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    ANTIREFLECTIVE SILICA COATINGS BASED ON SOL-GEL TECHNIQUE WITH CONTROLLABLE PORE SIZE, DENSITY, AND DISTRIBUTION BY MANIPULATION OF INTER-PARTICLE INTERACTIONS USING PRE-FUNCTIONALIZED PARTICLES AND ADDITIVES
    5.
    发明申请
    ANTIREFLECTIVE SILICA COATINGS BASED ON SOL-GEL TECHNIQUE WITH CONTROLLABLE PORE SIZE, DENSITY, AND DISTRIBUTION BY MANIPULATION OF INTER-PARTICLE INTERACTIONS USING PRE-FUNCTIONALIZED PARTICLES AND ADDITIVES 审中-公开
    使用预功能颗粒和添加剂处理颗粒间相互作用的基于SOL-GEL技术的可控硅胶涂层，具有可控的孔径，密度和分布

    公开(公告)号：US20130034653A1

    公开(公告)日：2013-02-07

    申请号：US13195151

    申请日：2011-08-01

    申请人： Nitin Kumar ,  Nikhil D. Kalyankar ,  Zhi-Wen Sun

    发明人： Nitin Kumar ,  Nikhil D. Kalyankar ,  Zhi-Wen Sun

    IPC分类号： B05D5/06 ,  G02B5/22

    CPC分类号： C09D183/04 ,  B05D5/06 ,  C03C17/009 ,  C03C2217/425 ,  C03C2217/732 ,  C03C2218/113 ,  C08L83/04 ,  C23C18/00

    摘要： Methods and compositions for forming durable porous low refractive index coatings on substrates are provided. In one embodiment, a method of forming a porous coating on a substrate is provided. The method comprises coating a substrate with a sol-formulation comprising a silane-based binder, silica-based nanoparticles, and an inter-particle interaction modifier for regulating interactions between the silica-based nanoparticles and annealing the coated substrate. Porous coatings formed according to the embodiments described herein demonstrate good optical properties (e.g., a low refractive index) while maintaining good mechanical durability due to the presence of the inter-particle interaction modifier. The inter-particle interaction modifier increases the strength of the particle network countering capillary forces produced during drying to maintain the porosity structure.

    摘要翻译： 提供了在基底上形成耐久的多孔低折射率涂层的方法和组合物。 在一个实施方案中，提供了在基材上形成多孔涂层的方法。 该方法包括用包含硅烷基粘合剂，二氧化硅基纳米颗粒和颗粒间相互作用改性剂的溶胶制剂涂覆基材，以调节二氧化硅基纳米颗粒之间的相互作用并退火涂覆的基材。 根据本文所述的实施方案形成的多孔涂层由于存在颗粒间相互作用改性剂而保持良好的机械耐久性，表现出良好的光学性能（例如，低折射率）。 颗粒间相互作用调节剂增加了颗粒网络抵抗干燥期间产生的毛细管力的强度，以保持孔隙结构。

    Sol-gel based antireflective coatings using alkyltrialkoxysilane binders having low refractive index and high durability
    7.
    发明授权
    Sol-gel based antireflective coatings using alkyltrialkoxysilane binders having low refractive index and high durability 有权
    使用具有低折射率和高耐久性的烷基三烷氧基硅烷粘合剂的溶胶 - 凝胶基抗反射涂层

    公开(公告)号：US09109121B2

    公开(公告)日：2015-08-18

    申请号：US13273007

    申请日：2011-10-13

    申请人： Nikhil D. Kalyankar ,  Zhi-Wen Sun ,  Jeroen Van Duren ,  Mark Lewis ,  Liang Liang

    发明人： Nikhil D. Kalyankar ,  Zhi-Wen Sun ,  Jeroen Van Duren ,  Mark Lewis ,  Liang Liang

    IPC分类号： C03C17/00 ,  C03C17/22 ,  C03C17/30 ,  C09D1/00 ,  C09D5/00 ,  C09D7/12 ,  G02B1/115 ,  C08K3/36

    CPC分类号： C09D1/00 ,  C03C17/008 ,  C03C17/22 ,  C03C17/30 ,  C08K3/36 ,  C09D5/006 ,  C09D7/61 ,  C09D7/67 ,  G02B1/115

    摘要： Methods and compositions for forming porous low refractive index coatings on substrates are provided. The method comprises coating a substrate with a sol-formulation comprising silica based nanoparticles and an alkyltrialkoxysilane based binder. Use of the alkyltrialkoxysilane based binder results in a porous low refractive index coating having bimodal pore distribution including mesopores formed from particle packing and micropores formed from the burning off of organics including the alkyl chain covalently bonded to the silicon. The mass ratio of binder to particles may vary from 0.1 to 20. Porous coatings formed according to the embodiments described herein demonstrate good optical properties (e.g. a low refractive index) while maintaining good mechanical durability due to the presence of a high amount of binder and a close pore structure.

