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公开(公告)号：US20050033001A1
公开(公告)日：2005-02-10
申请号：US10918608
申请日：2004-08-12
申请人： James Cella , Slawomir Rubinsztajn
发明人： James Cella , Slawomir Rubinsztajn
摘要： A new silicone condensation reaction, the condensation between an alkoxy silane or siloxane or a dihydric phenol and an organo-hydrosilane or siloxane and catalysts therefore is described and claimed.
摘要翻译： 因此，新的有机硅缩合反应，烷氧基硅烷或硅氧烷或二元酚与有机氢硅烷或硅氧烷和催化剂之间的缩合被描述和要求保护。
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2.发明申请公开(公告)号：US20060211836A1
公开(公告)日：2006-09-21
申请号：US11081070
申请日：2005-03-15
IPC分类号： C08G77/20
摘要： Disclosed is a crosslinked polysiloxane network comprising both residual Si—H linkages and a Lewis acid catalyst, wherein the network is derived from a linear hydridosiloxane, a branched hydridosiloxane, a cyclic hydridosiloxane or a mixture of a linear hydridosiloxane or branched hydridosiloxane and a cyclic hydridosiloxane. Disclosed also is a method to produce the crosslinked polysiloxane network, alternatively accompanied by a silane with aliphatic, aromatic, or cycloaliphatic substituents by reacting in the presence of an effective amount of a Lewis acid catalyst a linear hydridosiloxane, a branched hydridosiloxane, a cyclic hydridosiloxane or a mixture of a linear hydridosiloxane or branched hydridosiloxane and a cyclic hydridosiloxane.
摘要翻译： 公开了一种包含残留Si-H键和路易斯酸催化剂的交联聚硅氧烷网络，其中网络衍生自线性氢硅氧烷，支链氢硅氧烷，环状氢化硅氧烷或直链羟基硅氧烷或支链氢硅氧烷和环状硅氢化合物的混合物 。 还公开了一种制备交联聚硅氧烷网络的方法，或者伴随着具有脂族，芳族或脂环族取代基的硅烷，在有效量的路易斯酸催化剂的存在下，使用线性羟基硅氧烷，支链氢硅氧烷，环状氢化硅氧烷 或直链羟基硅氧烷或支链氢硅氧烷和环状氢化硅氧烷的混合物。
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公开(公告)号：US20060152149A1
公开(公告)日：2006-07-13
申请号：US11326949
申请日：2006-01-06
申请人： Kyle Litz , James Cella , Qing Ye
发明人： Kyle Litz , James Cella , Qing Ye
IPC分类号： H01J1/62 , C08F230/04 , C07F15/00
CPC分类号： C07D487/22
摘要： Novel metal porphyrin compositions useful as organic phosphors are provided. The novel compositions are prepared from commercially available porphyrin-containing starting materials. In one instance a novel palladium-containing porphyrin composition having a number average molecular weight of greater than 12,000 grams per mole was prepared from 5,10,15,20-tetrakis(3′,5′-di(hydroxy)phenyl)-21H-23H-porphyrin by reaction first with palladium(II) acetylacetonate, followed by reaction with 2-bromo-2-methylpropionyl bromide, and subsequent group transfer reaction of the alpha-bromo ester groups with 9,9-dioctyl-2-vinylfluorene in the presence of CuBr as a radical initiator. The product polymer exhibited a number average molecular weight of 12,884 grams per mole, a weight average molecular weight of 14,338 grams per mole, and a robust red phosphorescent emission. Porphyrin containing copoylmers comprising structural units derived from 9,9-dioctyl-2-vinylfluorene and 9-anthracenylmethyl methacrylate were prepared in a similar fashion.
