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    Antibiotics, a process for their preparation and their use as plant protection agents
    3.
    发明授权
    Antibiotics, a process for their preparation and their use as plant protection agents 失效
    抗生素，它们的制备过程及其作为植物保护剂的用途

    公开(公告)号：US4585761A

    公开(公告)日：1986-04-29

    申请号：US265523

    申请日：1981-05-20

    申请人： Hans Zahner ,  Hartwig Holst ,  Gerhard Zoebelein ,  Adelinde Keckeisen

    发明人： Hans Zahner ,  Hartwig Holst ,  Gerhard Zoebelein ,  Adelinde Keckeisen

    IPC分类号： A01N63/02 ,  A01N43/50 ,  A01N43/54 ,  C07H19/052 ,  C07H19/06 ,  C12P19/28 ,  C12P19/38 ,  C12P19/40 ,  C12R1/465 ,  A01N31/00 ,  C07H17/00

    CPC分类号： C07H19/06 ,  A01N43/50 ,  A01N43/54 ,  C07H19/052 ,  C12P19/28 ,  C12P19/385 ,  C12R1/465

    摘要： A method of combating arthropods, comprising applying to the arthropods, or to a habitat infested therewith an arthropodicidally effective amount of an antibiotic which (a) is colorless, very readily soluble in water and in pyridine but insoluble in other customary organic solvents, gives a positive reaction with ninhydrin, sodium metaperiodate/benzidine and potassium permanganate and gives a yellow coloration with iron (III) chloride, (b) has the UV and IR spectra substantially as shown in FIGS. 1 and 2, (c) on chemical degradation yields uracil, an amino-hexuronic acid and an amino-acid containing a pyridine ring, (d) on paper electrophoresis proves to be an amphoteric substance and has an isoelectric point at about pH 6 and (e) consists of the elements carbon, hydrogen, oxygen and nitrogen, or one or more active components of the antibiotic mixture, the active agent being applied alone or in admixture with a diluent or carrier. The antibiotic is known as Nikkomycin which is apparently a mixture of components of the formula ##STR1## in which R.sub.1 is ##STR2## and R.sub.2 is hydrogen, ##STR3##

    摘要翻译： 一种防治节肢动物的方法，包括向节肢动物或其感染的栖息地施用节肢动物有效量的抗生素，该抗生素（a）为无色，非常易于溶于水和吡啶，但不溶于其它常规的有机溶剂，得到 与茚三酮，偏高碘酸钠/联苯胺和高锰酸钾发生阳性反应，并与氯化铁（III）发生黄色着色，（b）基本上具有如图1和2所示的UV和IR光谱。 1和2，（c）化学降解产生尿嘧啶，氨基 - 己糖醛酸和含有吡啶环的氨基酸，（d）在纸电泳上证明是两性物质，并具有约pH 6的等电点， （e）由碳，氢，氧和氮的元素或抗生素混合物的一种或多种活性组分组成，活性剂单独施用或与稀释剂或载体混合。 抗生素被称为尼科霉素，其显然是式（IMAGE）的组分的混合物，其中R1是，R2是氢， + TR

    Antibiotics, a process for their preparation and their use as plant protection agents
    4.
    发明授权
    Antibiotics, a process for their preparation and their use as plant protection agents 失效
    抗生素，它们的制备过程及其作为植物保护剂的用途

    公开(公告)号：US4287186A

    公开(公告)日：1981-09-01

    申请号：US106223

    申请日：1979-12-21

    申请人： Hans Zahner ,  Hartwig Holst ,  Gerhard Zoebelein ,  Adelinde Keckeisen

    发明人： Hans Zahner ,  Hartwig Holst ,  Gerhard Zoebelein ,  Adelinde Keckeisen

    IPC分类号： A01N63/02 ,  A01N43/50 ,  A01N43/54 ,  C07H19/052 ,  C07H19/06 ,  C12P19/28 ,  C12P19/38 ,  C12P19/40 ,  C12R1/465 ,  A61K31/71

