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    Process for Producing Cyclic Compounds
    2.
    发明申请
    Process for Producing Cyclic Compounds 有权
    生产环状化合物的方法

    公开(公告)号：US20070173643A1

    公开(公告)日：2007-07-26

    申请号：US11688022

    申请日：2007-03-19

    申请人： Todd Werpy ,  John Frye ,  James White ,  Johnathan Holladay ,  Alan Zacher

    发明人： Todd Werpy ,  John Frye ,  James White ,  Johnathan Holladay ,  Alan Zacher

    IPC分类号： C07D207/267 ,  C07D223/10 ,  C07D205/02

    CPC分类号： C07D207/404

    摘要： The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkylating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Ammonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100° C. to about 400° C. to produce N-methyl succinimide which is purified and hydrogenated to form NMP.

    摘要翻译： 本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。 环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。 本发明包括生产N-烷基产物的方法。 调节溶液的氨含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。 加入烷基化剂并将该初始化合物烷基化并环化。 本发明包括制备N-甲基吡咯烷酮（NMP）的方法。 将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。 甲基化剂与琥珀酸酯在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

    Methods of producing compounds from plant material
    3.
    发明申请
    Methods of producing compounds from plant material 审中-公开
    从植物材料生产化合物的方法

    公开(公告)号：US20050064560A1

    公开(公告)日：2005-03-24

    申请号：US10980927

    申请日：2004-11-03

    申请人： Todd Werpy ,  Andrew Schmidt ,  John Frye ,  Alan Zacher ,  James Franz ,  Mikhail Alnajjar ,  Gary Neuenschwander ,  Eric Alderson ,  Rick Orth

    发明人： Todd Werpy ,  Andrew Schmidt ,  John Frye ,  Alan Zacher ,  James Franz ,  Mikhail Alnajjar ,  Gary Neuenschwander ,  Eric Alderson ,  Rick Orth

    IPC分类号： C08B30/10 ,  C11B1/10 ,  C12P19/02

    CPC分类号： C07C29/00 ,  C07C29/60 ,  C08B30/10 ,  C11B1/10 ,  C07C31/202 ,  C07C31/225 ,  C07C31/205

    摘要： The invention includes methods of processing plant material by adding water to form a mixture, heating the mixture, and separating a liquid component from a solid-comprising component. At least one of the liquid component and the solid-comprising component undergoes additional processing. Processing of the solid-comprising component produces oils, and processing of the liquid component produces one or more of glycerol, ethylene glycol, lactic acid and propylene glycol. The invention includes a process of forming glycerol, ethylene glycol, lactic acid and propylene glycol from plant matter by adding water, heating and filtering the plant matter. The filtrate containing starch, starch fragments, hemicellulose and fragments of hemicellulose is treated to form linear poly-alcohols which are then cleaved to produce one or more of glycerol, ethylene glycol, lactic acid and propylene glycol. The invention also includes a method of producing free and/or complexed sterols and stanols from plant material.

    摘要翻译： 本发明包括通过加入水以形成混合物来加工植物材料的方法，加热混合物，以及从含固体组分分离液体组分。 液体组分和固体组分中的至少一种经受另外的处理。 固体成分组分的加工产生油，并且液体组分的加工产生甘油，乙二醇，乳酸和丙二醇中的一种或多种。 本发明包括通过加水，加热和过滤植物物质从植物物质形成甘油，乙二醇，乳酸和丙二醇的方法。 将含有淀粉，淀粉碎片，半纤维素和半纤维素片段的滤液处理形成线性多元醇，然后将其切割以产生甘油，乙二醇，乳酸和丙二醇中的一种或多种。 本发明还包括从植物材料生产游离和/或络合的甾醇和甾烷醇的方法。

    Methods of producing compounds from plant materials
    4.
    发明申请
    Methods of producing compounds from plant materials 有权
    从植物材料生产化合物的方法

    公开(公告)号：US20050065337A1

    公开(公告)日：2005-03-24

    申请号：US10980928

    申请日：2004-11-03

    申请人： Todd Werpy ,  Andrew Schmidt ,  John Frye ,  Alan Zacher ,  James Franz ,  Mikhail Alnajjar ,  Gary Neuenschwander ,  Eric Alderson ,  Rick Orth

    发明人： Todd Werpy ,  Andrew Schmidt ,  John Frye ,  Alan Zacher ,  James Franz ,  Mikhail Alnajjar ,  Gary Neuenschwander ,  Eric Alderson ,  Rick Orth

    IPC分类号： C08B30/10 ,  C11B1/10 ,  C07H1/06

    CPC分类号： C07C29/00 ,  C07C29/60 ,  C08B30/10 ,  C11B1/10 ,  C07C31/202 ,  C07C31/225 ,  C07C31/205

    摘要： The invention includes methods of processing plant material by adding water to form a mixture, heating the mixture, and separating a liquid component from a solid-comprising component. At least one of the liquid component and the solid-comprising component undergoes additional processing. Processing of the solid-comprising component produces oils, and processing of the liquid component produces one or more of glycerol, ethylene glycol, lactic acid and propylene glycol. The invention includes a process of forming glycerol, ethylene glycol, lactic acid and propylene glycol from plant matter by adding water, heating and filtering the plant matter. The filtrate containing starch, starch fragments, hemicellulose and fragments of hemicellulose is treated to form linear poly-alcohols which are then cleaved to produce one or more of glycerol, ethylene glycol, lactic acid and propylene glycol. The invention also includes a method of producing free and/or complexed sterols and stanols from plant material.

