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公开(公告)号：US06927240B2
公开(公告)日：2005-08-09
申请号：US10220787
申请日：2001-02-21
IPC分类号： A61K8/02 , A61K8/04 , A61K8/30 , A61K8/31 , A61K8/34 , A61K8/37 , A61K8/39 , A61K8/42 , A61K8/55 , A61K8/58 , A61K8/60 , A61K8/64 , A61K8/73 , A61Q17/04 , A61Q19/00 , B01F17/22 , B01F17/34 , B01F17/42 , B01F17/56 , B01J2/02 , B01J2/18 , A01N25/00 , A61N47/00 , B29G9/00
CPC分类号： B01J2/18 , A61K8/02 , A61K8/0225 , A61K8/342 , A61K8/375 , A61K8/39 , A61K8/604 , A61K8/645 , A61Q19/00 , B01J2/02
摘要： A process for making granular solids involving: (a) providing a substantially anhydrous preparation, which is solid at room temperature and contain at least one cosmetic feed material; (b) liquifying the substantially anhydrous preparation to form a melt; (c) providing a vibrating casting plate used for droplet formation; (d) introducing the melt onto the vibrating casting plate to form melt droplets thereon; (e) providing a cooling medium; and (f) contacting the melt droplets with the cooling medium which is passed countercurrently to the melt droplets, thus forming the granular solids, and wherein the granular solids have a monodisperse particle size distribution and are substantially free of particles having a diameter of less than 0.3 mm.
摘要翻译： 制备颗粒状固体的方法包括：（a）提供基本上无水的制剂，其在室温下为固体并含有至少一种化妆品原料; （b）液化基本上无水的制剂以形成熔体; （c）提供用于液滴形成的振动铸造板; （d）将熔体引入到振动铸塑板上以在其上形成熔体液滴; （e）提供冷却介质; 和（f）使熔体液滴与冷却介质接触，冷却介质与熔融液体逆流通过，从而形成颗粒状固体，并且其中颗粒状固体具有单分散粒度分布，并且基本上不含直径小于 0.3毫米。
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公开(公告)号：US5712235A
公开(公告)日：1998-01-27
申请号：US617906
申请日：1996-03-15
申请人： Claus Nieendick , Gerhard Wollmann , Bernd Richter , Karl-Heinz Schmid , Andreas Syldath , Bernd Fabry
发明人： Claus Nieendick , Gerhard Wollmann , Bernd Richter , Karl-Heinz Schmid , Andreas Syldath , Bernd Fabry
IPC分类号： C11D9/26 , C07C53/126 , C07C59/125 , C11D1/52 , C11D1/66 , C11D9/30 , C11D9/32 , C11D10/04 , C11D17/00 , C11D1/68 , C11D1/74 , C11D3/22
CPC分类号： C11D10/04 , C07C53/126 , C07C59/125 , C11D17/006 , C11D1/525 , C11D1/662
摘要： New toilet soaps contain: (a1) 4 to 7% by weight alkyl and/or alkenyl oligoglycosides and/or (a2) 2 to 7% by weight fatty acid N-allcylpolyhydroxyalkylamide; (b) 45 to 95% by weight soap and (c) 0 to 10% by weight anionic surfactants selected from the group of alkyl sulphates, isethionates, taurides, sarcosinates, mono- and dialkylsulfosuccinates, ether carboxylic acids, sulphotriglycerides and alkyloligoglucoside sulphates. These new soaps are characterized among others by an improved creaminess, a high foaming power, remarkable cosmetic compatibility with the skin and mechanical firmness.
