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1.发明授权Method for producing aliphatic carboxylic acids from aldehydes by microreaction technology 失效通过微反应技术从醛制备脂肪族羧酸的方法公开(公告)号：US08664434B2
公开(公告)日：2014-03-04
申请号：US13138719
申请日：2010-03-03
申请人： Tonia Weber , Alexander Kaufmann , Oliver Borgmeier , Thorsten Kreickmann , Heinz Strutz , Diana Utz , Elias Klemm , Claudia Liebold
发明人： Tonia Weber , Alexander Kaufmann , Oliver Borgmeier , Thorsten Kreickmann , Heinz Strutz , Diana Utz , Elias Klemm , Claudia Liebold
IPC分类号： C07C51/16
CPC分类号： C07C51/235 , B01J19/0093 , C07C53/124 , C07C53/126 , C07C53/122
摘要： A process for preparing aliphatic carboxylic acids having 3 to 10 carbon atoms by oxidizing the corresponding aldehydes with oxygen or oxygen-containing gases, characterized in that (i) the oxidation is performed in a microreactor at elevated pressure and with an oxygen excess based on the stoichiometrically required amount of oxygen, and (ii) in that the reaction mixture removed from the microreactor is passed through at least one postreactor without further addition of oxygen, and (iii) wherein the oxidation reaction in the microreactor is performed under such conditions that aldehyde and corresponding peracid formed are present in the reaction mixture removed in a molar ratio within a range of 1:(0.9 to 1.1), preferably of 1:(0.95 to 1.05).
摘要翻译： 通过用氧或含氧气体氧化相应的醛来制备具有3至10个碳原子的脂族羧酸的方法，其特征在于：（i）在微反应器中在升高的压力下进行氧化，并且基于 化学计量所需量的氧，和（ii）将从微反应器中除去的反应混合物通过至少一个后反应器而不进一步加入氧，和（iii）其中在微反应器中的氧化反应在醛 并且形成的相应的过酸存在于反应混合物中，摩尔比在1：（0.9〜1.1），优选1：（0.95〜1.05）的范围内除去。
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2.发明申请公开(公告)号：US20120035393A1
公开(公告)日：2012-02-09
申请号：US13138719
申请日：2010-03-03
申请人： Tonia Weber , Alexander Kaufmann , Oliver Borgmeier , Thorsten Kreickmann , Heinz Strutz , Diana Utz , Elias Klemm , Claudia Liebold
发明人： Tonia Weber , Alexander Kaufmann , Oliver Borgmeier , Thorsten Kreickmann , Heinz Strutz , Diana Utz , Elias Klemm , Claudia Liebold
IPC分类号： C07C51/235
CPC分类号： C07C51/235 , B01J19/0093 , C07C53/124 , C07C53/126 , C07C53/122
摘要： A process for preparing aliphatic carboxylic acids having 3 to 10 carbon atoms by oxidizing the corresponding aldehydes with oxygen or oxygen-containing gases, characterized in that (i) the oxidation is performed in a microreactor at elevated pressure and with an oxygen excess based on the stoichiometrically required amount of oxygen, and (ii) in that the reaction mixture removed from the microreactor is passed through at least one postreactor without further addition of oxygen, and (iii) wherein the oxidation reaction in the microreactor is performed under such conditions that aldehyde and corresponding peracid formed are present in the reaction mixture removed in a molar ratio within a range of 1:(0.9 to 1.1), preferably of 1:(0.95 to 1.05).
摘要翻译： 通过用氧或含氧气体氧化相应的醛来制备具有3至10个碳原子的脂族羧酸的方法，其特征在于：（i）在微反应器中在升高的压力下进行氧化，并且基于 化学计量所需量的氧，和（ii）将从微反应器中除去的反应混合物通过至少一个后反应器而不进一步加入氧，和（iii）其中在微反应器中的氧化反应在醛 并且形成的相应的过酸存在于反应混合物中，摩尔比在1：（0.9〜1.1），优选1：（0.95〜1.05）的范围内除去。
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公开(公告)号：US20100294673A1
公开(公告)日：2010-11-25
申请号：US12810798
申请日：2008-12-01
申请人： Matthias Koch , Joerg Pahnke , Gerhard Jonschker , Stefan Spange , Patrick Kempe , Silke Grund , Elias Klemm
发明人： Matthias Koch , Joerg Pahnke , Gerhard Jonschker , Stefan Spange , Patrick Kempe , Silke Grund , Elias Klemm
CPC分类号： B01J20/20 , B01J20/26 , B01J20/28042 , B01J20/28054 , B01J20/3078 , C01B3/0015 , C04B35/52 , C08G61/02 , C08G61/125 , C08G2261/1422 , C08G2261/3222 , C08G2261/3424 , C08K3/013 , C08K3/36 , C08L61/06 , F17C11/005 , Y02E60/321 , Y02E60/328 , C08L65/00
摘要： The invention relates to monolithic materials which consist of porous, preferably highly porous, carbon and are suitable, inter alia, for the storage of gases, such as, for example, hydrogen and methane, and for absorptive and adsorptive gas purification.
