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    Alkylaromatic process with removal of aromatic by-products
    1.
    发明授权
    Alkylaromatic process with removal of aromatic by-products 失效
    去除芳香族副产物的烷基芳族化合物

    公开(公告)号：US5276231A

    公开(公告)日：1994-01-04

    申请号：US919311

    申请日：1992-07-27

    申请人： Joseph A. Kocal ,  Donald J. Korous

    发明人： Joseph A. Kocal ,  Donald J. Korous

    IPC分类号： C07C15/107 ,  C07C2/66 ,  C07C2/68

    CPC分类号： C07C15/107

    摘要： An improved process for the production of alkylated aromatic compounds by paraffin dehydrogenation and aromatic alkylation is disclosed. Aromatic by-products normally formed in paraffin dehydrogenation are selectively removed using at least one aromatics removal zone. Removal of these aromatic by-products significantly reduces the deactivation rate of solid alkylation catalysts. The improved process produces a detergent alkylate product that is significantly more linear than that produced by the prior art process.

    摘要翻译： 公开了通过石蜡脱氢和芳族烷基化制备烷基化芳族化合物的改进方法。 通常使用至少一个芳族化合物去除区选择性地除去在链烷烃脱氢中通常形成的芳族副产物。 去除这些芳族副产物显着降低了固体烷基化催化剂的失活速率。 改进的方法产生的洗涤剂烷基化产物比现有技术方法显着更线性。

    Process for producing terephthalic acid
    2.
    发明授权
    Process for producing terephthalic acid 有权
    对苯二甲酸生产方法

    公开(公告)号：US08884055B2

    公开(公告)日：2014-11-11

    申请号：US13155553

    申请日：2011-06-08

    申请人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    发明人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC分类号： C07C51/16 ,  C07C51/265

    CPC分类号： C07C51/265 ,  C07C51/42 ,  Y02P20/52 ,  Y02P20/542 ,  C07C63/26

    摘要： A solid terephthalic acid composition and a process for producing terephthalic acid from para-xylene. The process comprises forming a mixture comprising the para-xylene, a solvent, a bromine source, and a catalyst; and oxidizing the para-xylene by contacting the mixture with an oxidizing agent at oxidizing conditions to produce a solid oxidation product comprising terephthalic acid, para-toluic acid, 4-carboxybenzaldehyde. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an dialkyl imidazolium ionic liquid; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium. The solid terephthalic acid composition comprises, less than about 4,000 ppm-wt 4-carboxybenzaldehyde content, and more than about 2,000 ppm-wt a para-toluic acid.

    摘要翻译： 固体对苯二甲酸组合物和由对二甲苯生产对苯二甲酸的方法。 该方法包括形成包含对二甲苯，溶剂，溴源和催化剂的混合物; 并通过在氧化条件下将氧化剂与氧化剂接触来氧化对二甲苯以产生包含对苯二甲酸，对甲苯甲酸，4-羧基苯甲醛的固体氧化产物。 溶剂包括具有1至7个碳原子的羧酸和二烷基咪唑鎓离子液体; 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。 固体对苯二甲酸组合物包含小于约4,000ppm重量的4-羧基苯甲醛含量和大于约2,000ppm重量的对甲苯甲酸。

    PROCESS FOR OXIDIZING ALKYL AROMATIC COMPOUNDS
    4.
    发明申请
    PROCESS FOR OXIDIZING ALKYL AROMATIC COMPOUNDS 有权
    用于氧化烷基芳族化合物的方法

    公开(公告)号：US20120004449A1

    公开(公告)日：2012-01-05

    申请号：US13155519

    申请日：2011-06-08

    申请人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina L. Kuznetsova ,  Bair S. Bal'zhinimaev

    发明人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina L. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC分类号： C07C51/265 ,  C07C51/42 ,  C07C51/16

    CPC分类号： C07C51/265 ,  C07C63/16 ,  C07C63/24 ,  C07C63/26 ,  C07C63/06

    摘要： A process and a mixture for oxidizing an alkyl-aromatic compound comprises forming a mixture comprising the alkyl-aromatic compound, a solvent, a bromine source, and a catalyst; and contacting the mixture with an oxidizing agent at oxidizing conditions to produce an oxidation product comprising at least one of an aromatic aldehyde, an aromatic alcohol, an aromatic ketone, and an aromatic carboxylic acid. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an ionic liquid selected from the group consisting of an imidazolium ionic liquid, a pyridinium ionic liquid, a phosphonium ionic liquid, a tetra alkyl ammonium ionic liquid, and combinations thereof. The catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium.

