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    Arc electrodes for synthesis of carbon nanostructures
    6.
    发明授权
    Arc electrodes for synthesis of carbon nanostructures 失效
    用于合成碳纳米结构的电弧电极

    公开(公告)号：US06794598B2

    公开(公告)日：2004-09-21

    申请号：US10433028

    申请日：2003-07-25

    申请人： Houjin Huang ,  Hisashi Kajiura ,  Mitsuaki Miyakoshi ,  Atsuo Yamada ,  Masashi Shiraishi

    发明人： Houjin Huang ,  Hisashi Kajiura ,  Mitsuaki Miyakoshi ,  Atsuo Yamada ,  Masashi Shiraishi

    IPC分类号： B23K1500

    CPC分类号： B82Y30/00 ,  B82Y10/00 ,  H01J37/32055 ,  H01J37/32532 ,  H01J37/32541 ,  H01J37/3255 ,  Y10S977/843 ,  Y10S977/844 ,  Y10S977/896

    摘要： An arc electrode structure, for producing carbon nanostructures, which includes a first electrode and two or more second electrodes disposed within a chamber is provided. The electrodes are connected to a voltage potential to produce an arc-plasma region. The first electrode has a sloped surface with a plurality of holes therein for holding catalyst. The first electrode's sloped surface, and the positioning of the plurality of second electrodes allows control of the direction and region of arc-plasma. Further, the first electrode has a central bore which may be either a blind bore, or a through bore. The blind bore collects unwanted deposits that slide off of the sloped surface of the first electrode. The throughbore either allows soot and carbon nanostructures to be removed from the chamber, or allows organic vapor to be introduced into the chamber. When the throughbore is used to introduce organic vapor into the chamber, the vapor is directed through the arc-plasma region so that carbon nanostructures are built up by a CVD process rather than being broken off of carbon electrodes.

    摘要翻译： 提供了一种用于制造碳纳米结构的电弧电极结构，其包括第一电极和设置在室内的两个或更多个第二电极。 电极连接到电压电位以产生电弧等离子体区域。 第一电极具有倾斜表面，其中具有多个孔用于保持催化剂。 第一电极的倾斜表面和多个第二电极的定位允许控制电弧等离子体的方向和区域。 此外，第一电极具有可以是盲孔或通孔的中心孔。 盲孔收集从第一电极的倾斜表面滑出的不需要的沉积物。 通孔可以允许煤烟和碳纳米结构从室中移出，或允许有机蒸汽被引入室中。 当通孔用于将有机蒸汽引入室中时，蒸汽被引导通过电弧等离子体区域，使得碳纳米结构由CVD工艺构成，而不是被碳电极断开。

    Carbon Nanotube and Manufacturing Method Thereof, and Carbon Nanotube Manufacturing Equipment
    7.
    发明申请
    Carbon Nanotube and Manufacturing Method Thereof, and Carbon Nanotube Manufacturing Equipment 审中-公开
    碳纳米管及其制造方法和碳纳米管制造设备

    公开(公告)号：US20080124502A1

    公开(公告)日：2008-05-29

    申请号：US10564565

    申请日：2004-07-15

    申请人： Houjin Huang ,  Hisashi Kajiura ,  Masafumi Ata

    发明人： Houjin Huang ,  Hisashi Kajiura ,  Masafumi Ata

    IPC分类号： D01F9/12 ,  C01B31/00 ,  C01B31/02 ,  B01J8/00

    CPC分类号： D01F9/127 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  C01B32/164 ,  C01B2202/02 ,  C01B2202/04 ,  C01B2202/34 ,  Y10T428/13

    摘要： A manufacturing method of carbon nanotubes capable of mass-producing DWCNT with high throughput and a low defect incidence ratio is provided. In a vacuum chamber (1), a first electrode (2) having a hollow (2a) and a rod-like second electrode (3) are included. Inert gas such as helium gas, nitrogen gas, and argon gas is introduced into the vacuum chamber (1), the atmosphere not containing hydrogen gas and oxygen gas is created, and in this state, arc discharge is generated between the first electrode (2) and the second electrode (3). The heat generated by arc discharge is moderately stored on the surface of the inner side surrounded by the first electrode (2), and temperatures on the surface of the first electrode (2) are maintained at the temperatures suitable for producing the DWCNT (8). Thereby, the thready DWCNT (8) can be continuously produced without pause starting with a catalyst (6).

    摘要翻译： 提供能够大量生产高产量和低缺陷发生率的DWCNT的碳纳米管的制造方法。 在真空室（1）中，包括具有中空部（2a）和棒状第二电极（3）的第一电极（2）。 惰性气体如氦气，氮气和氩气被引入真空室（1），不产生氢气和氧气的气氛，在这种状态下，在第一电极（2） ）和第二电极（3）。 由电弧放电产生的热适度地储存在由第一电极（2）包围的内侧的表面上，并且第一电极（2）的表面上的温度保持在适于生产DWCNT（8）的温度下， 。 因此，可以不间断地从催化剂（6）开始直接制造DWCNT（8）。