摘要翻译： 本发明涉及由多孔，优选高度多孔的碳组成的整体材料，特别适用于储存气体，例如氢气和甲烷，以及用于吸收和吸附气体净化。
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公开(公告)号：US20070053808A1
公开(公告)日：2007-03-08
申请号：US10553312
申请日：2004-03-31
申请人： Georg Markowz , Johannes Albrecht , Johannes Ehrlich , Michael Jucys , Elias Klemm , Armin Oliveira , Reinhard Machnik , Juergen Rapp , Ruediger Schuette , Steffen Schirrmeister , Olaf Morstein , Hartmut Hederer , Martin Schmitz-Niederau
发明人： Georg Markowz , Johannes Albrecht , Johannes Ehrlich , Michael Jucys , Elias Klemm , Armin Oliveira , Reinhard Machnik , Juergen Rapp , Ruediger Schuette , Steffen Schirrmeister , Olaf Morstein , Hartmut Hederer , Martin Schmitz-Niederau
CPC分类号： B01F5/0471 , B01F13/0059 , B01F2005/0034 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00889
摘要： The present invention discloses a microreactor for performing heterogeneous catalytic reactions, being of plate or stack construction for industrial use, with provision made for chambers between the plates for the chemical reaction and for the heat removal. Inside the reaction chambers, catalyst material is applied to the internal walls or filled into recesses, and in all chambers there are spacers. In particular the slot-shaped reaction chambers have channels with a hydraulic diameter smaller than 1500 μm and a ratio of free slot width to free slot height in the range of 10 to 450.
摘要翻译： 本发明公开了一种用于进行非均相催化反应的微反应器，它是用于工业应用的板或堆叠结构，为用于化学反应和排热的板之间的室提供。 在反应室内部，将催化剂材料施加到内壁或填充到凹部中，并且在所有室中都存在间隔物。 特别地，槽形反应室具有液压直径小于1500μm的通道，并且自由槽宽度与自由槽高度的比率在10至450的范围内。
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5.发明授权Method for obtaining a gaseous phase from a liquid medium and device for carrying out the same 有权用于从液体介质获得气相的方法和用于执行该气相的装置公开(公告)号：US07722740B2
公开(公告)日：2010-05-25
申请号：US10531609
申请日：2003-10-14
申请人： Elias Klemm , Johannes Albrecht , Armin Lange de Oliveira , Georg Markowz , Stefan Gross , Ruediger Schuette , Johannes Ehrlich , Steffen Schirrmeister , Olaf von Morstein
发明人： Elias Klemm , Johannes Albrecht , Armin Lange de Oliveira , Georg Markowz , Stefan Gross , Ruediger Schuette , Johannes Ehrlich , Steffen Schirrmeister , Olaf von Morstein
IPC分类号： B01D1/22
CPC分类号： F28F3/048 , B01B1/005 , B01D1/22 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/00871 , B01J2219/00873 , C01B15/01 , F28D3/00 , F28F3/083 , F28F2260/02
摘要： A modular construction micro-reactor with parallel microchannels on fluid guide plates for chemical reactions, but not for evaporation purposes is known. A modular construction falling film evaporator is disclosed, comprising a stack of alternate gap-like evaporation chambers and sheet-like evaporator modules with an assembly of parallel microchannels, whereby the evaporation chambers are open above and/or below across the whole width of the module and the stack is arranged in a container. The falling film evaporator is used in a method for obtaining a gaseous phase from a liquid medium on a technical scale and is suitable for the concentration of thermolabile solutions and rapidly adjustable production of a gas stream.
