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    Process for the preparation of N-phosphonomethylglycine and derivatives thereof
    5.
    发明申请
    Process for the preparation of N-phosphonomethylglycine and derivatives thereof 有权
    N-膦酰基甲基甘氨酸及其衍生物的制备方法

    公开(公告)号：US20050054871A1

    公开(公告)日：2005-03-10

    申请号：US10924265

    申请日：2004-08-23

    申请人： James Coleman ,  Jerry Ebner ,  Eric Haupfear ,  Patrick Lennon ,  Joseph Schaper ,  Samuel Tremont ,  Serge Wolfson ,  Philip Brodsky

    发明人： James Coleman ,  Jerry Ebner ,  Eric Haupfear ,  Patrick Lennon ,  Joseph Schaper ,  Samuel Tremont ,  Serge Wolfson ,  Philip Brodsky

    IPC分类号： C07F9/28 ,  C07F9/38

    CPC分类号： C07F9/3813 ,  Y02P20/582

    摘要： N-phosphonomethylamines are produced by reaction of an amine substrate with a halomethylphosphonic acid or salt thereof, a hydroxymethylphosphonic acid or salt thereof, or a dehydrated self-ester dimer, trimer or oligomer of hydroxymethylphosphonic acid. Among the products that may be prepared according to the process are N-phosphonomethylaminocarboxylic acids such as (e.g.) glyphosate, N-phosphonomethylaminoalkanols such as (e.g.) hydroxyethlaminomethylphosphonic acid, and N-acylaminomethylphosphonic acids such as (e.g.) N-carbamylaminomethylphosphonic acid. Certain reactions are conducted with a substantial excess of amine reactant in order to drive the conversion while avoiding excessive formation of bis(N-phosphonomethyl)amine by-products. Other reactions use a secondary amine substrate (such as iminodiacetic acid) and can be conducted at substantial equimolar ratios of halomethylaminomethylphosphonic acid or hydroxyaminomethylphosphonic acid to secondary amine reactant without significant formation of bis(phosphonomethyl)amine by-products. Further disclosed is a process for the preparation of hydroxymethylphosphonic acid self-ester dimers, trimers and oligomers by azeotropic dehydration.

    摘要翻译： N-膦酰基甲胺通过胺底物与卤甲基膦酸或其盐，羟甲基膦酸或其盐或羟甲基膦酸的脱水的自酯二聚物，三聚体或低聚物的反应来制备。 可根据该方法制备的产物是N-膦酰基乙基氨基羧酸，例如（例如）草甘膦，N-膦酰基甲基氨基链烷醇如（例如）羟基乙基氨基甲基膦酸和N-酰基氨基甲基膦酸如（例如）N-氨基甲酰基氨基甲基膦酸。 某些反应用大量过量的胺反应物进行，以驱动转化，同时避免过度形成双（N-膦酰基甲基）胺副产物。 其他反应使用仲胺底物（例如亚氨基二乙酸），并且可以以基本上等摩尔比率的卤代甲基氨基甲基膦酸或羟基氨基甲基膦酸与仲胺反应物进行反应，而不显着形成双（膦酰基甲基）胺副产物。 进一步公开了通过共沸脱水制备羟甲基膦酸自酯二聚体，三聚体和低聚物的方法。

    Process and apparatus for preparing frozen confection
    6.
    发明申请
    Process and apparatus for preparing frozen confection 审中-公开
    制备冷冻甜食的方法和设备

    公开(公告)号：US20050129819A1

    公开(公告)日：2005-06-16

    申请号：US10732629

    申请日：2003-12-10

    申请人： Patrick Lennon

    发明人： Patrick Lennon

    IPC分类号： A01J1/00

    CPC分类号： A23G9/285 ,  A23G9/22 ,  A23G9/44 ,  A23G9/48

    摘要： A method of making a combined frozen confection, equipment for forming same. The equipment especially comprises a filling nozzle. The invention is particularly directed to combined frozen confections formed in pop ups or the like. The combined frozen confection is especially a pop up having a shape extruded down the center, preferably an intricate shape such as a star or a pineapple, which remains recognizable over the length of the pop up cylinder. A second confection, preferably one having a different color or other appearance, flows into the pop-up cylinder around the periphery of the centrally extruded frozen confection to form a frozen confection combining the extruded frozen confection design and the peripheral frozen confection identifiable by consumers as different.

    摘要翻译： 一种冷冻甜食联合方法，其形成设备。 该设备特别包括一个填充喷嘴。 本发明特别涉及在弹出窗等中形成的组合冷冻甜点。 组合的冷冻甜食特别是具有从中心向下挤出的形状的弹出物，优选地是复杂的形状，例如星形或菠萝，其在弹出筒的长度上保持可识别。 第二个糖果，优选具有不同颜色或其他外观的糖果，流入围绕中央挤出的冷冻甜食周边的弹出圆筒，以形成冷冻甜食，将挤出的冷冻甜食设计和消费者可识别的外围冷冻甜点组合 不同。