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    POLYESTER POLYOLS MADE OF ISOPHTHALIC ACID AND/OR TEREPHTHALIC ACID AND OLIGOALKYL OXIDES
    6.
    发明申请
    POLYESTER POLYOLS MADE OF ISOPHTHALIC ACID AND/OR TEREPHTHALIC ACID AND OLIGOALKYL OXIDES 有权
    异辛酸和/或正十二酸和低聚乙烯氧化物的聚酯多元醇

    公开(公告)号：US20120123009A1

    公开(公告)日：2012-05-17

    申请号：US13322989

    申请日：2010-05-18

    申请人： Hartmut Nefzger ,  Erika Bauer ,  Johannes Van De Braak ,  Jürgen Schlossmacher ,  Silvia Kasperek

    发明人： Hartmut Nefzger ,  Erika Bauer ,  Johannes Van De Braak ,  Jürgen Schlossmacher ,  Silvia Kasperek

    IPC分类号： C08L75/06 ,  C08J9/00 ,  C07C69/82

    CPC分类号： C08G18/4252 ,  C08G18/4211 ,  C08G63/672 ,  C08G63/85 ,  C08G2101/0025 ,  C08G2101/005 ,  C08G2105/02

    摘要： The present invention relates to a method for producing a polyester polyol having a concentration of ether groups in the range from 9.0 mol/kg of polyester polyol to 22 mol/kg polyester polyol, characterized in that (i) in a first step (A) isophthalic acid, optionally in the form of a C1-C4 alkyl ester, and/or terephthalic acid, optionally in the form of a C1-C4 alkyl ester, is reacted with (B) oligoethylene glycol of the formula H—(OCH2CH2)n—OH having a numerical average number of oxyethylene groups n in the range from 3.0 to 9.0, in the presence of at least one catalyst selected from the group made up of tin(II) salts, bismuth(II) salts, and titanium tetraalkoxylates, at a temperature in the range from 160° C. to 240° C., and at a pressure in the range from 1 to 1013 mbar, for a duration in the range from 7 to 100 hours, and (ii) in a second step the reaction mixture resulting from step (i) is reacted with (C) phthalic acid and/or phthalic acid hydride, the polyester polyols obtained according to said method, and to the use thereof for producing PUR/PIR hard foam materials

    摘要翻译： 本发明涉及一种聚酯多元醇的制造方法，所述聚酯多元醇的浓度为9.0摩尔/千克聚酯多元醇至22摩尔/千克聚酯多元醇，其特征在于，（i）在第一步骤（A） 任选呈C1-C4烷基酯形式的间苯二甲酸和/或对苯二甲酸，任选呈C1-C4烷基酯形式，与式（B）的低聚乙二醇（H 2 OCH 2 CH 2）n -OH在数均平均数为3.0至9.0的范围内，在至少一种选自锡（II）盐，铋（II）盐和四烷氧基钛酸盐的催化剂存在下， 在160℃至240℃的温度范围内和在1至1013毫巴的压力下持续7至100小时的持续时间，和（ii）在第二步骤中 由步骤（i）得到的反应混合物与（C）邻苯二甲酸和/或邻苯二甲酸氢化物反应，聚酯多元醇 根据所述方法染色，以及其用于生产PUR / PIR硬泡沫材料的用途

    STABLE EMULSIONS AND THEIR USE IN THE PRODUCTION OF FOAMS BASED ON ISOCYANATE
    10.
    发明申请
    STABLE EMULSIONS AND THEIR USE IN THE PRODUCTION OF FOAMS BASED ON ISOCYANATE 审中-公开
    稳定的乳液及其在异氰酸酯生产中的应用

    公开(公告)号：US20140323605A1

    公开(公告)日：2014-10-30

    申请号：US14240770

    申请日：2012-08-22

    申请人： Reinhard Albers ,  Torsten Heinemann ,  Stephanie Vogel ,  Hartmut Nefzger ,  Frank Otto

    发明人： Reinhard Albers ,  Torsten Heinemann ,  Stephanie Vogel ,  Hartmut Nefzger ,  Frank Otto

    IPC分类号： C08G18/48 ,  C08L75/08

    CPC分类号： C08G18/48 ,  C08G18/4018 ,  C08G18/4216 ,  C08G18/425 ,  C08G18/4829 ,  C08G18/5033 ,  C08L71/02 ,  C08L75/08

    摘要： The invention relates to stable emulsions for the production of foams based on isocyanate, at least comprising three polyols A1a, A1b and A1c as well as at least one physical blowing agent T, wherein A1a is a polyether polyol obtained by addition of epoxides to starter compounds selected from carbohydrates and di- or higher-functional alcohols, A1b is a polyether polyol started on an aromatic amine, and A1c is a polyester polyol obtained by esterification of a polycarboxylic acid component and a polyalcohol component, wherein the total amount of aromatic dicarboxylic acid derivatives used in the esterification, calculated on the basis of the free aromatic dicarboxylic acids and based on the total mass of polyalcohol component and polycarboxylic acid component, is less than or equal to 48.5% by mass.

    摘要翻译： 本发明涉及用于生产基于异氰酸酯的泡沫的稳定乳液，至少包含三种多元醇A1a，A1b和A1c以及至少一种物理发泡剂T，其中A1a是通过向起始化合物中加入环氧化物得到的聚醚多元醇 选自碳水化合物和二官能或更高官能的醇，A1b是在芳族胺上开始的聚醚多元醇，A1c是通过多元羧酸组分和多元醇组分的酯化获得的聚酯多元醇，其中芳族二羧酸 以游离芳族二羧酸为基准，以多元醇成分和多元羧酸成分的总质量为基准计算的酯化衍生物的摩尔比小于或等于48.5质量％。