摘要翻译： 提供了可用作有机磷光体的新型金属卟啉组合物。 该新型组合物由市售的含卟啉原料制备。 在一种情况下，从5,10,15,20-四（3'，5'-二（羟基）苯基）-21H（5'）中制备数均分子量大于12,000克/摩尔的新颖的含钯卟啉组合物 -23H-卟啉通过首先与乙酰丙酮钯（II）反应，随后与2-溴-2-甲基丙酰溴反应，随后将α-溴酯基与9,9-二辛基-2-乙烯基芴的组转移反应 存在CuBr作为自由基引发剂。 产物聚合物的数均分子量为12,884克/摩尔，重均分子量为14,338克/摩尔，并具有坚固的红色磷光发射。 含有衍生自9,9-二辛基-2-乙烯基芴和9-蒽基甲基甲基丙烯酸酯的结构单元的含卟啉的共聚酰基酯以类似的方式制备。
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公开(公告)号：US20050258407A1
公开(公告)日：2005-11-24
申请号：US11189911
申请日：2005-07-26
申请人： James Cella , Rachid Kerboua
发明人： James Cella , Rachid Kerboua
CPC分类号： C08G64/045
摘要： Crosslinking between polymer chains having olefin groups occurs by heating the polymer chains in the presence of a catalyst. Mixtures of polymer and catalyst can be dried and cast into films at ambient temperatures and remain non-crosslinked and soluble for extended periods. However, upon heating of the polymer to temperatures of about 300° C. or greater in the presence of a catalyst, the polymer chains of the film are cured to produce an insoluble crosslinked matrix. The sudden and relatively complete nature of the crosslinking between the polymers under specific conditions is particularly useful to allow chromophores poled in a noncrosslinked polymer mixture to retain their uniform orientation after crosslinking has occurred.
摘要翻译： 在具有烯烃基团的聚合物链之间的交联通过在催化剂存在下加热聚合物链而发生。 聚合物和催化剂的混合物可以在环境温度下干燥并浇注成膜，并保持非交联并长时间溶解。 然而，当在催化剂存在下将聚合物加热到约300℃或更高的温度时，该膜的聚合物链被固化以产生不溶的交联基质。 在特定条件下聚合物之间交联的突然且相对完整的性质特别有用，以使非交联聚合物混合物中的发色团保持其交联发生后的均匀取向。
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公开(公告)号：US20070225464A1
公开(公告)日：2007-09-27
申请号：US11748195
申请日：2007-05-14
申请人： Larry Lewis , Kelly Chichak , James Cella , Joseph Shiang
发明人： Larry Lewis , Kelly Chichak , James Cella , Joseph Shiang
摘要： Optoelectronic devices include polysiloxanes derived from hydrosilation of an organometallic compound of formula L2MZ, wherein L and Z are independently bidentate ligands; at least one of L and Z comprises alkenyl, alkenylaryl, alkenyloxy, alkenyloxyaryl, alkynyl, alkynylaryl, alkynyloxy, alkynyloxyaryl, substituted alkenyl, substituted alkenylaryl, substituted alkenyloxy, substituted alkenyloxyaryl, substituted alkynyl, substituted alkynylaryl, substituted alkynyloxy, substituted alkynyloxyaryl, acrylate, methacrylate, or a combination thereof; and M is Zr, Nb, Mo, Tc, Ru, Rh, Pd, Ag, Cd, Hf, Ta, W, Re, Os, Ir, Pt, Au, Hg, Ga, Ge, In, Sn, Sb, Tl, Pd, Bi, Po, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, or Lu.
摘要翻译： 光电器件包括衍生自式L 2 MZ的有机金属化合物的硅氢化的聚硅氧烷，其中L和Z独立地是二齿配体; L和Z中的至少一个包括烯基，烯基芳基，烯氧基，烯基氧基芳基，炔基，炔基芳基，炔氧基，炔氧基芳基，取代的烯基，取代的烯基芳基，取代的烯氧基，取代的烯基氧基芳基，取代的炔基，取代的炔基芳基，取代的炔氧基，取代的炔氧基芳基，丙烯酸酯， 甲基丙烯酸酯或其组合; 并且M是Zr，Nb，Mo，Tc，Ru，Rh，Pd，Ag，Cd，Hf，Ta，W，Re，Os，Ir，Pt，Au，Hg，Ga，Ge，In，Sn，Sb， ，Pd，Bi，Po，La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb，Dy，Ho，Er，Tm，Yb或Lu。
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公开(公告)号：US20070215879A1
公开(公告)日：2007-09-20
申请号：US11384769
申请日：2006-03-20
申请人： Jie Liu , James Cella , Larry Lewis , Anil Duggal , James Spivack , Qing Ye
发明人： Jie Liu , James Cella , Larry Lewis , Anil Duggal , James Spivack , Qing Ye
CPC分类号： C09K9/02 , C09K2211/1007 , C09K2211/1014 , C09K2211/1044 , H01G9/2059 , H01L51/4206 , H01L51/5032 , H01L51/5221 , Y02E10/542
摘要： Described herein is an organic opto-electronic device comprising a cathode comprising at least one zero-valent metal; an anode; an opto-electronically active organic material; wherein said cathode is in contact with at least one organic ammonium salt. In certain embodiments, the organic ammonium salt has structure (I) wherein R1-R4 are independently at each occurrence a C1-C20 aliphatic radical, a C3-C20 cycloaliphatic radical, or a C3-C20 aromatic radical is disclosed and wherein X+ is selected from the group consisting of monovalent inorganic anions, monovalent organic anions, polyvalent inorganic anions, polyvalent organic anions, and mixtures thereof.
