摘要:
In producing zirconia powder by desiliconizing heat treatment of a mixture of zircon powder and a powdery carbon-containing material, optionally with addition of a zirconia stabilizing oxide such as calcia or yttria, in a nonoxidizing atmosphere the conversion of silica into SiO and dissipation of gaseous SiO are promoted and completed by performing the heat treatment under reduced pressure, viz. at a pressure not higher than 0.6 atm. Zirconia powder of very high purity can surely be obtained, even when a large batch of the raw material mixture is treated, by performing the reduced pressure desiliconizing heat treatment in two stages: first at 1200.degree.-1550.degree. C. until almost complete conversion of silica to SiO and then at 1550.degree.-2000.degree. C. The mole ratio of C to SiO.sub.2 in the raw material mixture must be 0.4-2.0. For further enhancement of purity, zirconia powder obtained by the desiliconizing treatment may be subjected to oxidation heat treatment. Efficiency of the desiliconizing heat treatment can be enhanced by precedingly forming the raw material mixture into porous lump(s) whose bulk density is in the range from 0.7 to 2.0.
摘要:
A system for manufacturing fine-grained SiO powder includes means for heating a mixture of an SiO.sub.2 containing material and an Si and/or C containing material for generating SiO vapor, and for condensing the generated SiO vapor from a gaseous state in the presence of non-oxidizing gas and under substantially low pressure. Preferably, vacuum is maintained at the position where thermal reaction generates SiO vapor. Non-oxidizing gas serves for transferring vapor-state SiO and/or fine-grained SiO powder to an SiO collection chamber. This successfully prevents the SiO from being accumulated within a transfer pipe or duct and thus prevents the pipe or duct from being blocked. Furthermore, substantially low pressure (vacuum) atmosphere encourages SiO vapor generation from the reagent mixture and thus permits a lower heating temperature to cause SiO vapor generation.
摘要:
As to a method of producing grain oriented silicon steel sheets used in stacked lamination-core transformers, which realizes the improvement of magnetic properties, particularly extreme reduction of iron loss irrespectively of a high temperature heat treatment such as strain relief annealing and can attain the improvement of compressive stress dependence of magnetostriction and lamination factor, it is a main point that the steel sheet after the finish annealing is provided on its surface with a thin coat of at least one layer composed mainly of nitrides and carbides of Ti, Zr, Hf, V, Nb, Ta, Mn, Cr, Mo, W, Co, Ni, Al, B and Si and strongly adhered to the surface of the steel sheet through a mixed layer of base metal and thin coat.
摘要:
A mold for molding an industrial product from a powder by slip casting, which has good water-absorptivity, long life, high strength and excellent mold-releasability and is constituted from a composite base material of boron nitride and other ceramic constituents. With this mold, molding of ceramic products and the like can be performed with high efficiency without causing clogging.
摘要:
A cathode material for use in a lithium secondary battery of excellent thermal stability contributing to the improvement of safety of the battery and having large discharging capacity, as well as a method of manufacturing the cathode material for use in the lithium secondary battery, based on the improved method for measuring the thermal stability of the cathode material, the cathode material comprising a compound represented by the chemical formula: LixNiyCozMmO2 in which the material is powdery and the BET specific surface area is 0.8 m2/g or less, M in the chemical formula represents one or more of element selected from Ba, Sr and B, and x, y, z and m are, respectively, 0.9≦x≦1.1, 0.5≦y≦0.95, 0.05≦z≦0.5 and 0.0005≦m≦0.02.
摘要翻译:一种用于锂二次电池的阴极材料,具有良好的热稳定性,有助于提高电池的安全性并具有大的放电容量,以及一种制造用于锂二次电池的阴极材料的方法,基于 用于测量阴极材料的热稳定性的改进方法,阴极材料包含由化学式:LixNiyCozMmO2表示的化合物,其中材料是粉末,BET比表面积为0.8m 2 / g以下,化学式M 表示选自Ba,Sr和B中的一种或多种元素,x,y,z和m分别为0.9 <= x <=1.1,0.5≤y≤0.95,0.05≤z≤0.5和 0.0005 <= m <= 0.02。
摘要:
A substrate for print circuit board comprising a steel sheet, a forsterite film layer formed on at least one surface of the steel sheet, and an insulating film layer formed on the forsterite film layer by baking a coating solution mainly consisting of a phosphate and colloidal silica. A print circuit board having a conductive pattern on the insulating film layer of the substrate for print circuit board, and methods of manufacturing the substrate and the print circuit board. One of typical methods of manufacturing the substrate for print circuit board comprises steps of applying an annealing separator mainly consisting of MgO on the steel sheet and annealing it to form a forsterite film layer, applying and baking a coating solution mainly consisting of the phosphate and colloidal silica onto the forsterite film layer to form an insulating film layer. The print circuit board is obtained by bonding the conductive pattern to the insulating film layer and annealing at a temperature range of not lower than 300.degree. C. but lower than 1,050.degree. C.
摘要:
A heat-resistant insulating coating having a high adhesion can be formed on an oriented silicon steel sheet by the use of an aqueous coating dispersion containing colloidal silica dispersed therein, at least one of monobasic phosphates of Mg, Al, Sr, Ba and Fe, at least one compound selected from chromic acid anhydride, chromate and dichromate, and at least one fine particle oxide selected from SiO.sub.2, Al.sub.2 O.sub.3 and TiO.sub.2 having a primary particle size of 70-500A and an apparent density of not higher than 100 g/l. The steel sheet having the coating is low in the iron loss and magnetostriction and shows good heat-resistant property.
摘要翻译:可以通过使用分散有胶体二氧化硅的水性涂料分散体,Mg,Al,Sr,Ba,Fe的一价磷酸盐中的至少一种,在取向硅钢板上形成粘合性高的耐热绝缘涂层, 至少一种选自铬酸酐,铬酸盐和重铬酸盐的化合物和至少一种选自SiO 2,Al 2 O 3和TiO 2的细颗粒氧化物,其一次粒径为70-500A,表观密度不高于100g / l。 具有该涂层的钢板的铁损和磁致伸缩性低,表现出良好的耐热性。