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    High performance thermoelectric materials and their method of preparation
    3.
    发明授权
    High performance thermoelectric materials and their method of preparation 有权
    高性能热电材料及其制备方法

    公开(公告)号：US07723607B2

    公开(公告)日：2010-05-25

    申请号：US11106243

    申请日：2005-04-14

    申请人： Munirpallam Appadorai Subramanian ,  Tao He ,  James J. Krajewski

    发明人： Munirpallam Appadorai Subramanian ,  Tao He ,  James J. Krajewski

    IPC分类号： H01L35/20

    CPC分类号： C01G51/006 ,  C01P2002/52 ,  C01P2002/72 ,  C01P2002/76 ,  C01P2002/77 ,  C01P2006/40 ,  H01L35/18

    摘要： The present invention provides an indium-doped Co4Sb12 skutterudite composition in which some Co on the cubic lattice structure may be replaced with one or more members of the group consisting of Fe, Ni, Ru, Rh, Pd, Ir and Pt; some Sb on the planar rings may be replaced by one or more members of the group consisting of Si, Ga, Ge and Sn; and a second dopant atom is selected from a member of the group consisting of Ca, Sc, Zn, Sr, Y, Pd, Ag, Cd, Ba, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb and Lu. The composition is useful as a thermoelectric material. In preferred embodiments, the composition has a figure of merit greater than 1.0. The present invention also provides a process for the production of the composition, and thermoelectric devices using the composition.

    摘要翻译： 本发明提供一种铟掺杂的Co4Sb12方钴矿组合物，其中立方晶格结构上的一些Co可以被一个或多个由Fe，Ni，Ru，Rh，Pd，Ir和Pt组成的组中的一个或多个成员所取代; 平面环上的一些Sb可以由Si，Ga，Ge和Sn组成的组中的一个或多个成员代替; 并且第二掺杂剂原子选自Ca，Sc，Zn，Sr，Y，Pd，Ag，Cd，Ba，La，Ce，Pr，Nd，Sm，Eu，Gd，Tb，Dy ，Ho，Er，Tm，Yb和Lu。 该组合物可用作热电材料。 在优选的实施方案中，组合物的品质因数大于1.0。 本发明还提供一种制备该组合物的方法，以及使用该组合物的热电装置。

    Methods of making glass-crystalline particles including a glass component and a crystalline component
    5.
    发明授权
    Methods of making glass-crystalline particles including a glass component and a crystalline component 失效
    制造玻璃成分和结晶成分的玻璃结晶粒子的方法

    公开(公告)号：US08545733B2

    公开(公告)日：2013-10-01

    申请号：US12891244

    申请日：2010-09-27

    申请人： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    发明人： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    IPC分类号： H01B1/12

    CPC分类号： C03B19/1065

    摘要： Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.

    摘要翻译： 公开了一种制造包含玻璃组分和结晶组分的玻璃晶粒的方法，包括以下步骤：a）提供包含溶剂，玻璃组分组合物和结晶组分组合物的前体溶液; b）形成包含前体溶液的细碎液滴的气溶胶，其中液滴浓度低于液滴的碰撞和随后的聚结导致液滴浓度降低10％的浓度; c）加热气溶胶，其中在加热时形成玻璃晶体颗粒，其中所述玻璃晶体颗粒包含玻璃组分和结晶组分，并且其中所述结晶组分包含一种或多种金属氧化物; 和d）分离玻璃晶粒。

    METHODS OF MAKING GLASS-CRYSTALLINE PARTICLES INCLUDING A GLASS COMPONENT AND A CRYSTALLINE COMPONENT
    9.
    发明申请
    METHODS OF MAKING GLASS-CRYSTALLINE PARTICLES INCLUDING A GLASS COMPONENT AND A CRYSTALLINE COMPONENT 失效
    制造玻璃晶粒的方法，包括玻璃组分和晶体组分

    公开(公告)号：US20110233486A1

    公开(公告)日：2011-09-29

    申请号：US12891244

    申请日：2010-09-27

    申请人： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    发明人： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    IPC分类号： H01B1/20 ,  C03B19/10

    CPC分类号： C03B19/1065

    摘要： Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.

    摘要翻译： 公开了一种制造包含玻璃组分和结晶组分的玻璃晶粒的方法，包括以下步骤：a）提供包含溶剂，玻璃组分组合物和结晶组分组合物的前体溶液; b）形成包含前体溶液的细碎液滴的气溶胶，其中液滴浓度低于液滴的碰撞和随后的聚结导致液滴浓度降低10％的浓度; c）加热气溶胶，其中在加热时形成玻璃晶体颗粒，其中所述玻璃晶体颗粒包含玻璃组分和结晶组分，并且其中所述结晶组分包含一种或多种金属氧化物; 和d）分离玻璃晶粒。