摘要翻译： 本文描述的是一种有机光电子器件，其包括：包含至少一种零价金属的阴极; 阳极; 光电活性有机材料; 其中所述阴极与至少一种有机铵盐接触。 在某些实施方案中，有机铵盐具有结构（I），其中R 1至R 4各自独立地为C 1 -C 3 20脂肪族基团，C 3 -C 20脂环族基团或C 3 -C 20脂肪族基团， 20芳族基团，其中X +选自一价无机阴离子，一价有机阴离子，多价无机阴离子，多价有机阴离子及其混合物。
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公开(公告)号：US20060131565A1
公开(公告)日：2006-06-22
申请号：US11017473
申请日：2004-12-20
申请人： Larry Lewis , Kyle Litz , Jie Liu , James Cella , Joseph Shiang , Tami Faircloth
发明人： Larry Lewis , Kyle Litz , Jie Liu , James Cella , Joseph Shiang , Tami Faircloth
CPC分类号： C08G61/10 , C08G61/02 , C08G61/12 , C08G61/122 , C08G61/124 , C08G61/125 , C08G61/126 , H01L51/0035 , H01L51/0039 , H01L51/0094 , H01L51/102 , H01L51/5092 , H05B33/26 , Y10T428/31504 , Y10T428/31663
摘要： A surface modified electrode comprising at least one conductive layer, and at least one reduced polymeric material, wherein the reduced polymeric material comprises at least one additional electron relative to a corresponding neutral polymeric precursor; and at least one cationic species is provided. Coating compositions and coated articles comprising the reduced polymeric materials are also provided. The coating compositions lower the work function of the electrode surface, thereby facilitating the production of more efficient electrooptic devices.
摘要翻译： 包括至少一个导电层和至少一种还原的聚合材料的表面改性电极，其中所述还原的聚合物材料相对于相应的中性聚合物前体包含至少一种另外的电子; 并提供至少一种阳离子种类。 还提供了包含还原聚合物材料的涂料组合物和涂覆制品。 涂层组合物降低了电极表面的功能，从而有助于生产更有效的电光装置。
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8.发明申请公开(公告)号：US20060127562A1
公开(公告)日：2006-06-15
申请号：US11013165
申请日：2004-12-15
申请人： Larry Lewis , Venkatesan Manivannan , Tami Faircloth , Jie Liu , James Cella
发明人： Larry Lewis , Venkatesan Manivannan , Tami Faircloth , Jie Liu , James Cella
CPC分类号： H01L51/0024 , H01L51/0039 , H01L51/5012 , Y02E10/549 , Y02P70/521 , Y10S428/917
摘要： In one embodiment the present invention discloses a method for making a first layer in an electroactive device comprising the steps of (i) preparing a composition by mixing at least one adhesion promoter material and at least one electroactive material; and (ii) depositing said composition onto a second electroactive layer of said electroactive device; and (iii) optionally further depositing a third electroactive layer onto the surface of said first layer opposite the second layer, wherein said composition enables adhesion between said first layer and said second layer or between said first layer and said third layer, or between said first layer and both said second layer and said third layer. In another embodiment the present invention discloses a method for improving adhesion between layers in an electroactive device comprising the steps of (i) depositing a surface treatment composition comprising at least one adhesion promoter material on at least one surface of a first electroactive layer, and (ii) depositing a second electroactive layer onto the surface of said first layer comprising said adhesion promoter; wherein said composition enables adhesion between said first layer and said second layer of said electroactive device. Electroactive layers and electroactive devices comprising said layers are also disclosed, as well as methods to make said electroactive devices. In another embodiment adhesion promoters comprising 9,9-disubstituted fluorenyl compounds are disclosed, as well as methods for making the same.