    摘要翻译： 用于氧化烷基 - 芳族化合物的方法和混合物包括形成包含烷基 - 芳族化合物，溶剂，溴源和催化剂的混合物; 以及在氧化条件下使所述混合物与氧化剂接触以产生包含芳族醛，芳族醇，芳族酮和芳族羧酸中的至少一种的氧化产物。 溶剂包括具有1至7个碳原子的羧酸和选自咪唑鎓离子液体，吡啶鎓离子液体，鏻离子液体，四烷基铵离子液体及其组合的离子液体。 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。

    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS
    5.
    发明申请
    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS 有权
    用于连续生成聚合物的催化方法

    公开(公告)号：US20110313210A1

    公开(公告)日：2011-12-22

    申请号：US13193227

    申请日：2011-07-28

    申请人： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    发明人： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    IPC分类号： C07C31/20

    CPC分类号： C07C29/132 ,  C10G3/44 ,  C10G3/46 ,  C10G3/48 ,  C10G3/52 ,  C10G3/56 ,  C10G2300/1014 ,  Y02P20/52 ,  Y02P30/20 ,  C07C31/202 ,  C07C31/205

    摘要： A catalytic process for generating at least one polyol from a feedstock comprising cellulose is performed in a continuous manner. The process involves, contacting, continuously, hydrogen, water, and a feedstock comprising cellulose, with a catalyst to generate an effluent stream comprising at least one polyol, water, hydrogen, and at least one co-product. The water, hydrogen, and at least one co-product are separated from the effluent stream and recycled to the reaction zone. The polyol is recovered from the effluent stream.

    摘要翻译： 以包含纤维素的原料生成至少一种多元醇的催化方法是以连续方式进行的。 该方法包括使含有纤维素的氢，水和原料与催化剂连续地接触，以产生包含至少一种多元醇，水，氢和至少一种共同产物的流出物流。 将水，氢和至少一种副产物与流出物流分离并再循环至反应区。 从流出物流中回收多元醇。

    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS
    6.
    发明申请
    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS 有权

    公开(公告)号：US20110313209A1

    公开(公告)日：2011-12-22

    申请号：US13193200

    申请日：2011-07-28

    申请人： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    发明人： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    IPC分类号： C07C29/74

    CPC分类号： C07C29/132 ,  C07C31/20

    摘要： A catalytic process for generating at least one polyol from a feedstock comprising cellulose is performed in a continuous manner. The process involves, contacting, continuously, hydrogen, water, and a feedstock comprising cellulose, with a catalyst to generate an effluent stream comprising at least one polyol, water, hydrogen, and at least one co-product. The water, hydrogen, and at least one co-product are separated from the effluent stream and recycled to the reaction zone. The polyol is recovered from the effluent stream.

    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME
    8.
    发明申请
    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME 有权
    低氧生物质衍生的热解油及其生产方法

    公开(公告)号：US20110201855A1

    公开(公告)日：2011-08-18

    申请号：US12707433

    申请日：2010-02-17

    申请人： Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    发明人： Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    IPC分类号： C10G1/00

    CPC分类号： C10G3/44 ,  C10G3/45 ,  C10G3/47 ,  C10G3/48 ,  C10G3/49 ,  C10G2400/30 ,  Y02E50/14 ,  Y02P30/20

    摘要： Low oxygen biomass-derived pyrolysis oils and methods for producing them from carbonaceous biomass feedstock are provided. The carbonaceous biomass feedstock is pyrolyzed in the presence of a catalyst comprising base metal-based catalysts, noble metal-based catalysts, treated zeolitic catalysts, or combinations thereof to produce pyrolysis gases. During pyrolysis, the catalyst catalyzes a deoxygenation reaction whereby at least a portion of the oxygenated hydrocarbons in the pyrolysis gases are converted into hydrocarbons. The oxygen is removed as carbon oxides and water. A condensable portion (the vapors) of the pyrolysis gases is condensed to low oxygen biomass-derived pyrolysis oil.

    摘要翻译： 提供了低氧生物质衍生的热解油及其从碳质生物质原料生产它们的方法。 在含有贱金属基催化剂，贵金属基催化剂，经处理的沸石催化剂或其组合的催化剂存在下，碳质生物质原料热解产生裂解气。 在热解期间，催化剂催化脱氧反应，由此将热解气体中的至少一部分氧化烃转化成烃。 作为碳氧化物和水除去氧气。 热解气体的可冷凝部分（蒸汽）被冷凝成低氧生物质衍生的裂解油。