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公开(公告)号：US20140083634A1
公开(公告)日：2014-03-27
申请号：US13977794
申请日：2011-12-30
IPC分类号： D21B1/12
摘要： Described herein is nanocellulose produced by introducing a mixture of cellulose based fiber raw material and water through a refining gap, having a width smaller than 0.1 mm. In the refining gap, the fiber raw material is subjected to processing forces varying in the direction of introducing said mixture, by means of refining zones provided in the gap one after each other in the feeding direction, whereby the refining surfaces differ in surface patterning and/or surface roughness. The mixture of fiber raw material and water is guided past the refining surfaces in the feeding direction to different locations in the refining zone by by-pass channels provided in the stator. The width of the refining gap is maintained by the combined effect of the feeding pressure of the mixture of fiber raw material and water fed into the refining gap and the axial force of the rotor.
摘要翻译： 本文描述的是通过将纤维素纤维原料和水的混合物通过宽度小于0.1mm的精炼间隙引入的纳米纤维。 在精炼间隙中，纤维原料在进料方向上通过在间隙中设置的精炼区，在引入所述混合物的方向上施加变化的加工力，由此精炼表面在表面图案化和 /或表面粗糙度。 纤维原料和水的混合物通过设置在定子中的旁通通道在进料方向上引导到精炼区中的不同位置。 精炼间隙的宽度通过纤维原料和进料到精炼间隙的水的混合物的进料压力和转子的轴向力的组合效应来保持。
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公开(公告)号：US08945346B2
公开(公告)日：2015-02-03
申请号：US13977794
申请日：2011-12-30
摘要： Described herein is nanocellulose produced by introducing a mixture of cellulose based fiber raw material and water through a refining gap, having a width smaller than 0.1 mm. In the refining gap, the fiber raw material is subjected to processing forces varying in the direction of introducing said mixture, by means of refining zones provided in the gap one after each other in the feeding direction, whereby the refining surfaces differ in surface patterning and/or surface roughness. The mixture of fiber raw material and water is guided past the refining surfaces in the feeding direction to different locations in the refining zone by by-pass channels provided in the stator. The width of the refining gap is maintained by the combined effect of the feeding pressure of the mixture of fiber raw material and water fed into the refining gap and the axial force of the rotor.
摘要翻译： 本文描述的是通过将纤维素纤维原料和水的混合物通过宽度小于0.1mm的精炼间隙引入的纳米纤维。 在精炼间隙中，纤维原料在进料方向上通过在间隙中设置的精炼区，在引入所述混合物的方向上施加变化的加工力，由此精炼表面在表面图案化和 /或表面粗糙度。 纤维原料和水的混合物通过设置在定子中的旁通通道在进料方向上引导到精炼区中的不同位置。 精炼间隙的宽度通过纤维原料和进料到精炼间隙的水的混合物的进料压力和转子的轴向力的组合效应来保持。
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3.发明申请公开(公告)号：US20150057442A1
公开(公告)日：2015-02-26
申请号：US14128947
申请日：2012-06-20
申请人： Tomas Björkqvist , Sirkka Gustafsson , Timo Koskinen , Markus Nuopponen , Annikki Vahniäinen , Antti Fredrikson
发明人： Tomas Björkqvist , Helmer Gustafsson , Timo Koskinen , Markus Nuopponen , Annikki Vehniäinen , Antti Fredrikson
CPC分类号： D21D1/20 , B02C19/0056 , C08B15/00 , D21D1/306
摘要： In a method for manufacturing fibril cellulose, cellulose based fibre raw material is processed mechanically in a refining gap for separating fibrils. The fibres to be refined are subjected to the action of a surface roughness Ra provided by grits elevated from a refining surface delimiting the refining gap, said surface roughness being lower than 3 μm, advantageously lower than 2 μm. The refining surface is formed by spraying grits and binder onto a substrate.
