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1.发明授权Separations by simulated moving bed chromatography operating at low k' values using weakly interacting adsorbents as the stationary phase 失效通过使用弱相互作用吸附剂作为固定相的低k值操作的模拟移动床层析分离
公开(公告)号：US5645729A
公开(公告)日：1997-07-08
申请号：US572911
申请日：1995-12-15
CPC分类号： B01D15/1828 , C07B57/00 , B01D15/325 , B01D15/361 , B01D2215/023
摘要： Resolution of a mixture of organic materials by simulated moving bed chromatography using a weakly interacting adsorbent as a stationary phase can be routinely effected with a liquid mobile phase characterized by atypically low values of k' with recoveries of at least 95% and a purity of at least 95%. In particular, values in the range 0.1
摘要翻译： 通过使用弱相互作用的吸附剂作为固定相的模拟移动床层析分离有机材料的混合物可以常规地用液体流动相进行，其特征在于非常低的k'值，回收率至少为95％，纯度为 至少95％。 特别地，推荐0.1
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公开(公告)号：US07102044B1
公开(公告)日：2006-09-05
申请号：US10882887
申请日：2004-06-30
IPC分类号： C07C2/64
摘要： The present invention comprises a process for removal of oxygenates from a paraffin-rich or olefin-rich paraffin stream which comprises passing a feed stream, comprising one or more C10 to C15 feed paraffins or C10 to C15 olefin-rich paraffin stream and one or more oxygenates through an adsorbent bed comprising one or more adsorbents selected from silica gel, activated alumina and sodium x zeolites to remove essentially all of said oxygenates; and recovering said paraffins. A second adsorbent bed may be employed to more thoroughly remove these oxygenates.
摘要翻译： 本发明包括从富含链烷烃或富烯烃的石蜡流中除去含氧化合物的方法，该方法包括将含有一个或多个C 10的进料流通入C 15 通过吸附床将含有一种或多种选自硅胶，活性氧化铝和吸附剂的吸附剂的烷烃或C 10向富含C 15的富烯烃链烷烃流和一种或多种含氧化合物进料， 钠x沸石以除去基本上所有的含氧化合物; 并回收所述石蜡。 可以使用第二吸附剂床来更彻底地除去这些含氧化合物。
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公开(公告)号：US06436354B1
公开(公告)日：2002-08-20
申请号：US09670239
申请日：2000-09-26
申请人： James W. Priegnitz , Anil R. Oroskar , Kenneth J. Stippich, Jr. , Gavin P. Towler , Kurt M. Vanden Bussche
发明人： James W. Priegnitz , Anil R. Oroskar , Kenneth J. Stippich, Jr. , Gavin P. Towler , Kurt M. Vanden Bussche
IPC分类号： B01J802
CPC分类号： H01M8/0631 , B01J8/0453 , B01J8/0488 , B01J8/0496 , B01J2208/00132 , B01J2208/00309 , B01J2208/0053 , B01J2219/00006 , C01B3/323 , C01B3/384 , C01B3/48 , C01B3/583 , C01B2203/0233 , C01B2203/0288 , C01B2203/044 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0816 , C01B2203/0822 , C01B2203/0827 , C01B2203/0866 , C01B2203/0877 , C01B2203/0883 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/107 , C01B2203/1076 , C01B2203/1082 , C01B2203/1217 , C01B2203/1235 , C01B2203/1241 , C01B2203/1258 , C01B2203/127 , C01B2203/1276 , C01B2203/1619 , C01B2203/1661 , C01B2203/169 , H01M8/0612 , Y02P20/128
摘要： A process and apparatus are disclosed for the operation of a fuel cell to generate electric power from a feed stream comprising a hydrocarbon or an alcohol. The fuel cell comprises a proton exchange membrane which produces electric power from a hydrogen product stream which comprises essentially no carbon monoxide. The hydrogen product stream is produced from the feed stream in a novel steam reforming zone containing a steam reforming catalyst disposed in a bell-shaped catalyst zone. The bell-shaped catalyst zone is disposed over a combustion zone such that the exhaust gas from the combustion flows around the bell-shaped catalyst zone to heat the catalyst from the inside and the outside of the catalyst zone. Furthermore, the bell-shaped catalyst zone maintains a high inlet and a high outlet temperature to avoid methane slippage in the steam reforming zone. Heat for the steam reforming zone is provided by a fuel stream and at least a portion of the anode waste gas stream from the fuel cell.
