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    Process for a beta-phase nickel aluminide overlay coating
    3.
    发明授权
    Process for a beta-phase nickel aluminide overlay coating 有权
    一种β相镍铝覆盖涂层的工艺

    公开(公告)号：US07244467B2

    公开(公告)日：2007-07-17

    申请号：US10604368

    申请日：2003-07-15

    申请人： Theodore Robert Grossman ,  Ramgopal Darolia ,  Joseph David Rigney

    发明人： Theodore Robert Grossman ,  Ramgopal Darolia ,  Joseph David Rigney

    IPC分类号： C23C16/00

    CPC分类号： C23C14/5886 ,  C23C4/18 ,  C23C14/16 ,  C23C26/00 ,  C23C28/3215 ,  C23C28/345 ,  C23C28/3455

    摘要： A process for forming a beta-phase nickel aluminide (NiAl) overlay coating that is suitable for use as a bond coat for a thermal barrier coating (TBC). The overlay coating is deposited by a method that produces a generally columnar grain structure in which grains extend through the coating such that at least some grain boundaries are open at the coating surface. The coating is then peened with a particulate media, followed by heating the overlay coating to a temperature sufficient to cause the overlay coating to recrystallize and form new grain boundaries that are not open to the outer surface of the coating and significantly less susceptible to accelerated oxidation than the original grain boundaries. The particulate media is formed of a composition containing nickel and aluminum, such that an oxide scale that forms on the surface of the coating after the peening operation is substantially free of deleterious oxide compounds, notably iron-containing spinels.

    摘要翻译： 用于形成适合用作热障涂层（TBC）的粘合涂层的β-相镍铝化物（NiAl）覆盖涂层的方法。 覆盖涂层通过产生大致柱状晶粒结构的方法沉积，其中晶粒延伸穿过涂层，使得至少一些晶界在涂层表面开口。 然后用颗粒介质对涂层进行喷丸处理，然后将覆盖涂层加热至足以使覆盖涂层再结晶并形成不对涂层外表面开放的新晶粒边界，并显着降低易受加速氧化影响的温度 比原来的晶界。 颗粒介质由包含镍和铝的组合物形成，使得在喷丸操作之后在涂层表面上形成的氧化皮基本上不含有害氧化物化合物，特别是含铁尖晶石。

    Method for preventing the formation of secondary reaction zone in susceptible articles, and articles prepared by the method
    4.
    发明授权
    Method for preventing the formation of secondary reaction zone in susceptible articles, and articles prepared by the method 有权
    用于防止易感物品中二次反应区形成的方法，以及通过该方法制备的制品

    公开(公告)号：US06843861B2

    公开(公告)日：2005-01-18

    申请号：US10071129

    申请日：2002-02-08

    申请人： Theodore Robert Grossman ,  Ronald Gustav Rajala ,  Dwayne Edward Burnett ,  William Scott Walston ,  Wendy Howard Murpjy

    发明人： Theodore Robert Grossman ,  Ronald Gustav Rajala ,  Dwayne Edward Burnett ,  William Scott Walston ,  Wendy Howard Murpjy

    IPC分类号： C23C10/02 ,  C23C10/52 ,  C23C10/60 ,  F01D5/28 ,  C23C8/04 ,  B32B15/10 ,  B41M3/12

    CPC分类号： F01D5/288 ,  C23C10/02 ,  C23C10/52 ,  C23C10/60 ,  Y02T50/67 ,  Y10T428/1275

    摘要： A coated nickel-base superalloy article, which is otherwise susceptible to the formation of a secondary reaction zone, is prepared by furnishing a nickel-base superalloy article substrate having thereon an initial aluminum-containing coating comprising an initial-coating additive zone and an initial-coating diffusion zone. The article is susceptible to the formation of the secondary reaction zone if heated to an elevated SRZ reaction temperature for an SRZ reaction period of time. The formation of the secondary reaction zone is avoided by first removing the initial-coating additive zone and the initial-coating diffusion zone, and thereafter depositing a subsequent aluminum-containing coating onto the article substrate. The subsequent aluminum-containing coating includes a subsequent-coating additive zone and a subsequent-coating diffusion zone. The article substrate with the subsequent aluminum-containing coating is otherwise susceptible to the formation of the secondary reaction zone if heated to the elevated SRZ reaction temperature for the SRZ reaction period of time.

