Process for preparing polyoxyalkylene glycol ethers using alkoxylated alkylphenol-aldehyde resins as demulsifiers
    5.
    发明申请
    Process for preparing polyoxyalkylene glycol ethers using alkoxylated alkylphenol-aldehyde resins as demulsifiers 审中-公开
    使用烷氧基化烷基酚醛树脂作为破乳剂制备聚氧亚烷基二醇醚的方法

    公开(公告)号:US20080045666A1

    公开(公告)日:2008-02-21

    申请号:US11893900

    申请日:2007-08-17

    IPC分类号: C08F8/02

    CPC分类号: C08G65/329

    摘要: The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and a compound of the formula 1 in which R2 is a straight-chain or branched C1- to C20-alkyl radical, p is from 1 to 75, X is one 1,2-alkylene group or different 1,2-alkylene groups having from 2 to 4 carbon atoms, and k is from 1 to 200 to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.

    摘要翻译: 本发明提供了通过使烷氧基化物与烷基化剂反应制备聚氧亚烷基二醇单醚和/或二醚的方法,该方法包括加入水和其中R 2为直链的式1化合物 或支链C 1至C 20 - 烷基,p为1至75,X为一个1,2-亚烷基或不同的1,2-亚烷基 具有2至4个碳原子,并且k对于形成的醇盐,烷基化剂和聚氧亚烷基二醇醚的混合物为1至200。

    Process for preparing polyoxyalkylene glycol ethers using alkoxylated oligo- or polyethyleneimines as demulsifiers
    6.
    发明申请
    Process for preparing polyoxyalkylene glycol ethers using alkoxylated oligo- or polyethyleneimines as demulsifiers 审中-公开
    使用烷氧基化的寡聚或聚乙烯亚胺作为破乳剂制备聚氧亚烷基二醇醚的方法

    公开(公告)号:US20080045652A1

    公开(公告)日:2008-02-21

    申请号:US11893923

    申请日:2007-08-17

    IPC分类号: C08G67/00

    CPC分类号: C08G65/329

    摘要: The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and oligo- or polyethyleneimines which have been alkoxylated with from 1 to 100 C2- to C4-alkylene oxide groups or a mixture of such alkylene oxide groups per free NH group to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.

    摘要翻译: 本发明提供了通过使烷氧基化物与烷基化剂反应来制备聚氧亚烷基二醇单醚和/或二醚的方法,该方法包括加入水和低聚或聚乙烯亚胺,所述低聚或聚乙烯亚胺在1至100℃2 - 至C 4 - 亚烷基氧基或每个游离NH基团的这种烯化氧基团的混合物与形成的醇盐,烷基化剂和聚氧亚烷基二醇醚的混合物。

    Process for preparing polyoxyalkylene glycol ethers using block polymers as demulsifiers
    7.
    发明申请
    Process for preparing polyoxyalkylene glycol ethers using block polymers as demulsifiers 审中-公开
    使用嵌段聚合物作为破乳剂制备聚氧亚烷基二醇醚的方法

    公开(公告)号:US20080045667A1

    公开(公告)日:2008-02-21

    申请号:US11894014

    申请日:2007-08-17

    IPC分类号: C08F8/02

    CPC分类号: C08G65/329 C08G65/2696

    摘要: The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and block polymers which are obtainable from a compound which comprises from 1 to 30 carbon atoms and from 1 to 25 hydroxyl groups, amino groups or both by its blockwise alkoxylation with at least 2 different blocks of in each case from 1 to 200 mol of C2- to C4-alkylene oxide to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.

    摘要翻译: 本发明提供了一种通过使烷氧基化物与烷基化剂反应来制备聚氧亚烷基二醇单醚和/或二醚的方法,该方法包括加入水和嵌段聚合物,该聚合物可从含有1至30个碳原子的化合物和1至25个羟基 基团,氨基或两者通过其阻断性烷氧基化与至少2个不同的嵌段在每种情况下为1至200摩尔C 2至C 4 - 亚烷基氧基至 形成的醇盐,烷化剂和聚氧亚烷基二醇醚的混合物。

    Demulsifiers
    9.
    发明申请
    Demulsifiers 审中-公开
    破乳剂

    公开(公告)号:US20050203193A1

    公开(公告)日:2005-09-15

    申请号:US10515897

    申请日:2003-05-16

    摘要: The invention relates to polymers that can be obtained by: A) reacting an epoxidized ester, which is selected from one or more unsaturated fatty acids having 8 to 26 C atoms and a polyol having 2 to 6 OH groups, with a monoamine, diamine or polyamine; B) alkoxylating the polyamine obtained hereby with a C2 to C4 alkylene oxide in molar excess so that the average degree of alkoxylation per OH group ranges from 1 to 100. The polymers have a numerical average molecular weight ranging from 500 to 100,000 g/mol. The invention also relates to the use of these polymers in quantities ranging from 0.0001 to 5% by weight with regard to the oil as demulsifiers for oil-in-water emulsions.

    摘要翻译: 本发明涉及可以通过以下方法获得的聚合物:A)使选自具有8至26个C原子的一种或多种不饱和脂肪酸和具有2-6个OH基团的多元醇的环氧化酯与单胺,二胺或 多胺 B)以C摩尔过量的方式将C 2 N 2 C 2 C 2 O 3烷氧基化,使得每OH基团的平均烷氧基化度在1至100范围内。 聚合物的数均分子量为500〜100,000g / mol。 本发明还涉及这些聚合物在0.0001至5重量%范围内的用途,作为油包水乳液的破乳剂。

    Alkoxylation catalyst
    10.
    发明授权
    Alkoxylation catalyst 失效
    烷氧基化催化剂

    公开(公告)号:US06365541B1

    公开(公告)日:2002-04-02

    申请号:US09257630

    申请日:1999-02-25

    IPC分类号: B01J3100

    摘要: An alkoxylation catalyst is prepared by a) reaction of one mol of a dicarboxylic acid with from 1.5 to 8 mol of an alkoxylated alcohol to form the corresponding dicarboxylic monoester, b) formation of an alkaline earth metal salt of the dicarboxylic monoester by addition of water and from 0.45 to 0.55 mol of a basic alkaline earth metal compound per mol of dicarboxylic acid originally used, c) partial neutralization of the alkaline earth metal salt by addition of from 0.25 to 0.7 mol of H2SO4 per mol of basic alkaline earth metal compound originally used and d) removal of the water present at a temperature of less than 100° C. The catalyst prepared in this way makes it possible to prepare colorless alkoxylates having a narrow homologue distribution.

    摘要翻译: 通过a)使一摩尔二羧酸与1.5至8摩尔烷氧基化醇反应形成相应的二羧酸单酯来制备烷氧基化催化剂,b)通过加入水形成二羧酸单酯的碱土金属盐;和 原始使用的每摩尔二羧酸为0.45〜0.55摩尔的碱土金属化合物,c)通过加入0.25〜0.7摩尔H 2 SO 4 /摩尔碱性碱土金属化合物,最初使用的部分中和 和d)去除在低于100℃的温度下存在的水。以这种方式制备的催化剂使得可以制备具有窄的同系物分布的无色烷氧基化物。