摘要翻译： 在原纤维纤维素的制造方法中，纤维素纤维原料在用于分离原纤维的精制间隙中进行机械加工。 待精制的纤维经受限定精炼间隙的精炼表面升高的砂粒提供的表面粗糙度Ra的作用，所述表面粗糙度低于3μm，有利地低于2μm。 精磨表面通过将砂粒和粘合剂喷射到基材上而形成。
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4.发明授权Method for processing nanofibrillar cellulose and product obtained by the method 有权纳米纤维素纤维素加工方法及其制备方法公开(公告)号：US09469696B2
公开(公告)日：2016-10-18
申请号：US13984550
申请日：2012-02-08
CPC分类号： C08B15/04 , B01J13/0069 , D01D5/06 , D01F2/00 , D21H11/18
摘要： The invention relates to a method for processing an aqueous gel of nanofibrillar cellulose by removing water from the aqueous gel by means of an organic solvent miscible with water. In the method: aqueous gel is introduced into a volume of organic solvent miscible with water in a controlled manner so that the aqueous gel is kept as a separate phase and forms discrete physical entities containing the nanofibrillar cellulose within the phase; water is changed with the organic solvent in said discrete physical entities of nanofibrillar cellulose; and the physical entities are separated from the volume of organic solvent.
摘要翻译： 本发明涉及通过借助与水混溶的有机溶剂从水凝胶中除去水来处理纳米纤丝纤维素水凝胶的方法。 在该方法中：将水性凝胶以受控的方式引入与水混溶的体积的有机溶剂中，使得水性凝胶保持为分离相，并在相内形成含有纳米纤维素纤维素的离散物理实体; 在纳米纤维素纤维素的离散物理实体中，水与有机溶剂发生变化; 并且物理实体与有机溶剂的体积分离。
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5.发明授权Method for catalytic oxidation of cellulose and method for making a cellulose product 有权纤维素的催化氧化方法及制备纤维素产品的方法公开(公告)号：US09410285B2
公开(公告)日：2016-08-09
申请号：US14124520
申请日：2012-06-08
摘要： In a method for catalytic oxidation of cellulose a heterocyclic nitroxyl radical is used as catalyst, hypochlorite is used as main oxidant acting as oxygen source, and a tertiary amine or chlorine dioxide as an activator of the heterocyclic nitroxyl radical.
摘要翻译： 在纤维素的催化氧化方法中，使用杂环硝酰自由基作为催化剂，次氯酸盐用作作为氧源的主要氧化剂，叔胺或二氧化氯作为杂环硝酰基的活化剂。
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6.发明申请METHOD FOR CATALYTIC OXIDATION OF CELLULOSE AND METHOD FOR MAKING A CELLULOSE PRODUCT 有权纤维素催化氧化方法及制备纤维素产品的方法公开(公告)号：US20140110070A1
公开(公告)日：2014-04-24
申请号：US14124520
申请日：2012-06-08
IPC分类号： D21C3/00
摘要： In a method for catalytic oxidation of cellulose a heterocyclic nitroxyl radical is used as catalyst, hypochlorite is used as main oxidant acting as oxygen source, and a tertiary amine or chlorine dioxide as an activator of the heterocyclic nitroxyl radical.
摘要翻译： 在纤维素的催化氧化方法中，使用杂环硝酰自由基作为催化剂，次氯酸盐用作作为氧源的主要氧化剂，叔胺或二氧化氯作为杂环硝酰基的活化剂。
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公开(公告)号：US20140374045A1
公开(公告)日：2014-12-25
申请号：US14376875
申请日：2013-02-11
申请人： Markus Nuopponen , Monika Osterberg , Janne Laine , Jaakko Pere
发明人： Markus Nuopponen , Monika Osterberg , Janne Laine , Jaakko Pere
CPC分类号： D21B1/063 , D21B1/16 , D21C3/04 , D21C3/26 , D21C9/007 , D21C9/02 , D21C9/18 , D21H11/10 , D21H11/16 , D21H11/18 , D21H17/65 , D21H17/66
摘要： A Method of pretreating native cellulose pulp in the manufacture of nanofibrillated cellulose, and a nanofibrillated cellulose product obtainable by the method.