摘要翻译： 公开了一种用于操作燃料电池以从包含烃或醇的进料流产生电力的方法和装置。 燃料电池包括质子交换膜，其从基本上不含一氧化碳的氢产物流产生电力。 氢气产物流在新型蒸汽重整区中由进料流产生，该蒸汽重整区含有设置在钟形催化剂区中的蒸汽重整催化剂。 钟形催化剂区域设置在燃烧区域上，使得来自燃烧的废气流过钟形催化剂区域，以从催化剂区域的内部和外部加热催化剂。 此外，钟形催化剂区域保持高的入口和高出口温度，以避免蒸汽重整区域中的甲烷滑移。 用于蒸汽重整区的热量由燃料流和来自燃料电池的至少一部分阳极废气流提供。
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4.发明授权
公开(公告)号：US4483980A
公开(公告)日：1984-11-20
申请号：US532248
申请日：1983-09-14
摘要： A process for the recovery of glucose from an aqueous mixture of glucose and polysaccharides. The mixture is contacted with an X zeolite containing potassium cations at exchangeable cationic sites and selectively adsorbing glucose in the zeolite. The polysaccharides are removed from the zeolite and the adsorbed glucose recovered by means of a desorbent liquid. Preferred systems for effecting the process are countercurrent and co-current simulating moving beds.
摘要翻译： 从葡萄糖和多糖的水性混合物中回收葡萄糖的方法。 使混合物与含有可交换阳离子位点的钾阳离子的X沸石接触并选择性吸附沸石中的葡萄糖。 从沸石中除去多糖，并通过解吸液体回收吸附的葡萄糖。 实现该过程的优选系统是逆流和并流模拟移动床。
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公开(公告)号：US4408065A
公开(公告)日：1983-10-04
申请号：US246547
申请日：1981-03-23
IPC分类号： C07C69/88
CPC分类号： C07C69/88
摘要： An adsorptive separation process for separating methylparaben from a feed mixture comprising methylparaben and wintergreen oil, which process comprises contacting the feed mixture with an adsorbent comprising a type X or type Y zeolite, selectively adsorbing substantially all of the methylparaben to the substantial exclusion of the wintergreen oil and thereafter recovering high-purity methylparaben. A desorption step may be used to desorb the adsorbed methylparaben. The process is carried out preferably in the liquid phase.
摘要翻译： 用于从包含对羟基苯甲酸甲酯和冬青油的进料混合物中分离对羟基苯甲酸甲酯的吸附分离方法，该方法包括使进料混合物与包含X型或Y型沸石的吸附剂接触，所述吸附剂选择性吸附基本上所有的对羟基苯甲酸甲酯，基本排除冬青 油，然后回收高纯度对羟基苯甲酸甲酯。 解吸步骤可用于解吸所吸附的对羟基苯甲酸甲酯。 该方法优选在液相中进行。
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6.发明授权Separations by simulated moving bed chromatography operating at low K' values using weakly interating adsorbents as the stationary phase 失效通过使用弱相互作用吸附剂作为固定相的以低K'值运行的模拟移动床层析分离
公开(公告)号：US5626762A
公开(公告)日：1997-05-06
申请号：US573977
申请日：1995-12-18
申请人： James W. Priegnitz , Beth McCulloch
发明人： James W. Priegnitz , Beth McCulloch
CPC分类号： B01D15/1828 , C07B57/00 , B01D2215/023
摘要： Resolution of a mixture of organic materials by simulated moving bed chromatography using a weakly interacting adsorbent as a stationary phase can be routinely effected with a liquid mobile phase characterized by atypically low values of k' with recoveries of at least 95% and a purity of at least 95%. In particular, values in the range 0.1
摘要翻译： 通过使用弱相互作用的吸附剂作为固定相的模拟移动床层析分离有机材料的混合物可以常规地用液体流动相进行，其特征在于非常低的k'值，回收率至少为95％，纯度为 至少95％。 特别地，推荐0.1
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公开(公告)号：US5179219A
公开(公告)日：1993-01-12
申请号：US615106
申请日：1990-11-19
申请人： James W. Priegnitz
发明人： James W. Priegnitz
CPC分类号： C11B3/10 , C11B7/0025
摘要： The separation of free fatty acids from triglycerides is performed by an adsorptive chromatographic process in liquid phase with silica gel as the adsorbent. A ketone, having from 3 to 8 carbon atoms, such as 2-heptanone, an ester or an ether can be selected as the desorbent.
摘要翻译： 游离脂肪酸与甘油三酸酯的分离是通过硅胶作为吸附剂的液相吸附色谱法进行的。 可以选择具有3至8个碳原子的酮，例如2-庚酮，酯或醚，作为解吸剂。
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8.发明授权Separation of citric acid from fermentation broth with a weakly basic anionic exchange resin adsorbent 失效用弱碱性阴离子交换树脂吸附剂从发酵液中分离柠檬酸
公开(公告)号：US4851573A
公开(公告)日：1989-07-25
申请号：US121830
申请日：1987-11-16
IPC分类号： C07C51/47
CPC分类号： C07C51/47
摘要： Citric acid is separated from a fermentation broth by using an adsorbent comprising a water-insoluble macroreticular or gel weakly basic anionic exchange resin possessing tertiary amine functional groups or pyridine functional groups, said anionic exchange resin comprising a cross-linked acrylic or styrene resin matrix. Citric acid is desorbed by water or dilute sulfuric acid. The pH of the feed is maintained below the first ionization constant (pKa.sub.1) of citric acid to maintain selectivity.