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公开(公告)号：US20070215865A1
公开(公告)日：2007-09-20
申请号：US11384770
申请日：2006-03-20
申请人： Jie Liu , James Cella , Larry Lewis , Anil Duggal , James Spivack , Qing Ye
发明人： Jie Liu , James Cella , Larry Lewis , Anil Duggal , James Spivack , Qing Ye
CPC分类号： H05B33/14 , H01G9/2004 , H01L51/0037 , H01L51/5032 , H01L51/5231 , Y02E10/542
摘要： Described herein is an organic opto-electronic device comprising a cathode comprising at least one zero-valent metal; an anode; an opto-electronically active organic material; wherein said cathode is in contact with at least one organic phosphonium salt. In certain embodiments, the organic phosphonium salt has structure (I) wherein R1-R4 are independently at each occurrence a C1-C20 aliphatic radical, a C3-C20 cycloaliphatic radical, or a C3-C20 aromatic radical is disclosed and wherein X− is selected from the group consisting of monovalent inorganic anions, monovalent organic anions, polyvalent inorganic anions, polyvalent organic anions, and mixtures thereof.
摘要翻译： 本文描述的是一种有机光电子器件，其包括：包含至少一种零价金属的阴极; 阳极; 光电活性有机材料; 其中所述阴极与至少一种有机鏻盐接触。 在某些实施方案中，有机鏻盐具有结构（I），其中R 1至R 4各自独立地为C 1 -C 3 20脂肪族基团，C 3 -C 20脂环族基团或C 3 -C 20脂肪族基团， 20芳族基团，其中X - 选自一价无机阴离子，一价有机阴离子，多价无机阴离子，多价有机阴离子及其混合物。
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10.发明申请公开(公告)号：US20060131567A1
公开(公告)日：2006-06-22
申请号：US11110276
申请日：2005-04-19
申请人： Jie Liu , Larry Lewis , Anil Duggal , Kyle Litz , James Cella , Joseph Shiang , Tami Faircloth
发明人： Jie Liu , Larry Lewis , Anil Duggal , Kyle Litz , James Cella , Joseph Shiang , Tami Faircloth
CPC分类号： H01L51/0043 , H01L51/0021 , H01L51/0035 , H01L51/0039 , H01L51/0094 , H01L51/5092 , H01L51/5221 , Y02E10/549 , Y10T428/31504 , Y10T428/31663
摘要： An electrooptic device and a surface modified electrode comprising a reduced organic material are provided. The reduced organic materials lower the work function of an electrode surface; they are also electro-active. These capabilities facilitate their use in production of more efficient electrooptic devices. The electrooptic device has at least a first conductive layer, a second conductive layer, and an electro-active layer comprising the reduced organic material disposed between the first and second conductive layers. The surface modified electrode comprises at least one conductive layer and at least one reduced organic material disposed upon a surface of said conductive layer. Methods for using the organic electro-active material for producing electrooptic devices, and operating the electrooptic devices are also disclosed. Coating compositions and coated articles comprising the reduced organic materials are also provided.
摘要翻译： 提供电光装置和包含还原有机材料的表面改性电极。 还原的有机材料降低了电极表面的功函数; 它们也是电活动的。 这些功能便于其在生产更高效的电光设备中使用。 电光装置具有至少第一导电层，第二导电层和包含设置在第一和第二导电层之间的还原有机材料的电活性层。 表面改性电极包括至少一个导电层和设置在所述导电层的表面上的至少一个还原的有机材料。 还公开了使用有机电活性材料制造电光装置和操作电光装置的方法。 还提供了包含还原的有机材料的涂料组合物和涂层制品。
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