摘要翻译： 一种在制造纳米纤维素纤维素中预处理天然纤维素纸浆的方法，以及通过该方法获得的纳米纤维素纤维素产品。
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公开(公告)号：US20140114059A1
公开(公告)日：2014-04-24
申请号：US14126481
申请日：2012-06-13
申请人： Juha Tamper , Markus Nuopponen , Harri Kosonen
发明人： Juha Tamper , Markus Nuopponen , Harri Kosonen
IPC分类号： C08B37/00
CPC分类号： C08B37/0003 , C08B1/08 , C08B11/12 , C08L2205/16 , D21C9/004 , D21C9/005 , D21C9/007 , D21H11/18 , D21H11/20
摘要： A method for manufacturing cellulosic material includes: introducing cellulose fibers as cellulosic raw material to a system, conveying the cellulose fibers to an extruder comprising a mixing part and/or a refining part, dosing at least one chemical to the system before the extruder and/or in the extruder and performing a reaction between the cellulose fibers and the chemical(s) at least partly in the extruder, wherein the reaction is performed at a consistency of at least 40%, and/or dosing at least one chemical to the system before the extruder and/or in the extruder and mixing the cellulose fibers and the chemical(s) in the mixing part of the extruder, wherein the mixing step is performed at a consistency of at least 40%, and/or refining the introduced cellulose fibers at least partly in the refining part of the extruder, wherein the refining step is performed at a consistency of at least 5%.
摘要翻译： 制造纤维素材料的方法包括：将纤维素纤维作为纤维素原料引入系统，将纤维素纤维输送到包含混合部分和/或精炼部分的挤出机中，在挤出机之前向系统中加入至少一种化学品和/ 或在挤出机中，并且至少部分地在挤出机中进行纤维素纤维和化学品之间的反应，其中反应以至少40％的稠度和/或向系统给药至少一种化学品进行 在挤出机之前和/或在挤出机中并将纤维素纤维和化学品混合在挤出机的混合部分中，其中混合步骤以至少40％的稠度进行，和/或精制所引入的纤维素 纤维至少部分地在挤出机的精炼部分中，其中精炼步骤以至少5％的稠度进行。
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9.发明申请METHOD FOR MANUFACTURING NANOFIBRILLATED CELLULOSE PULP AND USE OF THE PULP IN PAPER MANUFACTURING OR IN NANOFIBRILLATED CELLULOSE COMPOSITES 审中-公开用于制造纳米纤维素浆的方法和纸浆制造中或在纳米纤维素复合材料中使用纸浆的方法公开(公告)号：US20130000855A1
公开(公告)日：2013-01-03
申请号：US13511956
申请日：2010-11-05
摘要： A method for manufacturing pulp. The manufactured pulp includes at least 30 w-% nanofibrillated cellulose material measured from the dried pulp. A raw material is introduced to a system. The raw material includes cellulose. At least one type of an optical brightening agent is dosed as a refining additive to the system. The raw material is refined in the presence of the dosed optical brightening agent in at least one pre-refining stage or fibrillation stage to form fibrillar cellulose material.
摘要翻译： 纸浆的制造方法。 所制造的纸浆包括从干燥的纸浆测量的至少30w-纳米纤维素材料。 将原材料引入系统。 原料包括纤维素。 将至少一种类型的荧光增白剂作为精制添加剂配制到体系中。 在至少一个预精制阶段或原纤维阶段中，在定量的荧光增白剂的存在下将原料精制，以形成纤维状纤维素材料。
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公开(公告)号：US20140083416A1
公开(公告)日：2014-03-27
申请号：US14006477
申请日：2012-03-21
申请人： Markus Nuopponen , Anne Meriluoto , Eero Kontturi
发明人： Markus Nuopponen , Anne Meriluoto , Eero Kontturi
IPC分类号： C08B15/00
摘要： The invention relates to a process for preparing micro- and nanocrystailine cellulose material in the presence of an acid. More specifically, the invention relates to a process, in which the cellulose material is hydrolyzed in the presence of an acid in the gas phase while the moisture content of cellulose is between 1% and 80%, the cellulose material is surface-modified, and mech anically treated in order to obtain micro- and/or nanocrystailine cellulose material. The invention also relates to a cellulose product prepared by the said process and the use thereof in food and liquid crystal applications as well as in optical, cosmetic and medical applications.
摘要翻译： 本发明涉及一种在酸存在下制备微米和纳米骨架纤维素材料的方法。 更具体地，本发明涉及一种方法，其中纤维素材料在气相存在下在酸的存在下水解，而纤维素的水分含量在1％至80％之间，纤维素材料被表面改性，并且 机械处理以获得微米和/或纳米骨架纤维素材料。 本发明还涉及通过所述方法制备的纤维素产品及其在食品和液晶应用以及光学，化妆品和医学应用中的应用。
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