    CPC分类号： C07H19/06 ,  A01N43/50 ,  A01N43/54 ,  C07H19/052 ,  C12P19/28 ,  C12P19/385 ,  C12R1/465

    摘要： A method of combating arthropods, comprising applying to the arthropods, or to a habitat infested therewith an arthropodicidally effective amount of an antibiotic which (a) is colorless, very readily soluble in water and in pyridine but insoluble in other customary organic solvents, gives a positive reaction with ninhydrin, sodium metaperiodate/benzidine and potassium permanganate and gives a yellow coloration with iron (III) chloride, (b) has the UV and IR spectra substantially as shown in FIGS. 1 and 2, (c) on chemical degradation yields uracil, an amino-hexuronic acid and an amino-acid containing a pyridine ring, (d) on paper electrophoresis proves to be an amphoteric substance and has an isolectric point at about pH 6 and (e) consists of the elements carbon, hydrogen, oxygen and nitrogen, or one or more active components of the antibiotic mixture, the active agent being applied alone or in admixture with a diluent or carrier. The antibiotic is known as Nikkomycin which is apparently a mixture of components of the formula ##STR1## in which R.sub.1 is ##STR2## and R.sub.2 is hydrogen, ##STR3##

    摘要翻译： 一种防治节肢动物的方法，包括向节肢动物或其感染的栖息地施用节肢动物有效量的抗生素，该抗生素（a）为无色，非常易于溶于水和吡啶，但不溶于其它常规的有机溶剂，得到 与茚三酮，偏高碘酸钠/联苯胺和高锰酸钾发生阳性反应，并与氯化铁（III）发生黄色着色，（b）基本上具有如图1和2所示的UV和IR光谱。 1和2，（c）化学降解产生尿嘧啶，氨基 - 己糖醛酸和含有吡啶环的氨基酸，（d）在纸电泳上证明是两性物质，并且具有约pH 6的等电点， （e）由碳，氢，氧和氮的元素或抗生素混合物的一种或多种活性组分组成，活性剂单独施用或与稀释剂或载体混合。 抗生素被称为尼古霉素，其显然是式（IMAGE）的组分的混合物，其中R1是，R2是氢，

    Antibiotic and use thereof
    7.
    发明授权
    Antibiotic and use thereof 失效
    抗生素及其用途

    公开(公告)号：US4277478A

    公开(公告)日：1981-07-07

    申请号：US41279

    申请日：1979-05-21

    申请人： Hans Zahner ,  Hannelore Drautz ,  Walter Keller

    发明人： Hans Zahner ,  Hannelore Drautz ,  Walter Keller

    IPC分类号： A61K31/435 ,  C07D491/14 ,  C07D491/16 ,  C12P1/06 ,  C12P17/18 ,  A61K31/535 ,  C07D491/153

    CPC分类号： C07D491/14 ,  C12P17/18

    摘要： The invention relates to the new antibiotic Lysolipin including two components X and I, and derivatives thereof. Lysolipin is formed when the strain Streptomyces violaceoniger (Waksman et Curtis) Waksman et Henrici Tu 96, which strain has been deposited under the reference NRRL 8097 at the Northern Regional Laboratory, U.S. Department of Agriculture, Peoria, Illinois, is cultured in a nutrient medium. The structural formulae of the 2 components are ##STR1## Lysolipin I and X and their derivatives have antibacterial activity and are effective against yeast - like fungi, such as Candida albicans. Their antibiotic action probably depends on an inhibition of the cell wall synthesis.

    摘要翻译： 本发明涉及包含两种组分X和I的新型抗生素赖溶脂蛋白及其衍生物。 当菌株Streptomyces violaceoniger（Waksman et Curtis）Waksman et HenriciTü96将菌株以参考文献NRRL 8097保藏在美国伊利诺伊州皮奥里亚州的美国农业部北部地区实验室时，形成溶纤剂，培养于营养培养基 。 2种成分的结构式为Lysolipin I，Lysolipin X Lysolipin I和X及其衍生物具有抗菌活性，对酵母菌真菌如白色念珠菌有效。 它们的抗生素作用可能取决于细胞壁合成的抑制。

    2-Pyridyl-2-thiazoline-4-carboxylic acid derivatives
    9.
    发明授权
    2-Pyridyl-2-thiazoline-4-carboxylic acid derivatives 失效
    2-吡啶基-2-噻唑啉-4-羧酸衍生物

