摘要:
Precipitated silica with the following physical-chemical characteristics: ______________________________________ BET surface: DIN 66131 100-130 m.sup.2 /g DBP absorption DIN 53601 .gtoreq.275 g/100 g (anhydrous) ASTM D 2414 Loss on drying DIN ISO 787/II (2 h/105.degree. C.) ASTM D 280 3.5-5.5 wt. % JIS K 5101/21 Oversize with ALPINE air-jet sieve: >63 .mu.m .ltoreq.10.0 wt. % >150 .mu.m .ltoreq.0.1 wt. % >250 .mu.m .ltoreq.0.01 wt. % Chloride content: .ltoreq.100 ppm ______________________________________ is prepared by introducing water into a precipitation vessel, adding water glass until an alkali value of 5-15 is reached, then adding further water glass and sulfuric acid simultaneously, interrupting the precipitated silica suspension with sulfuric acid to a pH-value of 8.5, with stirring, then continuing acidification with concentrated sulfuric acid to a pH-value of 4, then separating and washing the precipitated silica which has a solids content in the suspension of approx. 88 g/l, liquefying the filter cake obtained, drying it with a spray drier and grinding it. The precipitated silica may be used for the production of battery separators.
摘要翻译:具有以下物理化学特性的沉淀二氧化硅: - BET表面:DIN 66131 100-130 m2 / g - DBP吸收DIN 53601> / = 275 g / 100 g - (无水)ASTM D 2414 - 干燥失重DIN ISO 787 / II - (2h / 105℃)ASTM D 280 3.5-5.5wt。 % - JIS K 5101/21 - 用 - ALPINE喷气筛过大 - - > 63微米10.0重量% % - >150μm = 0.1wt。 % - >250μm<0.01wt。 % - 氯化物含量: = 100ppm - 通过将水引入沉淀容器中,加入水玻璃直到达到碱值5-15,然后同时加入另外的水玻璃和硫酸,中断沉淀二氧化硅悬浮液 在搅拌下用硫酸至pH值8.5,然后用浓硫酸继续酸化至pH值为4,然后分离和洗涤沉淀二氧化硅,其悬浮液中固体含量约为 88g / l,液化所得滤饼,用喷雾干燥器干燥并研磨。 沉淀二氧化硅可用于生产电池隔板。
摘要:
A process for preparing microporous separating elements for batteries by intensive mixing of a high molecular weight polyethylene with a precipitated silica having specific chemical and physical characteristics, a process liquid and a stabilizer to form a powder mixture, which is extruded to form a film, from which the process liquid is removed, thereby leaving the desired microporous separating elements which are recovered.
摘要:
The present invention relates to a method of purifying strong acids or strongly acidic media to remove di- and higher valent metal ions, which can be used within the context of the production of high-purity silica. The invention further relates to the use of special ion exchangers for carrying out the method according to the invention and the resultant high-purity silicas.
摘要:
A zeolite catalyst and a method for reduction of nitrogen oxides present in waste gas streams is described. The method includes mixing the waste gas containing nitrogen oxides with ammonia. At an elevated temperature, this mixture is passed over a zeolite catalyst. Preferably, the zeolite catalyst is in a monolithic or honeycomb form. The zeolite catalyst includes one or more of the following subgroup metals: copper, iron, molybdeum and cerium. The zeolite catalysts made in accordance with this invention show better conversion of nitrogen oxides and longer life than known catalysts.
摘要:
The object of the invention is a more energy-efficient system for utilizing waste heat and residual gases from the engineered generation of carbon compounds, such as carbon black, graphite or from sugar pyrolysis, using a coupling of energy-heat or a thermal heat-generating plant for generating electrical energy, in particular for operating melt furnaces, and/or for utilizing the waste heat in endothermal processes. The invention also relates to the use of waste heat.
摘要:
The precipitated silica has the following physico-chemical parameters: BET surface area (DIN 66131) in m2/g 400-600 DBP index (DIN 53601) in g/100 g 300-360 Compacted density (DIN 53194) in g/l 70-140 Grindometer value (ISO 1524) in &mgr;m 15-50 Size distribution index I
摘要:
Precipitated silicas, characterized in that they have a CTAB surface area (in accordance with ASTM D 3765-92) of 200 to 400 m.sup.2 /g, a DBP index (in accordance with ASTM D 2414) between 230 and 380 ml/100 g as powder and 180-250 g/100 g as granulate, a silanol group density (V.sub.2 -NaOH consumption) of 20 to 30 ml and the following macropore size distribution which is typical of the surface area range involved, determined by means of Hg porosimetry (DIN 66 133) for specific pore size intervals (incremental mode of application): ______________________________________ CTAB surface CTAB surface CTAB surface area range: area range: area range: 200-250 250-300 300-400 Pore size m.sup.2 /g m.sup.2 /g m.sup.2 /g interval �nm! Hg consumption in ml/g of silica ______________________________________ 10-20 0.27-0.49 0.35-0.50 0.32-0.42 20-30 0.22-0.32 0.15-0.30 0.17-0.22 30-40 0.15-0.21 0.12-0.17 0.12-0.15 40-50 0.11-0.16 0.09-0.12 0.08-0.11 50-60 0.08-0.12 0.06-0.10 0.06-0.09 ______________________________________
摘要:
The invention relates to a complete method for producing pure silicon that is suitable for use as solar-grade silicon, comprising the reduction of a purified silicon oxide using one or more pure carbon sources, the purified silicon oxide, which was purified as silicon oxide dissolved in an aqueous phase, having a content of other polyvalent metals or metal oxides, in relation to the silicon oxide, of less than or equal to 300 ppm, preferably less than 100 ppm, especially preferably less than 50 ppm and according to the invention less than 10 ppm of the other metals and being obtained advantageously by gel formation in alkaline conditions. The invention also relates to a formulation containing an activator and to the use of purified silicon oxide together with an activator for producing silicon.
摘要:
Precipitated silica having the following parameters: BET surface area 80-180 m2/g CTAB surface area 80-139 m2/g BET/CTAB ratio 1.0-1.6 Sears No. (consumption of 5-25 ml 0.1 N NaOH) DBP No. 200-300 ml/100 g Al2O3 content
摘要:
Precipitated silica, having the following physico-chemical parameters: BET surface area 120-300 m2/g CTAB surface area 100-300 m2/g BET/CTAB ratio 0.8-1.3 Sears index (consumption of 6-25 ml 0.1 N NaOH) DBP index 150-300 g/100 g wk coefficient