摘要翻译： 通过使用包含具有叔胺官能团或吡啶官能团的水不溶性大网络或凝胶弱碱性阴离子交换树脂的吸附剂将柠檬酸与发酵液分离，所述阴离子交换树脂包含交联的丙烯酸或苯乙烯树脂基质。 柠檬酸被水或稀硫酸解吸。 饲料的pH值保持在柠檬酸的第一电离常数（pKa1）以下以保持选择性。
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公开(公告)号：US4340724A
公开(公告)日：1982-07-20
申请号：US890778
申请日：1978-03-27
摘要： A process for separating a ketose from a feed mixture comprising a ketose and an aldose which process comprises contacting the mixture with an adsorbent comprising a Y or X zeolite containing one or more selected cations at the exchangeable cationic sites thereby selectively adsorbing a ketose from the feed mixture and thereafter recovering the ketose. Preferably the ketose will be recovered by desorption from the adsorbent with a desorbent material.
摘要翻译： 一种从包含酮糖和醛糖的进料混合物中分离酮糖的方法，该方法包括使混合物与包含在可交换的阳离子位点上含有一个或多个选定阳离子的Y或X沸石的吸附剂接触，从而从进料中选择性吸附酮糖 混合物，然后回收酮糖酮。 优选地，通过用解吸剂材料从吸附剂解吸来回收酮糖。
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公开(公告)号：US6162267A
公开(公告)日：2000-12-19
申请号：US210042
申请日：1998-12-11
申请人： James W. Priegnitz , Anil R. Oroskar , Kenneth J. Stippich, Jr. , Gavin P. Towler , Kurt Vanden Bussche
发明人： James W. Priegnitz , Anil R. Oroskar , Kenneth J. Stippich, Jr. , Gavin P. Towler , Kurt Vanden Bussche
CPC分类号： H01M8/0631 , B01J8/0453 , B01J8/0488 , B01J8/0496 , B01J2208/00132 , B01J2208/00309 , B01J2208/0053 , B01J2219/00006 , C01B3/323 , C01B3/384 , C01B3/48 , C01B3/583 , C01B2203/0233 , C01B2203/0288 , C01B2203/044 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0816 , C01B2203/0822 , C01B2203/0827 , C01B2203/0866 , C01B2203/0877 , C01B2203/0883 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/107 , C01B2203/1076 , C01B2203/1082 , C01B2203/1217 , C01B2203/1235 , C01B2203/1241 , C01B2203/1258 , C01B2203/127 , C01B2203/1276 , C01B2203/1619 , C01B2203/1661 , C01B2203/169 , H01M8/0612 , Y02P20/128
摘要： A process and apparatus are disclosed for the operation of a fuel cell to generate electric power from a feed stream comprising a hydrocarbon or an alcohol. The fuel cell comprises a proton exchange membrane which produces electric power from a hydrogen product stream which comprises essentially no carbon monoxide. The hydrogen product stream is produced from the feed stream in a novel steam reforming zone containing a steam reforming catalyst disposed in a bell-shaped catalyst zone. The bell-shaped catalyst zone is disposed over a combustion zone such that the exhaust gas from the combustion flows around the bell-shaped catalyst zone to heat the catalyst from the inside and the outside of the catalyst zone. Furthermore, the bell-shaped catalyst zone maintains a high inlet and a high outlet temperature to avoid methane slippage in the steam reforming zone. Heat for the steam reforming zone is provided by a fuel stream and at least a portion of the anode waste gas stream from the fuel cell.
摘要翻译： 公开了一种用于操作燃料电池以从包含烃或醇的进料流产生电力的方法和装置。 燃料电池包括质子交换膜，其从基本上不含一氧化碳的氢产物流产生电力。 氢气产物流在新型蒸汽重整区中由进料流产生，该蒸汽重整区含有设置在钟形催化剂区中的蒸汽重整催化剂。 钟形催化剂区域设置在燃烧区域上，使得来自燃烧的废气流过钟形催化剂区域，以从催化剂区域的内部和外部加热催化剂。 此外，钟形催化剂区域保持高的入口和高出口温度，以避免蒸汽重整区域中的甲烷滑移。 用于蒸汽重整区的热量由燃料流和来自燃料电池的至少一部分阳极废气流提供。
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