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    Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins
    6.
    发明授权
    Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins 有权
    含有菱沸石的分子筛的合成及其在含氧化合物转化为烯烃的用途

    公开(公告)号：US07754187B2

    公开(公告)日：2010-07-13

    申请号：US11820908

    申请日：2007-06-21

    申请人： Guang Cao ,  Machteld M. Mertens ,  Anil S. Guram ,  Hailian Li ,  Jeffrey C. Yoder

    发明人： Guang Cao ,  Machteld M. Mertens ,  Anil S. Guram ,  Hailian Li ,  Jeffrey C. Yoder

    IPC分类号： C01B37/02 ,  C01B39/04

    CPC分类号： C01B39/48 ,  B01J29/70 ,  B01J29/80 ,  C01B39/023 ,  C07C1/20 ,  Y02P30/42 ,  C07C11/02

    摘要： A method is disclosed of synthesizing a crystalline material comprising a CHA framework type molecular sieve and having a composition involving the molar relationship: (n)X2O3:YO2, wherein X is a trivalent element; Y is a tetravalent element; and n is from 0 to less than 0.01. The method comprises preparing a reaction mixture capable of forming said material, said mixture comprising a source of water, a source of an oxide of a tetravalent element Y and optionally a source of an oxide of a trivalent element X, wherein the reaction mixture is substantially free of fluoride ions added as HF; maintaining the reaction mixture under conditions sufficient to form crystals of the crystalline material; and than recovering the crystalline material. The reaction mixture comprises either a specific directing agent for directing the formation of a CHA framework type molecular sieve and/or a H2O:YO2 molar ratio of greater than 20. In one embodiment, the resultant crystalline material is free of stacking faults and/or any intergrown phase with an AEI framework type molecular sieve.

    摘要翻译： 公开了一种合成包含CHA骨架型分子筛并具有摩尔关系的组成的结晶材料的方法：（n）X 2 O 3：YO 2，其中X是三价元素; Y是四价元素; 并且n为0至小于0.01。 该方法包括制备能够形成所述材料的反应混合物，所述混合物包含水源，四价元素Y的氧化物源和任选的三价元素X的氧化物源，其中反应混合物基本上 不含氟离子作为HF添加; 在足以形成结晶材料晶体的条件下保持反应混合物; 而不是回收结晶材料。 反应混合物包括用于引导形成CHA骨架型分子筛和/或H 2 O:YO 2摩尔比大于20的特定导向剂。在一个实施方案中，所得结晶材料不含堆垛层错和/或 任何与AEI框架型分子筛的共生相。

    Synthesis Of Aluminophosphate And Metalloaluminophosphate Molecular Sieves
    8.
    发明申请
    Synthesis Of Aluminophosphate And Metalloaluminophosphate Molecular Sieves 有权
    磷酸铝和金属铝磷酸盐分子筛的合成

    公开(公告)号：US20090247802A1

    公开(公告)日：2009-10-01

    申请号：US12059178

    申请日：2008-03-31

    申请人： Guang Cao ,  Mobae Afeworki ,  Matu J. Shah ,  Machteld Maria Mertens

    发明人： Guang Cao ,  Mobae Afeworki ,  Matu J. Shah ,  Machteld Maria Mertens

    IPC分类号： C01B25/12 ,  C07C1/02

    CPC分类号： C01B37/08 ,  B01J29/83 ,  B01J29/85 ,  C01B37/04 ,  C01B39/54 ,  C07C1/20 ,  Y02P30/20 ,  Y02P30/42 ,  Y10S423/30 ,  C07C11/02

    摘要： In a method of synthesizing an aluminophosphate or metalloaluminophosphate molecular sieve, a synthesis mixture is provided comprising water, a source of aluminum, a source of phosphorus, optionally a source of a metal other than aluminum, a tertiary amine, and an alkylating agent capable of reacting with said tertiary amine to form a quaternary ammonium compound capable of directing the synthesis of said molecular sieve. The synthesis mixture is maintained under conditions sufficient to cause the alkylating agent to react with the tertiary amine to produce the quaternary ammonium compound and to induce crystallization of the molecular sieve.

    摘要翻译： 在合成磷酸铝或金属铝磷酸盐分子筛的方法中，提供了合成混合物，其包含水，铝源，磷源，任选的除铝之外的金属源，叔胺和烷基化剂，其能够 与所述叔胺反应形成能够引导所述分子筛合成的季铵化合物。 将合成混合物保持在足以使烷基化剂与叔胺反应以产生季铵化合物并诱导分子筛结晶的条件下。

    Synthesis of molecular sieves having the CHA framework type
    9.
    发明授权
    Synthesis of molecular sieves having the CHA framework type 有权
    具有CHA骨架类型的分子筛的合成

    公开(公告)号：US06793901B2

    公开(公告)日：2004-09-21

    申请号：US10171257

    申请日：2002-06-12

    申请人： Guang Cao ,  Matu J. Shah ,  Karl G. Strohmaier ,  Richard B. Hall

    发明人： Guang Cao ,  Matu J. Shah ,  Karl G. Strohmaier ,  Richard B. Hall

    IPC分类号： C01B3706

    CPC分类号： B01J29/85 ,  B01J29/83 ,  C10G3/49 ,  C10G3/62 ,  C10G2400/20 ,  Y02P30/20 ,  Y10S423/30

    摘要： The invention is directed to a method for preparing microporous aluminophosphate or silicoaluminophosphate molecular sieves having the CHA framework type, the process comprising the steps of a) forming a reaction mixture comprising a source of aluminum, a source of phosphorus, optionally a source of silicon, at least one source of fluoride ions and at least one template containing one or more N,N-dimethylamino moieties, b) inducing crystallization of aluminophosphate and/or silicoaluminophosphate molecular sieve from the reaction mixture; c) recovering aluminophosphate and/or silicoaluminophosphate molecular sieve from the reaction mixture. The invention also relates to the molecular sieves obtained by this method and to molecular sieve catalyst compositions containing these molecular sieves.

    摘要翻译： 本发明涉及一种制备具有CHA骨架类型的微孔磷酸铝或硅铝磷酸盐分子筛的方法，该方法包括以下步骤：a）形成包含铝源，磷源，任选的硅源的反应混合物， 至少一个氟离子源和至少一个含有一个或多个N，N-二甲基氨基部分的模板，b）从反应混合物中诱导磷酸铝和/或硅铝磷酸盐分子筛的结晶; c）从反应混合物中回收磷酸铝和/或硅铝磷酸盐分子筛。 本发明还涉及通过该方法获得的分子筛和含有这些分子筛的分子筛催化剂组合物。