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    Sulfonation, sulfation and sulfamation
    1.
    发明授权
    Sulfonation, sulfation and sulfamation 失效
    磺化，硫酸化和磺化

    公开(公告)号：US06384271B1

    公开(公告)日：2002-05-07

    申请号：US09848842

    申请日：2001-05-04

    Applicant: Stephen Ernest Jacobson ,  David Richard Corbin

    Inventor： Stephen Ernest Jacobson ,  David Richard Corbin

    IPC: C07C30901

    CPC classification number: C07C303/06 ,  C07B45/02 ,  C07C309/30

    Abstract: A process that can be used for sulfonating, sulfating, or sulfamating an organic compound is disclosed. The process can comprise, consist essentially of, or consist of, contacting the organic compound with sulfur trioxide under a condition sufficient to effect the sulfonation, sulfation, or sulfamation of the organic compound. The organic compound can be an aromatic compound, alcohol, carbohydrate, amine, amide, protein, or combinations of two or more thereof. The sulfur trioxide can be present in a complex comprising an inorganic support such as zeolite, silicalite, silica, titanosilicate, borosilicate, clay, aluminophosphate, and combinations of two or more thereof.

    Abstract translation: 公开了可用于磺化，硫酸化或磺化有机化合物的方法。 该方法可以在有机化合物的磺化，硫酸化或磺化作用足够的条件下，包含有机化合物与三氧化硫的接触，或由其组成。 有机化合物可以是芳族化合物，醇，碳水化合物，胺，酰胺，蛋白质或其两种或多种的组合。 三氧化硫可以存在于包含无机载体如沸石，硅沸石，二氧化硅，钛硅酸盐，硼硅酸盐，粘土，磷酸铝及其两种或更多种的组合的络合物中。

    Sulfonation, sulfation, and sulfamation
    2.
    发明授权
    Sulfonation, sulfation, and sulfamation 失效

    公开(公告)号：US06462215B1

    公开(公告)日：2002-10-08

    申请号：US10067643

    申请日：2002-02-04

    Applicant: Stephen Ernest Jacobson ,  David Richard Corbin

    Inventor： Stephen Ernest Jacobson ,  David Richard Corbin

    IPC: C07C30500

    CPC classification number: C07C303/06 ,  C07B45/02 ,  C07C309/30

    Abstract: A process that can be used for sulfonating, sulfating, or sulfamating an organic compound is disclosed. The process can comprise, consist essentially of, or consist of, contacting the organic compound with sulfur trioxide under a condition sufficient to effect the sulfonation, sulfation, or sulfamation of the organic compound. The organic compound can be an aromatic compound, alcohol, carbohydrate, amine, amide, protein, or combinations of two or more thereof. The sulfur trioxide can be present in a complex comprising an inorganic support such as zeolite, silicalite, silica, titanosilicate, borosilicate, clay, aluminophosphate, and combinations of two or more thereof.

    Sulfur trioxide delivery system
    3.
    发明授权
    Sulfur trioxide delivery system 失效
    三氧化硫输送系统

    公开(公告)号：US06773490B2

    公开(公告)日：2004-08-10

    申请号：US09848896

    申请日：2001-05-04

    Applicant: Stephen Ernest Jacobson ,  Howard M. Blank ,  David Richard Corbin

    Inventor： Stephen Ernest Jacobson ,  Howard M. Blank ,  David Richard Corbin

    IPC: B01D5926

    CPC classification number: B01J20/28078 ,  B01D15/00 ,  B01J20/103 ,  B01J20/18 ,  C01B17/90 ,  Y10S502/517

    Abstract: A process for reversible sorption of sulfur trioxide onto a sorbent comprising a) contacting from about 15% to 100% sulfur trioxide with the sorbent under anhydrous conditions at a temperature of from about 35° C. to about 150° C. thereby sorbing the sulfur trioxide onto the sorbent, b) desorbing sulfur trioxide from the sorbent at a temperature of from about 150° C. to about 350° C. at about atmospheric pressure, or under a vacuum pressure, and c) recycling said sorbent by continuously repeating steps a) and b), wherein said sorbent consists essentially of silica or zeolite having a silicon to aluminum ratio in the ranges of from about 1 to about 4.4 or greater than about 5.1, and having a pore size of at least 0.5 nm is disclosed.

    Abstract translation: 一种用于将三氧化硫可逆吸附到吸附剂上的方法，其包括a）在无水条件下，在约35℃至约150℃的温度下，使约15％至100％的三氧化硫与吸附剂接触，从而吸附硫 三氧化硫在吸附剂上，b）在约大气压或真空压力下，在约150℃至约350℃的温度下从吸附剂解吸三氧化硫，以及c）通过连续重复步骤回收所述吸附剂 a）和b），其中所述吸附剂基本上由二氧化硅或沸石组成，其硅与铝的比例为约1至约4.4或大于约5.1，孔径至少为0.5nm。

    Sulfonation, sulfation, and sulfamation
    4.
    发明授权
    Sulfonation, sulfation, and sulfamation 失效
    磺化，硫酸化和磺化

    公开(公告)号：US06448435B1

    公开(公告)日：2002-09-10

    申请号：US10067639

    申请日：2002-02-04

    Applicant: Stephen Ernest Jacobson ,  David Richard Corbin

    Inventor： Stephen Ernest Jacobson ,  David Richard Corbin

    IPC: C07C31100

    CPC classification number: C07C303/06 ,  C07B45/02 ,  C07C309/30

    Abstract: A process that can be used for sulfonating, sulfating, or sulfamating an organic compound is disclosed. The process can comprise, consist essentially of, or consist of, contacting the organic compound with sulfur trioxide under a condition sufficient to effect the sulfonation, sulfation, or sulfamation of the organic compound. The organic compound can be an aromatic compound, alcohol, carbohydrate, amine, amide, protein, or combinations of two or more thereof. The sulfur trioxide can be present in a complex comprising an inorganic support such as zeolite, silicalite, silica, titanosilicate, borosilicate, clay, aluminophosphate, and combinations of two or more thereof.