摘要翻译： PCT No.PCT / EP94 / 02968 Sec。 371日期：1996年3月15日 102（e）1996年3月15日PCT 1994年9月6日PCT公布。 出版物WO95 / 07975 日期1995年3月23日新厕所肥皂包含：（a1）4至7重量％的烷基和/或烯基寡糖苷和/或（a2）2至7重量％的脂肪酸N-全酰基聚羟烷基酰胺; （b）45至95重量％的皂和（c）0至10重量％的阴离子表面活性剂，其选自烷基硫酸盐，羟乙磺酸盐，牛磺酸盐，肌氨酸盐，单和二烷基磺基琥珀酸盐，醚羧酸，甘油三酸甘油酯和烷基寡葡糖苷硫酸盐。 这些新肥皂的特征在于其改善的奶油味，高发泡力，与皮肤的显着的化学兼容性和机械硬度。
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3.发明申请Composition for controlled tempering by means of phase change, production and use thereof 审中-公开通过相变，生产和使用控制回火的组成公开(公告)号：US20060233986A1
公开(公告)日：2006-10-19
申请号：US10544023
申请日：2003-12-19
申请人： Bernhard Gutsche , Gerhard Wollmann , Albert Strube , Eike Mahnke
发明人： Bernhard Gutsche , Gerhard Wollmann , Albert Strube , Eike Mahnke
IPC分类号： B32B27/32
CPC分类号： C09K5/063 , A61F2007/0292 , F28D20/02 , F28D2020/0008 , Y02E60/145 , Y02E60/147 , Y10T428/1334
摘要： This disclosure relates to a heat or cold storage composition comprising at least one continuous and at least one discontinuous phase, the continuous phase being liquid or at least plastic at a temperature of −10 to 50° C. and the discontinuous phase—present in the continuous phase—being particulate and containing as phase change material (PCM) at least 10% by weight of an organic compound with a melting point of 0 to 50° C. and at least one structuring polymeric compound. It also relates to the use of a composition according to the invention for controlled heating/cooling by phase change and to a device for the controlled heating/cooling of an object by phase change at least comprising a container for holding a composition according to the invention.
摘要翻译： 本公开涉及包含至少一个连续和至少一个不连续相的热或冷储存组合物，所述连续相是液体或在-10至50℃的温度下至少是塑料，并且所述不连续相存在于 连续相分散的颗粒并含有至少10重量％的熔点为0至50℃的有机化合物和至少一种结构化聚合化合物作为相变材料（PCM）。 它还涉及根据本发明的组合物用于通过相变的受控加热/冷却以及通过相变的用于受控加热/冷却物体的装置的用途，所述相变至少包括用于保持根据本发明的组合物的容器 。
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公开(公告)号：US06911164B2
公开(公告)日：2005-06-28
申请号：US10259684
申请日：2002-09-27
摘要： A process for making spherically-shaped sterol preparations involving: (a) providing a liquid sterol preparation; (b) forming the liquid sterol preparation into liquid sterol droplets; and (c) solidifying the liquid sterol droplets to form the spherically-shaped sterol preparations.
摘要翻译： 制备球形甾醇制剂的方法，包括：（a）提供液体甾醇制剂; （b）将液体甾醇制剂形成液体甾醇液滴; 和（c）固化液体甾醇液滴以形成球形甾醇制剂。
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5.发明授权
公开(公告)号：US4976892A
公开(公告)日：1990-12-11
申请号：US323517
申请日：1989-03-14
CPC分类号： C11C3/02
摘要： A process for the continuous transesterification of C.sub.6 -C.sub.22 fatty acid lower alkyl esters, particularly methyl esters, with polyhydric C.sub.2 -C.sub.5 alcohols, particularly glycerol, in a reaction column comprising a rectifying and reaction section, alkaline catalysts and polyhydric alcohol are introduced into the upper part of the reaction column and boiling fatty acid methyl ester is introduced into the middle part of the reaction column. The product collected in the sump of the column is removed, heated and returned to the lower part of the reaction column. Product is removed from the sump. Lower alkanols passing from the reaction column section to the rectifying section are rectified. The reaction column is operated in boiling equilibrium in its lower part and predominantly in an absorption/desorption equilibrium in its upper part.
