60 ,  C07C51/62 ,  C07C309/06 ,  C07C53/21 ,  C07C53/50 ,  C07C59/135

    摘要： Various 13C and 14C carbon labeled compounds Rf—bCF(U)y(T)zFormula 1A or Rf—bCF2bCF(U)y(T)zFormula 1B wherein Rf is a linear or branched perfluoroalkyl radical Z(CmF2m)—, m is 1, 3 to 20, or a mixture thereof; Z is F when m is 1, and Z is F, Cl, or H when m is 3 to 20 or a mixture thereof; b is 13 or 14; y is 1, and z is 0 or 1; and when y and z are each 1, U is F, and T is selected from the group consisting of monovalent radicals —X wherein X is I or Br, —CH2—CH2—X, —CH═CH2, —CH2—CH2—OH, —CH2—COOH, —CH2OH, —bCH2OH, —COOH, —bCOOH, —O—CF(CF3)—C(O)F, —O—CF(CF3)—X, —SO2Y wherein Y is H, F or Cl, and —SO3H; and when y is 1, and z is 0, U is selected from the group consisting of divalent radicals ═CH—COOH, ═CH—CH2—OH, and ═O, are disclosed, and a process for their preparation which selectively introduces 13C and 14C carbon labels into a fluoroalkyl chain.

    摘要翻译： 各种 13 C和14 C碳标记的化合物<？in-line-formula description =“In-line Formulas”end =“lead”？> R f 式（1A）或<β在线公式描述=“In” -line公式“end =”tail“？> <？in-line-formula description =”In-line Formulas“end =”lead“？> R CF（U）y（T）>>>>> formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas>>>>>>>>>>>>>>>>>>> formulas formulas formulas formulas formulas description =“In-line Formulas”end =“tail”？>其中R f是直链或支链的全氟烷基Z（C m 2 F 2 m） SUB-） - ，m为1,3至20，或其混合物; 当m为1时，Z为F，当m为3至20时Z为F，Cl或H或其混合物; b为13或14; y为1，z为0或1; 当y和z各自为1时，U为F，T选自单价基团-X，其中X为I或Br，-CH 2 -CH 2， -X，-CH-CH 2，-CH 2 -CH 2 -OH，-CH 2 CH 2， SO 2 -COOH，-CH 2 OH， - CH 2 CH 2 OH，-COOH， - CO 2 COOH ，-O-CF（CF 3） - C（O）F，-O-CF（CF 3） - X，-SO 2

    Flourinated compositions comprising phosphorus
    8.
    发明授权
    Flourinated compositions comprising phosphorus 有权
    包含磷的含氟组合物

    公开(公告)号：US06828284B2

    公开(公告)日：2004-12-07

    申请号：US09923838

    申请日：2001-08-06

    申请人： Jon Lee Howell ,  Erik William Perez

    发明人： Jon Lee Howell ,  Erik William Perez

    IPC分类号： C10M13100

    CPC分类号： C10M137/02 ,  C10M105/74 ,  C10M137/12 ,  C10M2213/06 ,  C10M2213/0626 ,  C10M2223/02 ,  C10M2223/023 ,  C10M2223/08 ,  C10M2223/083 ,  C10N2240/204 ,  C10N2250/10 ,  Y10T428/31544

    摘要： A composition that is or comprises a phosphorus-, perfluoropolyether-, and perfluoroalkyl-containing compound is provided. The compound comprises either (i) mono- or polyalkylene oxide linking groups between the phosphorus and the fluorocarbon group, or (ii) no linking group between the phosphorus and fluorocarbon group, or (iii) individual mixtures of (i) and (ii); and the fluorocarbon group can be the perfluoropolyether or perfluoroalkyl group. The compound can also be a partially esterified phosphate, a partially esterified phosphonate, a salt of a partially esterified phosphate, a salt of a partially esterified phosphonate, or mixtures of two or more thereof.

    摘要翻译： 提供了包含磷，全氟聚醚和全氟烷基的化合物的组合物。 该化合物包括（i）磷和氟碳基团之间的单 - 或聚环氧烷连接基团，或（ii）磷和碳氟化合物基团之间没有连接基团，或（iii）（i）和（ii） ; 氟碳基可以是全氟聚醚或全氟烷基。 该化合物还可以是部分酯化的磷酸酯，部分酯化的膦酸酯，部分酯化的磷酸酯的盐，部分酯化的膦酸盐的盐，或其两种或多种的混合物。

    Phosphorus-containing stabilizers for fluoroolefins
    10.
    发明授权
    Phosphorus-containing stabilizers for fluoroolefins 有权
    用于氟烯烃的含磷稳定剂

    公开(公告)号：US08529786B2

    公开(公告)日：2013-09-10

    申请号：US12377474

    申请日：2007-08-31

    申请人： Thomas J. Leck ,  Nandini C. Mouli ,  Barbara Haviland Minor ,  Mario Joseph Nappa ,  Jon Lee Howell

    发明人： Thomas J. Leck ,  Nandini C. Mouli ,  Barbara Haviland Minor ,  Mario Joseph Nappa ,  Jon Lee Howell

    IPC分类号： C09K5/04

    CPC分类号： C09K5/045 ,  C09K2205/126

    摘要： The present disclosure relates to compositions comprising at least one fluoroolefin and an effective amount of a stabilizer comprising at least one phosphorus-containing compound selected from the group consisting of thiophosphates, butylated triphenylphosphorothionates, and organophosphates. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.

    摘要翻译： 本公开涉及包含至少一种氟代烯烃和有效量的稳定剂的组合物，其包含至少一种选自硫代磷酸酯，丁基化三苯基硫代硫酸酯和有机磷酸酯的含磷化合物。 稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。