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公开(公告)号：US20110160371A1
公开(公告)日：2011-06-30
申请号：US12840715
申请日：2010-07-21
申请人： Jihad Mohammed DAKKA , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smimova , Jorg Friedrich Wilhelm Weber , Stephen Zushma
发明人： Jihad Mohammed DAKKA , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smimova , Jorg Friedrich Wilhelm Weber , Stephen Zushma
IPC分类号： C08K5/07 , C07C69/616 , C07C69/612
CPC分类号： C08K5/12 , C07C51/31 , C07C67/08 , C07C67/31 , C07C69/73 , C07C69/732 , C07C69/738 , C07C2602/10 , C08K5/10 , C07C59/84 , C07C59/86
摘要： Provided is a process for making non-phthalate plasticizers, by acylating an aromatic compound with a succinic anhydride to form a keto-acid, and then esterifying the keto-acid with C4-C13 OXO-alcohols to form a plasticizer compound. The aromatic rings of the aromatic compound may also be optionally hydrogenated.
摘要翻译： 提供了制备非邻苯二甲酸酯增塑剂的方法，通过用琥珀酸酐酰化芳族化合物以形成酮酸，然后用C4-C13OXO-醇酯化酮酸以形成增塑剂化合物。 芳族化合物的芳环也可以任选氢化。
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公开(公告)号：US08604114B2
公开(公告)日：2013-12-10
申请号：US12840715
申请日：2010-07-21
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smirnova , Jörg Friedrich Wilhelm Weber , Stephen Zushma
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smirnova , Jörg Friedrich Wilhelm Weber , Stephen Zushma
CPC分类号： C08K5/12 , C07C51/31 , C07C67/08 , C07C67/31 , C07C69/73 , C07C69/732 , C07C69/738 , C07C2602/10 , C08K5/10 , C07C59/84 , C07C59/86
摘要： Provided is a process for making non-phthalate plasticizers, by acylating an aromatic compound with a succinic anhydride to form a keto-acid, and then esterifying the keto-acid with C4-C13 OXO-alcohols to form a plasticizer compound. The aromatic rings of the aromatic compound may also be optionally hydrogenated.
摘要翻译： 提供了制备非邻苯二甲酸酯增塑剂的方法，通过用琥珀酸酐酰化芳族化合物以形成酮酸，然后用C4-C13OXO-醇酯化酮酸以形成增塑剂化合物。 芳族化合物的芳环也可以任选氢化。
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公开(公告)号：US08568846B2
公开(公告)日：2013-10-29
申请号：US12880586
申请日：2010-09-13
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Jon Edmond Randolph Stanat , Karla Schall Colle , Francisco Manuel Benitez , Peter Stokes James , Allen David Godwin , Carl Robert Beck
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Jon Edmond Randolph Stanat , Karla Schall Colle , Francisco Manuel Benitez , Peter Stokes James , Allen David Godwin , Carl Robert Beck
CPC分类号： C07C67/38 , C08K5/103 , Y10T428/139 , Y10T442/20 , C07C69/30
摘要： Provided are compositions, processes for making, and processes for using neoalkyl polyol esters and triglycerides as plasticizers. In one form, a neoalkylester triglyceride plasticizers can be produced by (i) drying a polyol feedstream; (ii) contacting in a reactor the dried polyol feedstream with a neoacid feedstream under effective temperature, pressure and time to form a neoalkylester plasticizer effluent stream, and (iii) purifying the neoalkylester plasticizer effluent stream to remove unreacted polyol and unreacted neoacid to form a neoalkylester plasticizer. Such plasticizers can be phthalate-free and provide outstanding properties including a suitable melting or pour point, glass transition temperature, low volatility, increased compatibility, increased hydrolytic stability, and excellent low temperature properties in a range of polymeric resins.
摘要翻译： 提供了组合物，制备方法和使用新烷基多元醇酯和甘油三酸酯作为增塑剂的方法。 在一种形式中，新烷基酯甘油三酯增塑剂可以通过（i）干燥多元醇进料流来制备; （ii）在有效温度，压力和时间下在干燥的多元醇原料流中与干燥的多元醇原料流接触以形成新的烷基酯增塑剂流出物流，和（iii）纯化新烷基酯增塑剂流出物流以除去未反应的多元醇和未反应的新酸，形成 新烷基酯增塑剂。 这种增塑剂可以是无邻苯二甲酸酯，并且提供突出的性能，包括合适的熔点或倾点，玻璃化转变温度，低挥发性，增加的相容性，增加的水解稳定性和在一系列聚合物树脂中的优异的低温性能。
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公开(公告)号：US20110165355A1
公开(公告)日：2011-07-07
申请号：US12880586
申请日：2010-09-13
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Jon Edmond Randolph Stanat , Karla Schall Colle , Francisco Manuel Benitez , Peter Stokes James , Allen David Godwin , Carl Robert Beck
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Jon Edmond Randolph Stanat , Karla Schall Colle , Francisco Manuel Benitez , Peter Stokes James , Allen David Godwin , Carl Robert Beck
CPC分类号： C07C67/38 , C08K5/103 , Y10T428/139 , Y10T442/20 , C07C69/30
摘要： Provided are compositions, processes for making, and processes for using neoalkyl polyol esters and triglycerides as plasticizers. In one form, a neoalkylester triglyceride plasticizers can be produced by (i) drying a polyol feedstream; (ii) contacting in a reactor the dried polyol feedstream with a neoacid feedstream under effective temperature, pressure and time to form a neoalkylester plasticizer effluent stream, and (iii) purifying the neoalkylester plasticizer effluent stream to remove unreacted polyol and unreacted neoacid to form a neoalkylester plasticizer. Such plasticizers can be phthalate-free and provide outstanding properties including a suitable melting or pour point, glass transition temperature, low volatility, increased compatibility, increased hydrolytic stability, and excellent low temperature properties in a range of polymeric resins.