摘要翻译： 在包含精馏和反应部分的反应塔，碱性催化剂和多元醇中，将C6-C22脂肪酸低级烷基酯，特别是甲基酯与多元醇C 2 -C 5醇，特别是甘油连续酯交换的方法被引入 将反应塔上部和沸腾脂肪酸甲酯引入反应塔的中间部分。 将收集在柱的集水槽中的产物除去，加热并返回到反应塔的下部。 产品从集水槽中取出。 将从反应塔部分流出的低级链烷醇精馏。 反应塔在其下部以沸腾平衡运行，主要在上部的吸收/解吸平衡。
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公开(公告)号：US06956125B2
公开(公告)日：2005-10-18
申请号：US09923629
申请日：2001-08-07
IPC分类号： C07J9/00
CPC分类号： C07J9/00
摘要： The invention relates to a process for the production of sterols from fatty acid distillation residues, characterized in that the partial glycerides are subjected to a first transesterification step under mild conditions and, after working up and the removal of impurities, the sterol esters are subjected to a second transesterification step under more extreme conditions.
摘要翻译： 本发明涉及从脂肪酸蒸馏残余物生产固醇的方法，其特征在于在温和条件下对部分甘油酯进行第一酯交换步骤，在加工和除去杂质后，使甾醇酯经受 在更极端条件下的第二个酯交换步骤。
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7.发明授权
公开(公告)号：US5473089A
公开(公告)日：1995-12-05
申请号：US227846
申请日：1994-04-14
申请人： Bernhard Gutsche , Timothy J. Cassady , Lutz Jeromin , Gerhard Wollmann , Norman Milstein , Hans-Christian Raths
发明人： Bernhard Gutsche , Timothy J. Cassady , Lutz Jeromin , Gerhard Wollmann , Norman Milstein , Hans-Christian Raths
IPC分类号： C07C303/32 , C07C309/12 , C07B45/00
CPC分类号： C07C303/32
摘要： Ammonium fatty acid hydroxyalkanesulfonates are made by a process in which (a) ammonium hydroxyalkanesulfonate corresponding to general formula (I):HO--(C.sub.n H.sub.2n)--SO.sub.3 NH.sub.4 (I)wherein n=2 to 4, is subjected to the esterification reaction with a fatty acid corresponding to the formula (II)R--COOH (II)wherein RCO is an aliphatic, linear or branched acyl radical containing 6 to 18 carbon atoms, in the presence of an esterification catalyst, characterized in that (a) before the esterification reaction, the starting compounds corresponding to formulae (I) and (II) are dried at a temperature of 120.degree. C. to 160.degree. C. and under a pressure of 100 to 700 mbar; (b) the esterification reaction is carried out at a temperature above 160.degree. C. to 195.degree. C. and under a pressure of 250 mbar to atmospheric pressure; (c) water of solution and water of reaction formed are directly removed from the reaction mixture; (d) the catalyst is neutralized with a base on completion of the reaction.
摘要翻译： 脂肪酸羟基烷基磺酸铵通过以下方法制备：（a）对应于通式（I）的羟基链烷磺酸铵：其中n = 2至4的HO-（CnH2n）-SO3NH4（I）与脂肪进行酯化反应 对应于式（II）R-COOH（II）的酸，其中RCO是含有6至18个碳原子的脂族，直链或支链酰基，在酯化催化剂存在下，其特征在于（a）酯化反应 对应于式（I）和（II）的起始化合物在120℃至160℃的温度和100至700毫巴的压力下干燥; （b）酯化反应在160℃至195℃和250毫巴至大气压的压力下进行; （c）直接从反应混合物中除去所形成反应的溶液和水; （d）催化剂在反应完成时用碱中和。
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公开(公告)号：US5254722A
公开(公告)日：1993-10-19
申请号：US195995
申请日：1988-05-19
申请人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
发明人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
IPC分类号： C07C67/03 , B01J27/232 , C07B61/00 , C07C69/18 , C07C69/30
CPC分类号： C07C67/03
摘要： A process for the production of triglycerides of C.sub.1 -C.sub.4 alkyl esters of C.sub.6 -C.sub.22 fatty acids:a) where dry sodium carbonate catalyst is dissolved in glycerol and mixed with a molar excess of preferably the methyl ester of C.sub.6 -C.sub.22 fatty acid at a temperature between about 150.degree. C. and 250.degree. C. at less than atmospheric pressure and under substantially anhydrous conditions to produce an initial reaction mixture containing the corresponding triglycerides of said fatty acids, and partially reacted glycerol with unreacted hydroxyl groups (OH values 10-40),b) thereafter, a portion of the initial reaction mixture is reacted with additional C.sub.1 -C.sub.4 alkyl ester of C.sub.6 -C.sub.22 fatty acid under conditions to achieve substantially full conversion of said unreacted hydroxyl groups (OH values of 5 or less), andc) a product containing the corresponding triglycerides of said fatty acids is separated from unreacted alkyl ester and from the sodium carbonate catalyst. Improved light colored triglyceride products are achieved and can be separated readily from the sodium carbonate catalyst by filtration.