    摘要翻译： 通过提供其上具有初始含铝涂层的镍基超级合金制品基材来制备另外易于形成次级反应区的涂覆的镍基超合金制品，所述初始含铝涂层包含初始涂层添加区和初始涂层添加区 涂层扩散区。 如果在SRZ反应时间段内加热到升高的SRZ反应温度，则该制品易于形成次级反应区。 通过首先去除初始涂层添加剂区域和初始涂覆扩散区，然后将随后的含铝涂层沉积到制品基材上，避免二次反应区的形成。 随后的含铝涂层包括随后的涂层添加剂区域和随后的涂覆扩散区域。 如果加热到SRZ反应时间段的升高的SRZ反应温度，则具有随后的含铝涂层的制品基材否则易于形成次级反应区。

    Endurance of NiA1 coatings by controlling thermal spray processing variables
    5.
    发明授权
    Endurance of NiA1 coatings by controlling thermal spray processing variables 失效
    通过控制热喷涂处理变量，NiAl涂层的耐久性

    公开(公告)号：US06485792B1

    公开(公告)日：2002-11-26

    申请号：US09644491

    申请日：2000-08-23

    申请人： Richard John Grylls ,  Joseph David Rigney ,  Matthew David Saylor ,  Theodore Robert Grossman ,  Yuk-Chiu Lau

    发明人： Richard John Grylls ,  Joseph David Rigney ,  Matthew David Saylor ,  Theodore Robert Grossman ,  Yuk-Chiu Lau

    IPC分类号： C23C406

    CPC分类号： C23C4/18 ,  C23C4/08 ,  Y02T50/67

    摘要： A method for applying substantially stoichiometric NiAl to the surface of a superalloy substrate. These coatings are applied to substrates subjected to high temperatures and thermal cycling by providing a powder of the substantially stoichiometric material with the desired minor additions of rare earth elements, Cr or Zr. The coatings are applied by a thermal spray process utilizing hydrogen as a fuel while generating a highly reducing flame. The thermal spray method melts the powder and directs it onto the surface of the turbine component that is to be coated. The powder size is carefully controlled to prevent oxidation of the powder while providing a controlled surface finish. The surface roughness of the bond coat is further mechanically worked to a predetermined surface finish prior to application of the ceramic thermal barrier layer by a PVD method. Thermal barrier systems applied using these carefully controlled predetermined parameters provide outstanding resistance to TBC spallation under conditions of high cyclic stresses.

    摘要翻译： 将基本上化学计量的NiAl施加到超级合金基底的表面上的方法。 通过提供具有理想化学计量的材料的粉末和所需的稀土元素Cr或Zr的少量添加，将这些涂层施加到经受高温和热循环的基底上。 通过使用氢作为燃料的热喷涂方法施加涂层，同时产生高度还原的火焰。 热喷雾法将粉末熔化并将其引导到待涂覆的涡轮机部件的表面上。 仔细控制粉末尺寸以防止粉末氧化，同时提供受控的表面光洁度。 在通过PVD方法施加陶瓷热障层之前，将粘合涂层的表面粗糙度进一步机械加工至预定的表面光洁度。 使用这些仔细控制的预定参数应用的热障系统在高循环应力的条件下提供了出色的耐TBC剥落性能。

    Vacuum coater device and mechanism for supporting and manipulating workpieces in same
    6.
    发明授权
    Vacuum coater device and mechanism for supporting and manipulating workpieces in same 有权
    真空涂布机装置和机构，用于支撑和操纵工件

    公开(公告)号：US07997227B2

    公开(公告)日：2011-08-16

    申请号：US11685354

    申请日：2007-03-13

    申请人： Robert William Bruce ,  Theodore Robert Grossman ,  John Douglas Evans, Sr. ,  Brian Harvey Pilsner

    发明人： Robert William Bruce ,  Theodore Robert Grossman ,  John Douglas Evans, Sr. ,  Brian Harvey Pilsner

    IPC分类号： C23C16/448 ,  C23C16/458 ,  C23C16/48 ,  C23F1/00 ,  H01L21/306 ,  C23C16/06 ,  C23C16/30

    CPC分类号： C23C14/30 ,  C23C14/50 ,  C23C14/505 ,  C23C14/568

    摘要： An apparatus for providing a vacuum coating to a workpiece, including: a coating chamber containing a coating material, with the coating chamber being operable at an elevated temperature and a sub-atmospheric pressure; an electron beam gun projecting an electron beam into the coating chamber and onto the coating material, where the electron beam gun is operable to melt the coating material and to evaporate molten coating material; and, a mechanism for supporting manipulating the workpiece in the coating chamber. The supporting mechanism further includes: a coupling device for retaining the workpiece; a joint connected to the coupling device enabling movement of the workpiece in all directions; an intermediate member connecting the coupling device and the joint; and, a device connected to the intermediate member for moving the workpiece in a designated vertical plane. The supporting mechanism may also include a device connected to the intermediate member for moving the workpiece in a designated horizontal plane.