    Abstract translation: 公开了可用于磺化，硫酸化或磺化有机化合物的方法。 该方法可以在有机化合物的磺化，硫酸化或磺化作用足够的条件下，包含有机化合物与三氧化硫的接触，或由其组成。 有机化合物可以是芳族化合物，醇，碳水化合物，胺，酰胺，蛋白质或其两种或多种的组合。 三氧化硫可以存在于包含无机载体如沸石，硅沸石，二氧化硅，钛硅酸盐，硼硅酸盐，粘土，磷酸铝及其两种或更多种的组合的络合物中。

    Recovery of isoflavones and removal of oligosaccharides from aqueous mixtures using zeolites
    5.
    发明授权
    Recovery of isoflavones and removal of oligosaccharides from aqueous mixtures using zeolites 失效
    异构体的回收和使用沸石从含水混合物中除去寡糖

    公开(公告)号：US07618671B2

    公开(公告)日：2009-11-17

    申请号：US10983125

    申请日：2004-11-05

    Applicant: David Richard Corbin ,  Vasantha Nagarajan ,  Vidya Pai ,  Stuart M. Thomas

    Inventor： David Richard Corbin ,  Vasantha Nagarajan ,  Vidya Pai ,  Stuart M. Thomas

    IPC: A23L1/20 ,  A23L1/36 ,  A23L2/00 ,  A61K36/48 ,  C01B33/36

    CPC classification number: A23L33/185 ,  A23L5/273 ,  Y10S423/21 ,  Y10S423/27

    Abstract: The present invention provides a process using zeolites for recovering isoflavones and removing undesired oligosaccharides from aqueous mixtures, such as soy whey and other plant processing waste products. The aqueous mixture is treated with a large pore hydrophobic zeolite, such as zeolite Beta, to remove isoflavones, followed by treatment with an ultrastabilized, hydrophobic zeolite Y, such as CBV-901 or HiSiv™ 4000, to remove the undesired oligosaccharides raffinose and stachyose. The recovered isoflavones and digestible sugars, glucose, sucrose, and fructose, are useful in food products.

    Abstract translation: 本发明提供了一种使用沸石回收异黄酮并从含水混合物如大豆乳清和其它植物加工废物中除去不期望的寡糖的方法。 用大孔疏水性沸石如β沸石处理含水混合物以除去异黄酮，然后用超稳定的疏水性沸石Y（例如CBV-901或HiSiv TM 4000）处理以除去不期望的寡糖棉子糖 和水苏糖 回收的异黄酮和可消化糖，葡萄糖，蔗糖和果糖，可用于食品。

    Dehydrohalogenation processes
    8.
    发明授权
    Dehydrohalogenation processes 失效
    脱卤化氢工艺

    公开(公告)号：US5750808A

    公开(公告)日：1998-05-12

    申请号：US677063

    申请日：1996-07-09

    Applicant: Wendell Richard Cassel ,  David Richard Corbin ,  V.N. Mallikarjuna Rao

    Inventor： Wendell Richard Cassel ,  David Richard Corbin ,  V.N. Mallikarjuna Rao

    IPC: C07C17/25 ,  C07C17/269 ,  C07C17/395 ,  C07C17/00

    CPC classification number: C07C17/395 ,  C07C17/25 ,  C07C17/269

    Abstract: A process is disclosed for the dehydrohalogenation of partially halogenated ethanes of the formula C.sub.2 H.sub.a Cl.sub.b F.sub.c where a is an integer from 1 to 4, b is an integer from 0 to 3 and c is an integer form 1 to 5 to produce olefins selected from the group consisting of C.sub.2 H.sub.a-1 Cl.sub.b-1 F.sub.c and C.sub.2 H.sub.a-1 Cl.sub.b F.sub.c-1. The process involves contacting C.sub.2 H.sub.a Cl.sub.b F.sub.c with a zeolite selected from the group consisting of NaX and CsY. Selective reaction of one isomer from a mixture of two isomers is disclosed as a means for purification of the relatively unreactive isomer. Also disclosed is a process for producing perfluorocyclobutane which involves contacting CHF.sub.2 CClF.sub.2 with such zeolites.

    Abstract translation: 公开了用于式C 2 H a Cl b F c的部分卤代乙烷的脱卤化氢的方法，其中a是1至4的整数，b是0至3的整数，c是1至5的整数，以产生选自以下的烯烃： 的C2Ha-1Clb-1Fc和C2Ha-1ClbFc-1。 该方法包括使C 2 H a Cl b F cc与选自NaX和CsY的沸石接触。 公开了一种异构体从两种异构体的混合物的选择性反应，作为相对不反应异构体的纯化手段。 还公开了一种制备全氟环丁烷的方法，其涉及使CHF 2 CClF 2与这种沸石接触。

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