摘要翻译： 具有用于化学反应但不用于蒸发目的的流体引导板上具有平行微通道的模块化结构微反应器是已知的。 公开了一种模块化结构降膜蒸发器，其包括一组交替的间隙式蒸发室和具有平行微通道组件的片状蒸发器模块，由此蒸发室在模块的整个宽度上方和/或下方敞开 并且堆叠被布置在容器中。 降膜蒸发器用于在技术规模上从液体介质获得气相的方法，适用于浓缩不溶热溶液并快速调节气流的产生。
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6.发明申请Method for obtaining a gaseous phase from a liquid medium and device for carrying out the same 有权用于从液体介质获得气相的方法和用于执行该气相的装置公开(公告)号：US20060060305A1
公开(公告)日：2006-03-23
申请号：US10531609
申请日：2003-10-14
申请人： Elias Klemm , Johannes Albrecht , Armin Oliveira , Georg Markowz , Stefan Gross , Ruediger Schuette , Johannes Ehrlich , Steffen Schirrmeister , Olaf Morstein
发明人： Elias Klemm , Johannes Albrecht , Armin Oliveira , Georg Markowz , Stefan Gross , Ruediger Schuette , Johannes Ehrlich , Steffen Schirrmeister , Olaf Morstein
IPC分类号： B01D1/00
CPC分类号： F28F3/048 , B01B1/005 , B01D1/22 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/00871 , B01J2219/00873 , C01B15/01 , F28D3/00 , F28F3/083 , F28F2260/02
摘要： A modular construction micro-reactor with parallel microchannels on fluid guide plates for chemical reactions, but not for evaporation purposes is known. A modular construction falling film evaporator is disclosed, comprising a stack of alternate gap-like evaporation chambers and sheet-like evaporator modules with an assembly of parallel microchannels, whereby the evaporation chambers are open above and/or below across the whole width of the module and the stack is arranged in a container. The falling film evaporator is used in a method for obtaining a gaseous phase from a liquid medium on a technical scale and is suitable for the concentration of thermolabile solutions and rapidly adjustable production of a gas stream.
摘要翻译： 具有用于化学反应但不用于蒸发目的的流体引导板上具有平行微通道的模块化结构微反应器是已知的。 公开了一种模块化结构降膜蒸发器，其包括一组交替的间隙式蒸发室和具有平行微通道组件的片状蒸发器模块，由此蒸发室在模块的整个宽度上方和/或下方敞开 并且堆叠被布置在容器中。 降膜蒸发器用于在技术规模上从液体介质获得气相的方法，适用于浓缩不溶热溶液并快速调节气流的产生。
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公开(公告)号：US06476277B2
公开(公告)日：2002-11-05
申请号：US09915079
申请日：2001-07-24
申请人： Bernd Vogel , Elias Klemm , Mathias Seitz , Jochen Heller , Jörg Reiser
发明人： Bernd Vogel , Elias Klemm , Mathias Seitz , Jochen Heller , Jörg Reiser
IPC分类号： C07C3700
CPC分类号： C07C37/60 , Y10S977/775 , Y10S977/776 , Y10S977/779 , Y10S977/84 , Y10S977/896 , C07C39/07
摘要： The present invention relates to a process for preparing hydroxyaromatics by oxidizing aromatics with dinitrogen monoxide in the gas phase in the presence of nanocrystalline zeolites.
摘要翻译： 本发明涉及通过在纳米晶体沸石存在下在气相中用一氧化二氮氧化芳族化合物来制备羟基芳族化合物的方法。
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公开(公告)号：US07678361B2
公开(公告)日：2010-03-16
申请号：US10553312
申请日：2004-03-31
申请人： Georg Markowz , Johannes Albrecht , Johannes Ehrlich , Michael Jucys , Elias Klemm , Armin Lange De Oliveira , Reinhard Machnik , Juergen Rapp , Ruediger Schuette , Steffen Schirrmeister , Olaf Von Morstein , Hartmut Hederer , Martin Schmitz-Niederau
发明人： Georg Markowz , Johannes Albrecht , Johannes Ehrlich , Michael Jucys , Elias Klemm , Armin Lange De Oliveira , Reinhard Machnik , Juergen Rapp , Ruediger Schuette , Steffen Schirrmeister , Olaf Von Morstein , Hartmut Hederer , Martin Schmitz-Niederau
IPC分类号： B01J19/24 , C01B15/029 , C07C27/00 , C07C27/12 , C07C39/04 , C07C27/06 , C07D301/12
CPC分类号： B01F5/0471 , B01F13/0059 , B01F2005/0034 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00889
摘要： The present invention discloses a microreactor for performing heterogeneous catalytic reactions, being of plate or stack construction for industrial use, with provision made for chambers between the plates for the chemical reaction and for the heat removal. Inside the reaction chambers, catalyst material is applied to the internal walls or filled into recesses, and in all chambers there are spacers. In particular the slot-shaped reaction chambers have channels with a hydraulic diameter smaller than 1500 μm and a ratio of free slot width to free slot height in the range of 10 to 450.
摘要翻译： 本发明公开了一种用于进行非均相催化反应的微反应器，它是用于工业应用的板或堆叠结构，为用于化学反应和排热的板之间的室提供。 在反应室内部，将催化剂材料施加到内壁或填充到凹部中，并且在所有室中都存在间隔物。 特别地，槽形反应室具有水力直径小于1500μm的通道，并且自由槽宽度与自由槽高度的比率在10至450的范围内。
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