    摘要翻译： 本发明包括通过加入水以形成混合物来加工植物材料的方法，加热混合物，以及从含固体组分分离液体组分。 液体组分和固体组分中的至少一种经受另外的处理。 固体成分组分的加工产生油，并且液体组分的加工产生甘油，乙二醇，乳酸和丙二醇中的一种或多种。 本发明包括通过加水，加热和过滤植物物质从植物物质形成甘油，乙二醇，乳酸和丙二醇的方法。 将含有淀粉，淀粉碎片，半纤维素和半纤维素片段的滤液处理形成线性多元醇，然后将其切割以产生甘油，乙二醇，乳酸和丙二醇中的一种或多种。 本发明还包括从植物材料生产游离和/或络合的甾醇和甾烷醇的方法。

    Hydroxymethylfurfural Reduction Methods and Methods of Producing Furandimethanol
    5.
    发明申请
    Hydroxymethylfurfural Reduction Methods and Methods of Producing Furandimethanol 有权
    羟甲基糠醛还原方法和生产呋喃二甲醇的方法

    公开(公告)号：US20070287845A1

    公开(公告)日：2007-12-13

    申请号：US11760634

    申请日：2007-06-08

    申请人： Michael Lilga ,  Richard Hallen ,  Todd Werpy ,  James White ,  Johnathan Holladay ,  John Frye ,  Alan Zacher

    发明人： Michael Lilga ,  Richard Hallen ,  Todd Werpy ,  James White ,  Johnathan Holladay ,  John Frye ,  Alan Zacher

    IPC分类号： C07D307/02

    CPC分类号： C07D307/42 ,  C07D307/46

    摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250° C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30° C. A method of producing tetrahydrofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.

    摘要翻译： 提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有至少一种选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh的金属的催化剂接触， 温度小于或等于250℃。氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。 HMF在等于或高于30℃的温度下相对于果糖选择性地氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。 进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

    Deicing/anti-icing fluids
    6.
    发明申请
    Deicing/anti-icing fluids 有权
    除冰/防冰液

    公开(公告)号：US20050087720A1

    公开(公告)日：2005-04-28

    申请号：US10833942

    申请日：2004-04-28

    申请人： William Samuels ,  H. Conkle ,  Bruce Monzyk ,  Kevin Simmons ,  John Frye ,  Todd Werpy ,  Sara Kuczek ,  Satya Chauhan

    发明人： William Samuels ,  H. Conkle ,  Bruce Monzyk ,  Kevin Simmons ,  John Frye ,  Todd Werpy ,  Sara Kuczek ,  Satya Chauhan

    IPC分类号： C09K3/18

    CPC分类号： C09K3/18 ,  C09K3/185

    摘要： A nontoxic deicing/anti-icing fluid includes a freezing point depressant selected from short chain polyols having 3 to 5 carbons atoms, and mixtures thereof, a wetting agent, an antioxidant/preservative, and water. The fluid has an LD50 greater than about 10,000 mg/L. Another deicing/anti-icing fluid includes the freezing point depressant, a vinylpyrrolidone polymer having a molecular weight between about 10,000 and about 700,000, and water. A runway deicing fluid includes glycerol, a buffer, an antioxidant/preservative, and water. Another deicing/anti-icing fluid includes a freezing point depressant having hydrophobic character, a wetting agent comprising an organophosphorus compound capable of producing an organic wettable surface, and water.

    摘要翻译： 无毒除冰/防冰液体包括选自具有3至5个碳原子的短链多元醇及其混合物，润湿剂，抗氧化剂/防腐剂和水的凝固点抑制剂。 流体具有大于约10,000mg / L的LD 50。 另一种除冰/防冰液体包括冰点抑制剂，分子量介于约10,000至约700,000之间的乙烯基吡咯烷酮聚合物和水。 跑道除冰液包括甘油，缓冲剂，抗氧化剂/防腐剂和水。 另一种除冰/防冰流体包括具有疏水性的凝固点抑制剂，包含能够产生有机可湿性表面的有机磷化合物的润湿剂和水。

    Methods of making pyrrolidones
    8.
    发明授权
    Methods of making pyrrolidones 有权
    制备吡咯烷酮的方法

    公开(公告)号：US06632951B2

    公开(公告)日：2003-10-14

    申请号：US10280622

    申请日：2002-10-25

    申请人： Todd Werpy ,  John G. Frye, Jr. ,  Yong Wang ,  Alan H. Zacher

    发明人： Todd Werpy ,  John G. Frye, Jr. ,  Yong Wang ,  Alan H. Zacher

    IPC分类号： C07C207263

    CPC分类号： C07D207/267 ,  C07D201/02 ,  C07D201/08

    摘要： The present invention provides methods for making N-methylpyrrolidine and analogous compounds via hydrogenation. Novel catalysts for this process, and novel conditions/yields are also described. Other process improvements may include extraction and hydrolysis steps. Some preferred reactions take place in the aqueous phase. Starting materials for making N-methylpyrrolidine may include succinic acid, N-methylsuccinimide, and their analogs.

    摘要翻译： 本发明提供了通过氢化制备N-甲基吡咯烷和类似化合物的方法。 还描述了用于该方法的新型催化剂和新的条件/收率。 其他工艺改进可以包括提取和水解步骤。 一些优选的反应发生在水相中。 用于制备N-甲基吡咯烷的原料可包括琥珀酸，N-甲基琥珀酰亚胺及其类似物。