    摘要翻译： 一种用于向工件提供真空涂层的设备，包括：包含涂层材料的涂层室，涂层室可在升高的温度和低于大气压的压力下操作; 电子束枪将电子束投射到涂覆室和涂覆材料上，其中电子束枪可操作以熔化涂层材料并蒸发熔融涂覆材料; 以及用于支撑在涂布室中操作工件的机构。 支撑机构还包括：用于保持工件的联接装置; 连接到联接装置的联接器，其能够使工件在所有方向上移动; 连接所述联接装置和所述接头的中间构件; 以及连接到中间构件的装置，用于在指定的垂直平面中移动工件。 支撑机构还可以包括连接到中间构件的装置，用于在指定的水平面中移动工件。

    Method for applying a NiA1 based coating by an electroplating technique
    7.
    发明申请
    Method for applying a NiA1 based coating by an electroplating technique 审中-公开
    通过电镀技术涂覆NiAl基涂层的方法

    公开(公告)号：US20100021289A1

    公开(公告)日：2010-01-28

    申请号：US11214292

    申请日：2005-08-29

    申请人： Richard John Grylls ,  Theodore Robert Grossman

    发明人： Richard John Grylls ,  Theodore Robert Grossman

    IPC分类号： F01D9/02 ,  F01D5/18

    CPC分类号： C23C28/321 ,  C23C10/02 ,  C23C10/52 ,  C23C18/32 ,  C23C26/00 ,  C23C28/324 ,  C23C28/325 ,  C23C28/3455 ,  C25D15/02 ,  Y02T50/67 ,  Y02T50/6765

    摘要： The present invention provides a coated article made using a plating process, either electroless or electrolytic, whereby nickel is plated on the article using a solution that includes a suspension of powders or containing one or more of the following elements: Ni, Cr, Al, Zr, Hf, Ti, Ta, Si, Ca, Fe, Y and Ga. Optionally, the coating is then heat treated at a temperature above about 1600.degree. F. for an effective amount of time to allow to homogenize the coating by allowing effective interdiffusion between the species. The level of aluminum may be altered to produce a coating of the predominantly beta phase of the NiAl alloy composition. Optionally, a TBC layer is applied over the predominantly beta phase NiAl alloy composition metallic bond coat.

    摘要翻译： 本发明提供一种使用电镀方法制成的涂覆制品，无电解或电解，由此使用包含粉末悬浮液或含有以下元素中的一种或多种的溶液将镍镀在制品上：Ni，Cr，Al， Zr，Hf，Ti，Ta，Si，Ca，Fe，Y和Ga。任选地，然后将涂层在高于约1600℃的温度下进行热处理。 F.通过允许物种之间的有效相互扩散，有效量的时间允许涂层均化。 可以改变铝的水平以产生NiAl合金组合物的主要β相的涂层。 任选地，在主要β相NiAl合金组合物金属粘结涂层上施加TBC层。

    VACUUM COATER DEVICE AND MECHANISM FOR SUPPORTING AND MANIPULATING WORKPIECES IN SAME
    8.
    发明申请
    VACUUM COATER DEVICE AND MECHANISM FOR SUPPORTING AND MANIPULATING WORKPIECES IN SAME 有权
    用于支持和操作其工作的真空涂料装置和机构

    公开(公告)号：US20080223291A1

    公开(公告)日：2008-09-18

    申请号：US11685354

    申请日：2007-03-13

    申请人： Robert William Bruce ,  Theodore Robert Grossman ,  John Douglas Evans ,  Brian Harvey Pilsner

    发明人： Robert William Bruce ,  Theodore Robert Grossman ,  John Douglas Evans ,  Brian Harvey Pilsner

    IPC分类号： C23C14/00

    CPC分类号： C23C14/30 ,  C23C14/50 ,  C23C14/505 ,  C23C14/568

    摘要： An apparatus for providing a vacuum coating to a workpiece, including: a coating chamber containing a coating material, with the coating chamber being operable at an elevated temperature and a sub-atmospheric pressure; an electron beam gun projecting an electron beam into the coating chamber and onto the coating material, where the electron beam gun is operable to melt the coating material and to evaporate molten coating material; and, a mechanism for supporting manipulating the workpiece in the coating chamber. The supporting mechanism further includes: a coupling device for retaining the workpiece; a joint connected to the coupling device enabling movement of the workpiece in all directions; an intermediate member connecting the coupling device and the joint; and, a device connected to the intermediate member for moving the workpiece in a designated vertical plane. The supporting mechanism may also include a device connected to the intermediate member for moving the workpiece in a designated horizontal plane.

    摘要翻译： 一种用于向工件提供真空涂层的设备，包括：包含涂层材料的涂层室，涂层室可在升高的温度和低于大气压的压力下操作; 电子束枪将电子束投射到涂覆室和涂覆材料上，其中电子束枪可操作以熔化涂层材料并蒸发熔融涂覆材料; 以及用于支撑在涂布室中操作工件的机构。 支撑机构还包括：用于保持工件的联接装置; 连接到联接装置的联接器，其能够使工件在所有方向上移动; 连接所述联接装置和所述接头的中间构件; 以及连接到中间构件的装置，用于在指定的垂直平面中移动工件。 支撑机构还可以包括连接到中间构件的装置，用于在指定的水平面中移动工件。