摘要翻译： 制备C 6 -C 22脂肪酸的C 1 -C 4烷基酯的甘油三酸酯的方法：a）其中将干燥的碳酸钠催化剂溶解在甘油中，并与摩尔过量的优选C6-C22脂肪酸的甲酯在 温度在约150℃至250℃之间，低于大气压和基本无水条件下，以产生含有所述脂肪酸的相应甘油三酸酯和部分反应的甘油与未反应的羟基的初始反应混合物（OH值10- 40），b）此后，一部分初始反应混合物与另外的C 6 -C 22脂肪酸的C 1 -C 4烷基酯在使所述未反应的羟基基本上完全转化（OH值为5以下）的条件下反应， 和c）含有所述脂肪酸的相应甘油三酯的产物与未反应的烷基酯和碳酸钠催化剂分离。 实现了改进的浅色甘油三酸酯产物，并且可以通过过滤容易地与碳酸钠催化剂分离。
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9.发明授权
公开(公告)号：US6093844A
公开(公告)日：2000-07-25
申请号：US142783
申请日：1998-09-15
摘要： Proposed is a method of producing alkaline-earth salts of aliphatic .beta.-keto compounds by reacting alkaline-earth hydroxides with aliphatic .beta.-ketoesters and/or .beta.-diketones in the absence of solvent to give the corresponding alkaline-earth salts. The .beta.-keto compound is added in portions to the powdered alkaline-earth hydroxide and the reaction mixture subsequently dried. Good yields are obtained of a fine-grained, light colored product.
摘要翻译： PCT No.PCT / EP97 / 01156 Sec。 371日期：1998年9月15日 102（e）1998年9月15日PCT 1997年3月7日PCT PCT。 公开号WO97 / 34859 日期1997年9月25日提出的方法是在不存在溶剂的情况下使碱土金属氢氧化物与脂族β-酮酯和/或β-二酮反应生成脂肪族β-酮化合物的碱土金属盐，得到相应的碱土金属 盐。 将β-酮化合物分批加入粉状碱土金属氢氧化物中，然后将反应混合物干燥。 获得了细颗粒，浅色产品的良好产率。
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10.发明授权
公开(公告)号：US4698186A
公开(公告)日：1987-10-06
申请号：US821109
申请日：1986-01-21
申请人： Lutz Jeromin , Eberhard Peukert , Gerhard Wollmann
发明人： Lutz Jeromin , Eberhard Peukert , Gerhard Wollmann
摘要： A process for reducing the free fatty acid content of fats and oils by esterifying the free fatty acids with a lower monoalcohol in the presence of an acidic cation exchange resin as a solid esterification catalyst.
摘要翻译： 一种通过在酸性阳离子交换树脂作为固体酯化催化剂存在下，通过用较低一元醇酯化游离脂肪酸来降低脂肪和油的游离脂肪酸含量的方法。
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