摘要翻译： 提供了组合物，制备方法和使用新烷基多元醇酯和甘油三酸酯作为增塑剂的方法。 在一种形式中，新烷基酯甘油三酯增塑剂可以通过（i）干燥多元醇进料流来制备; （ii）在有效温度，压力和时间下在干燥的多元醇原料流中与干燥的多元醇原料流接触以形成新的烷基酯增塑剂流出物流，和（iii）纯化新烷基酯增塑剂流出物流以除去未反应的多元醇和未反应的新酸，形成 新烷基酯增塑剂。 这种增塑剂可以是无邻苯二甲酸酯，并且提供突出的性能，包括合适的熔点或倾点，玻璃化转变温度，低挥发性，增加的相容性，增加的水解稳定性和在一系列聚合物树脂中的优异的低温性能。
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5.发明申请METHODS OF MAKING 6-HYDROXYHEXANOPHENONE AND 5-BENZOYLPENTANOIC ACID AND MONO OR DIESTERS THEREOF 审中-公开制备6-羟基六氢呋喃酮和5-苯甲酰基戊酸及其单体或二氧化钛的方法公开(公告)号：US20120035308A1
公开(公告)日：2012-02-09
申请号：US13197253
申请日：2011-08-03
申请人： Kun Wang , Jihad Mohammed Dakka , Edmund John Mozeleski , Francisco Manuel Benitez , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova , Stephen Zushma
发明人： Kun Wang , Jihad Mohammed Dakka , Edmund John Mozeleski , Francisco Manuel Benitez , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova , Stephen Zushma
IPC分类号： C08K5/12 , C07C45/28 , C08K5/101 , C07C67/40 , C07C67/08 , C07C69/612 , C07C69/716
CPC分类号： C07C45/53 , C07C51/235 , C07C67/08 , C07C67/29 , C07C67/31 , C07C69/24 , C07C69/738 , C07C407/00 , C07C2601/14 , C08K5/10 , C07C49/82 , C07C409/14 , C07C59/84 , C07C69/732 , C07C69/73 , C07C69/28
摘要： Mono- or diester plasticizers of the formula: wherein A is either —OC(O)R′ or ═O, and X is either —COC(O)R or —C(O)OR, and R and R′ are C3 to C13 alkyl, which are the same or different, formed from cyclohexylbenzene and processes of making them.
摘要翻译： 单或二酯增塑剂，其通式为：其中A为-OC（O）R'或= O，X为-COC（O）R或-C（O）OR，R和R'为C 3〜 C13烷基，它们是相同或不同的，由环己基苯形成及其制备方法。
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6.发明授权Oil based polyols or diacids esterified with oxo-acids or oxo-alcohols for producing plasticizers 有权用含氧酸或羰基醇酯化的油基多元醇或二酸用于生产增塑剂公开(公告)号：US08329795B2
公开(公告)日：2012-12-11
申请号：US12830606
申请日：2010-07-06
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova
IPC分类号： C08K5/00
CPC分类号： C07C67/08 , C07C5/32 , C07C29/147 , C07C45/50 , C07C51/16 , C07C67/26 , C07C69/28 , C07C69/75 , C07C2601/14 , C07C2603/68 , C08K5/10 , C07C35/08 , C07C47/32 , C07C61/08
摘要： Oxo-diesters of cyclic olefins, methods of making them and their use as plasticizers in polymer compositions are disclosed.
摘要翻译： 公开了环烯烃的氧代二酯，其制备方法及其作为增塑剂在聚合物组合物中的用途。
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公开(公告)号：US20110184105A1
公开(公告)日：2011-07-28
申请号：US12892680
申请日：2010-09-28
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Francisco Manuel Benitez , Catherine Anne Faler , Allen David Godwin , Jörg Friedrich Wilhelm Weber , Diana S. Smirnova
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Francisco Manuel Benitez , Catherine Anne Faler , Allen David Godwin , Jörg Friedrich Wilhelm Weber , Diana S. Smirnova
CPC分类号： C07C69/612 , C07C69/76
摘要： A process for making non-phthalate, 1,2-phenylene oxo-diester plasticizers for polymer compositions, by selectively hydrogenating naphthalene to form a partially hydrogenated naphthalene, oxygenating said partially hydrogenated naphthalene to form phenylene diacids, and esterifying said phenylene diacids with oxo-alcohols to form 1,2-phenylene oxo-diesters. Also a process for making phenylene oxo-diester plasticizers by selectively brominating xylenes to form bisbromomethylbenzene, catalytic carboalkoxylation of the bromo-compound to form phenylene diacetate, followed by transesterification to form the phenylene oxo-diester.