    摘要翻译： 提供了在基底上形成多孔低折射率涂层的方法和组合物。 该方法包括用包含二氧化硅基纳米颗粒和烷基三烷氧基硅烷基粘合剂的溶胶制剂涂覆基材。 使用烷基三烷氧基硅烷基粘合剂导致具有双峰孔分布的多孔低折射率涂层，包括由颗粒填充形成的介孔和由共价键合到硅上的烷基链的有机物燃烧形成的微孔。 粘合剂与颗粒的质量比可以在0.1至20之间变化。根据本文所述实施方案形成的多孔涂层表现出良好的光学性能（例如低折射率），同时由于存在大量粘合剂而保持良好的机械耐久性， 密闭孔结构。

    SOL-GEL BASED ANTIREFLECTIVE COATINGS USING ALKYLTRIALKOXYSILANE BINDERS HAVING LOW REFRACTIVE INDEX AND HIGH DURABILITY
    8.
    发明申请
    SOL-GEL BASED ANTIREFLECTIVE COATINGS USING ALKYLTRIALKOXYSILANE BINDERS HAVING LOW REFRACTIVE INDEX AND HIGH DURABILITY 有权
    使用具有低折射率和高耐久性的烷基酮树脂粘合剂的基于溶胶凝胶的抗反射涂层

    公开(公告)号：US20130095237A1

    公开(公告)日：2013-04-18

    申请号：US13273007

    申请日：2011-10-13

    申请人： Nikhil D. Kalyankar ,  Zhi-Wen Sun ,  Jeroen Van Duren ,  Mark Lewis ,  Liang Liang

    发明人： Nikhil D. Kalyankar ,  Zhi-Wen Sun ,  Jeroen Van Duren ,  Mark Lewis ,  Liang Liang

    IPC分类号： B05D5/06 ,  C09D7/12 ,  B82Y30/00

    CPC分类号： C09D1/00 ,  C03C17/008 ,  C03C17/22 ,  C03C17/30 ,  C08K3/36 ,  C09D5/006 ,  C09D7/61 ,  C09D7/67 ,  G02B1/115

    摘要： Methods and compositions for forming porous low refractive index coatings on substrates are provided. The method comprises coating a substrate with a sol-formulation comprising silica based nanoparticles and an alkyltrialkoxysilane based binder. Use of the alkyltrialkoxysilane based binder results in a porous low refractive index coating having bimodal pore distribution including mesopores formed from particle packing and micropores formed from the burning off of organics including the alkyl chain covalently bonded to the silicon. The mass ratio of binder to particles may vary from 0.1 to 20. Porous coatings formed according to the embodiments described herein demonstrate good optical properties (e.g. a low refractive index) while maintaining good mechanical durability due to the presence of a high amount of binder and a close pore structure.

    摘要翻译： 提供了在基底上形成多孔低折射率涂层的方法和组合物。 该方法包括用包含二氧化硅基纳米颗粒和烷基三烷氧基硅烷基粘合剂的溶胶制剂涂覆基材。 使用烷基三烷氧基硅烷基粘合剂导致具有双峰孔分布的多孔低折射率涂层，包括由颗粒填充形成的介孔和由共价键合到硅上的烷基链的有机物燃烧形成的微孔。 粘合剂与颗粒的质量比可以在0.1至20之间变化。根据本文所述实施方案形成的多孔涂层表现出良好的光学性能（例如低折射率），同时由于存在大量粘合剂而保持良好的机械耐久性， 密闭孔结构。

    SOL-GEL BASED ANTIREFLECTIVE COATINGS USING PARTICLE-BINDER APPROACH WITH HIGH DURABILITY, MOISTURE RESISTANCE, CLOSED PORE STRUCTURE AND CONTROLLABLE PORE SIZE
    9.
    发明申请
    SOL-GEL BASED ANTIREFLECTIVE COATINGS USING PARTICLE-BINDER APPROACH WITH HIGH DURABILITY, MOISTURE RESISTANCE, CLOSED PORE STRUCTURE AND CONTROLLABLE PORE SIZE 审中-公开
    使用具有高耐久性，耐水分性，封闭孔结构和可控内孔尺寸的颗粒粘合剂方法的基于溶胶凝胶的抗反射涂层

