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    Process for the production of unsymmetrical tert-dialkyl ethers
    1.
    发明授权
    Process for the production of unsymmetrical tert-dialkyl ethers 失效
    用于生产不对称叔二烷基醚的方法

    公开(公告)号：US5364980A

    公开(公告)日：1994-11-15

    申请号：US816318

    申请日：1991-12-30

    Applicant: Michael C. Kerby ,  David E. W. Vaughan

    Inventor： Michael C. Kerby ,  David E. W. Vaughan

    IPC: B01J29/04 ,  C07C41/09 ,  C07C43/04

    CPC classification number: B01J29/049 ,  C07C41/09

    Abstract: A method for preparing unsymmetrical dialkyl ethers and derivatives thereof. The ethers are prepared by reacting a C.sub.1 to C.sub.3 aliphatic alcohol with a tertiary alcohol in the presence of a novel catalyst comprised of a transition metal pillared interlayered clay having generally separated layers wherein the interlayer distances are substantially greater than a precursor of the same but non-separated clay and wherein the product includes multimetallic pillars comprised of a cationic polymeric complex of the formula:Al.sup.iv (Al.sub.12-x M.sub.x).sup.vi O.sub.4 (OH).sub.24.sup.a+where x is a number from 1 to 6; a depends on the selection of M and N; N is selected from Al.sup.3+, Si.sup.4+, Ga.sup.3+, Ge.sup.4+, As.sup.5+, P.sup.5+, Cr.sup.3+, Fe.sup.3+, V.sup.5+, Ru.sup.3+, Ru.sup.4+, N.sup.3+ ; and M is selected from a metal from Groups 5B, 6B, 7B and 8 of the 4th, 5th and 6th Periods of the Periodic Table of the Elements.

    Abstract translation: 一种制备不对称二烷基醚及其衍生物的方法。 醚通过在具有通常分离的层的过渡金属柱状中间层粘土的新型催化剂存在下使C 1至C 3脂族醇与叔醇反应制备，其中层间距离基本上大于相同但不相同的前体 分离的粘土，并且其中所述产品包括由以下式的阳离子聚合物复合物组成的多金属柱：Aliv（Al12-xMx）viO4（OH）24a +，其中x为1至6的数; a取决于M和N的选择; N选自Al3 +，Si4 +，Ga3 +，Ge4 +，As5 +，P5 +，Cr3 +，Fe3 +，V5 +，Ru3 +，Ru4 +，N3 +; 并且M选自元素周期表的第4,5,6和8族的5B，6B，7B和8族的金属。

    Method for the synthesis of molecular sieves
    2.
    发明授权
    Method for the synthesis of molecular sieves 有权

    公开(公告)号：US06540970B1

    公开(公告)日：2003-04-01

    申请号：US09705352

    申请日：2000-11-03

    Applicant: Karl G. Strohmaier ,  David E. W. Vaughan

    Inventor： Karl G. Strohmaier ,  David E. W. Vaughan

    IPC: C01B3706

    CPC classification number: B01J29/85 ,  B01J29/84 ,  C01B37/06 ,  C01B37/065 ,  C01B37/08 ,  Y10S423/30

    Abstract: The present invention provides a method for the synthesis of MeAPO molecular sieves which includes the following steps: providing a source of alumina, a source of phosphorus, water, and a template suitable for forming a MeAPO molecular sieve; providing a source of metal (Me) including metal particles, the metal particles measuring, in their largest dimension, equal to or less than five nanometers; providing a water soluble organic solvent capable of solubilizing the source of metal; forming a synthesis mixture from the source of alumina, the source of phosphorus, the water, the template, the source of metal, and the solvent; and forming a MeAPO molecular sieve from the synthesis mixture.

    Pillared metakandite clay compositions as sorbents, catalysts and ceramic and refractory precursors
    5.
    发明授权
    Pillared metakandite clay compositions as sorbents, catalysts and ceramic and refractory precursors 失效
    作为吸附剂，催化剂和陶瓷和耐火前体的柱状赤铁矿粘土组合物

    公开(公告)号：US5416051A

    公开(公告)日：1995-05-16

    申请号：US985992

    申请日：1992-12-04

    Applicant: David E. W. Vaughan

    Inventor： David E. W. Vaughan

    IPC: B01J20/12 ,  B01J21/16 ,  B01J29/04

    CPC classification number: B01J29/049 ,  B01J20/12

    Abstract: This present invention includes a composition of matter made up of a kandite clay which has been treated with large molecules containing multi-atom metallic or semi-metallic species and heated to produce pillars within the clay which are located generally between the clay's layers. The pillared kandite composition is useful as a catalyst support, sorbent, or ion exchanger.The present invention also includes a process for producing the pillared kandite composition comprises mixing the finely divided clay in an aqueous solution with the pillaring medium and heating the resulting composition at a temperature high enough to decompose the added compound.

    Abstract translation: 本发明包括由已经用含有多原子金属或半金属物质的大分子处理并被加热以在粘土中产生通常位于粘土层之间的柱状物的康体土粘土组成的物质组合物。 柱状的Kandite组合物可用作催化剂载体，吸附剂或离子交换剂。 本发明还包括一种生产柱状水泥石组合物的方法，包括将水溶液中的细碎粘土与支撑介质混合，并在足够高的温度下加热所得组合物以分解所添加的化合物。

    Multimetallic pillared interlayered clay products and processes of making them
    10.
    发明授权
    Multimetallic pillared interlayered clay products and processes of making them 失效
    多金属支柱夹层粘土产品及其制造工艺

    公开(公告)号：US4666877A

    公开(公告)日：1987-05-19

    申请号：US756508

    申请日：1985-07-19

    Applicant: David E. W. Vaughan

    Inventor： David E. W. Vaughan

    IPC: B01J20/12 ,  B01J20/16 ,  B01J21/16 ,  B01J29/04 ,  C01B33/26 ,  C01B39/00

    CPC classification number: B01J29/049 ,  B01J20/16

    Abstract: This invention is a composition of matter made up of an expanded smectite clay having multimetallic pillars separating the clay layers. The expanded clay may be used as a shape selective catalyst, catalyst support, or as an adsorbent material. More particularly, this invention relates to expanded smectite clays wherein the pillars are made up of aluminum and one or more transition metals.

    Abstract translation: 本发明是由具有分离粘土层的多金属柱的膨胀蒙脱石粘土组成的物质组合物。 膨胀粘土可以用作形状选择催化剂，催化剂载体或作为吸附材料。 更具体地说，本发明涉及膨胀蒙脱石粘土，其中柱由铝和一种或多种过渡金属组成。

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