摘要翻译： 通过选择性氢化萘以形成部分氢化的萘来制备用于聚合物组合物的非邻苯二甲酸酯，1,2-亚苯基氧代二酯增塑剂的方法，将所述部分氢化的萘氧化以形成亚苯基二酸，并用所述亚苯基二酸酯化所述亚苯基二酸， 醇形成1,2-亚苯基氧代二酯。 也是通过选择性溴化二甲苯以形成双溴甲苯制备亚苯基二氧代二酯增塑剂的方法，溴化合物的催化羰基烷氧基化形成亚苯基二乙酸酯，然后酯交换以形成亚苯基氧代二酯。
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公开(公告)号：US20130035431A1
公开(公告)日：2013-02-07
申请号：US13198851
申请日：2011-08-05
申请人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
发明人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
IPC分类号： C08K5/12 , C07C69/736 , C07C67/08 , C07C67/343 , C08L33/00 , C08L67/00 , C08L75/04 , C08L31/04 , C08L21/00 , C07C69/612 , C08L27/06
CPC分类号： C07C67/08 , C07C67/343 , C07C69/612 , C07C69/734 , C08K5/0016 , C08K5/11
摘要： Provided are compounds of the formula: wherein m=0-3 and n=0-3, and R1 represents CxH2x wherein x=0 to 4 or cyclohexane; R2 represents H, a C1-C6 alkyl group at any of the ortho-, meta- or para-positions, a residue including heteroatoms chosen from O, N, and S, or mixtures thereof; and R3 and R4 represent hydrocarbon residues of OXO-C5-C9 alcohols which are different isomers of equal carbon number or different in carbon number. Also provided are processes for making the compounds and plasticized polymer compositions containing said compounds.
摘要翻译： 提供下式的化合物：其中m = 0-3且n = 0-3，并且R1表示CxH2x，其中x = 0至4或环己烷; R 2表示H，任何邻位，间位或对位的C 1 -C 6烷基，包括选自O，N和S的杂原子的残基或其混合物; 并且R 3和R 4代表相同碳数或碳数不同的不同异构体的OXO-C5-C9醇的烃残基。 还提供了制备含有所述化合物的化合物和增塑聚合物组合物的方法。
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公开(公告)号：US08604110B2
公开(公告)日：2013-12-10
申请号：US13198851
申请日：2011-08-05
申请人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
发明人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
CPC分类号： C07C67/08 , C07C67/343 , C07C69/612 , C07C69/734 , C08K5/0016 , C08K5/11
摘要： Provided are compounds of the formula: wherein m=0-3 and n=0-3, and R1 represents CxH2x wherein x=0 to 4 or cyclohexane; R2 represents H, a C1-C6 alkyl group at any of the ortho-, meta- or para-positions, a residue including heteroatoms chosen from O, N, and S, or mixtures thereof; and R3 and R4 represent hydrocarbon residues of OXO-C5-C9 alcohols which are different isomers of equal carbon number or different in carbon number. Also provided are processes for making the compounds and plasticized polymer compositions containing said compounds.
摘要翻译： 提供下式的化合物：其中m = 0-3且n = 0-3，并且R1表示CxH2x，其中x = 0至4或环己烷; R 2表示H，任何邻位，间位或对位的C 1 -C 6烷基，包括选自O，N和S的杂原子的残基或其混合物; 并且R 3和R 4代表相同碳数或碳数不同的不同异构体的OXO-C5-C9醇的烃残基。 还提供了制备含有所述化合物的化合物和增塑聚合物组合物的方法。
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10.发明申请OIL BASED POLYOLS OR DIACIDS ESTERIFIED WITH OXO-ACIDS OR OXO-ALCOHOLS FOR PRODUCING PLASTICIZERS 有权用于生产聚合物的含氧基或异丙醇的基于油的多元醇或多元醇公开(公告)号：US20110009548A1
公开(公告)日：2011-01-13
申请号：US12830606
申请日：2010-07-06
申请人： Jihad Mohammed DAKKA , Edmund Joseph Mozeleski , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova
发明人： Jihad Mohammed DAKKA , Edmund Joseph Mozeleski , Lisa Saunders Baugh , Allen David Godwin , Diana S. Smirnova
CPC分类号： C07C67/08 , C07C5/32 , C07C29/147 , C07C45/50 , C07C51/16 , C07C67/26 , C07C69/28 , C07C69/75 , C07C2601/14 , C07C2603/68 , C08K5/10 , C07C35/08 , C07C47/32 , C07C61/08
摘要： Oxo-diesters of cyclic olefins, methods of making them and their use as plasticizers in polymer compositions are disclosed.
摘要翻译： 公开了环烯烃的氧代二酯，其制备方法及其作为增塑剂在聚合物组合物中的用途。
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