    公开(公告)号：US4406905A

    公开(公告)日：1983-09-27

    申请号：US285909

    申请日：1981-07-23

    申请人： Hans Zahner ,  Hans-Ulrich Naegeli ,  Heinrich Peter

    发明人： Hans Zahner ,  Hans-Ulrich Naegeli ,  Heinrich Peter

    IPC分类号： C07D213/79 ,  C07D417/04 ,  C07F7/08 ,  C12P17/16 ,  A61K31/44 ,  C07D409/04

    CPC分类号： C07D213/79 ,  C07D417/04 ,  C07F7/0812 ,  C12P17/167 ,  C12R1/48

    摘要： The invention relates especially to 2-(3'-hydroxypyrid-2'-yl)-2-thiazoline-4-carboxylic acid derivatives of the formula (I) and salts and also certain metal complexes of these compounds, processes for their manufacture, pharmaceutical agents containing such compounds and the use of these compounds. ##STR1## In the formula, R.sup.1 represents free, etherified or esterified hydroxy, R.sup.2 represents hydrogen or an aliphatic, carbocyclic or carbocyclic-aliphatic radical having 1-12 carbon atoms, and R.sup.3 represents hydrogen or an unsubstituted aliphatic radical having 1-7 carbon atoms.The compounds of the formula (I) can be used, for example, for the abstraction of heavy metals from the organism of warm-blooded animals and/or they have an antibiotic action.

    摘要翻译： 本发明特别涉及式（I）的2-（3'-羟基吡啶-2'-基）-2-噻唑啉-4-羧酸衍生物及其盐以及这些化合物的某些金属配合物，其制备方法， 含有这些化合物的药剂和这些化合物的用途。 （I）式中，R1表示游离的醚化或酯化的羟基，R 2表示氢或具有1-12个碳原子的脂族，碳环或碳环脂族基，R3表示氢或未取代的具有1个 -7个碳原子。 式（I）的化合物可用于例如从温血动物的生物体中提取重金属和/或具有抗生素作用。

    Microbiological process for the preparation of (S,S)-N,N'-ethylenediaminedisuccinic acid
    10.
    发明授权
    Microbiological process for the preparation of (S,S)-N,N'-ethylenediaminedisuccinic acid 失效
    制备（S，S）-N，N'-乙二胺二琥珀酸的微生物过程

    公开(公告)号：US5874262A

    公开(公告)日：1999-02-23

    申请号：US952274

    申请日：1997-11-17

    申请人： Hans Zahner ,  Ingeborg Cebulla ,  Michael Harder

    发明人： Hans Zahner ,  Ingeborg Cebulla ,  Michael Harder

    IPC分类号： C09K3/00 ,  C11D3/33 ,  C12P13/00 ,  C12R1/01

    CPC分类号： C12P13/04 ,  Y10S435/822

    摘要： A microbiological process for the preparation of N,N'-ethylenediaminedisuccinic acid of formula (1), by (a) precultivation of a strain of the genus Amycolatopsis orientalis on a specified nutrient medium (1st preculture), (b) inoculation of a nutrient solution of the same composition as the base of the production fermenter by the 1st preculture (2nd preculture), (c) inoculation of the base nutrient solution in the production fermenter with the 2nd preculture and incubation in accordance with a specified timetable, (d) feeding of the production fermenter in the fed-batch process with a feeding solution under aerobic conditions at a pH of from 2 to 8 and at a temperature of from 15.degree. to 40.degree. C., wherein the base nutrient and feeding solutions are free of zinc-containing compounds, is described. The compound prepared by the process according to the invention is suitable as complexing agent with good biodegradability in detergents. ##STR1##

    摘要翻译： PCT No.PCT / EP96 / 01868 Sec。 371日期1998年1月23日 102（e）日期1998年1月23日PCT提交1996年5月4日PCT公布。 公开号WO96 / 36725 日期：1996年11月21日制备式（1）的N，N'-乙二胺二琥珀酸的微生物方法，通过（a）在特定的营养培养基（第一预培养物）上预先培养东方双歧杆菌属菌株 ）通过第一次预培养（第二次预培养）接种与生产发酵罐底部相同组成的营养液，（c）用第二次预培养接种生产发酵罐中的基础营养液并根据指定的温育 时间表，（d）在补充分批过程中的生产发酵罐在需氧条件下在pH为2至8和在15至40℃的温度下用进料溶液进料，其中所述基础营养物和 进料溶液中不含含锌化合物。 通过本发明方法制备的化合物适用于洗涤剂中具有良好生物降解性的络合剂。 （1）