    公开(公告)号：US20130034722A1

    公开(公告)日：2013-02-07

    申请号：US13195119

    申请日：2011-08-01

    申请人： Nikhil D. Kalyankar ,  Nitin Kumar

    发明人： Nikhil D. Kalyankar ,  Nitin Kumar

    IPC分类号： B05D5/06 ,  G02B5/22

    CPC分类号： G02B1/11 ,  G02B2207/107 ,  G02B2207/109 ,  Y10T428/249984

    摘要： Durable porous low refractive index coatings, methods and compositions for forming the porous low refractive index coatings are provided. The method comprises coating a substrate with a sol formulation comprising a silane-based binder having one or more reactive groups and silica based nanoparticles and annealing the coated substrate. The silane-based binder comprises from about 30 wt. % to about 70 wt. % ash contribution in the total ash content of the sol formulation. Porous coatings formed according to the embodiments described herein demonstrate good optical properties (e.g., a low refractive index) while maintaining good mechanical durability due to the presence of a high amount of binder and a closed pore structure.

    摘要翻译： 提供耐久的多孔低折射率涂层，用于形成多孔低折射率涂层的方法和组合物。 该方法包括用包含具有一个或多个反应性基团的硅烷基粘合剂和基于二氧化硅的纳米颗粒的溶胶制剂涂覆基材并对涂覆的基材进行退火。 硅烷基粘合剂包含约30wt。 ％至约70wt。 灰分对溶胶配方总灰分的贡献。 根据本文所述的实施方案形成的多孔涂层表现出良好的光学性能（例如，低折射率），同时由于存在大量粘合剂和闭孔结构而保持良好的机械耐久性。

    SOL-GEL BASED FORMULATIONS AND METHODS FOR PREPARATION OF HYDROPHOBIC ULTRA LOW REFRACTIVE INDEX ANTI-REFLECTIVE COATINGS ON GLASS
    10.
    发明申请
    SOL-GEL BASED FORMULATIONS AND METHODS FOR PREPARATION OF HYDROPHOBIC ULTRA LOW REFRACTIVE INDEX ANTI-REFLECTIVE COATINGS ON GLASS 审中-公开
    基于溶胶凝胶的制剂和制备疏水性超低折射率玻璃反反应涂层的方法

    公开(公告)号：US20120237676A1

    公开(公告)日：2012-09-20

    申请号：US13046899

    申请日：2011-03-14

    申请人： Nikhil D. Kalyankar ,  Nitin Kumar

    发明人： Nikhil D. Kalyankar ,  Nitin Kumar

    IPC分类号： B05D5/00 ,  B05D3/00 ,  C09D7/12 ,  B05D3/02

    CPC分类号： C03C17/007 ,  C03C17/34 ,  C03C2217/425 ,  C03C2217/732 ,  C03C2218/113 ,  C03C2218/32 ,  C08K5/5403 ,  C08K5/5419 ,  C09D1/00 ,  C09D5/006 ,  C09D7/63

    摘要： Embodiments of the invention relate generally to methods and compositions for forming porous low refractive index coatings on substrates. In one embodiment, a method of forming a porous coating on a substrate is provided. The method comprises coating a substrate with a sol-gel composition comprising at least one self assembling molecular porogen and annealing the coated substrate to remove the at least one self assembling molecular porogen to form the porous coating. Use of the self assembling molecular porogens leads to the formation of stable pores with larger volume and an increased reduction in the refractive index of the coating. Further, the size and interconnectivity of the pores may be controlled via selection of the self assembling molecular porogens structure, the total porogen fraction, polarity of the molecule and solvent, and other physiochemical properties of the gel phase.

    摘要翻译： 本发明的实施方案一般涉及在基底上形成多孔低折射率涂层的方法和组合物。 在一个实施方案中，提供了在基材上形成多孔涂层的方法。 该方法包括用包含至少一种自组装分子致孔剂的溶胶 - 凝胶组合物涂覆底物并退火涂覆的基底以除去至少一个自组装分子致孔剂以形成多孔涂层。 使用自组装分子致孔剂导致形成具有较大体积的稳定孔，并且涂层的折射率降低。 此外，孔的尺寸和互连性可以通过选择自组装分子致孔剂结构，总致孔剂级分，分子和溶剂的极性以及凝胶相的其它物理化学性质来控制。