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1.发明申请PROCESS FOR HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION OF AT LEAST ONE ORGANIC STARTING COMPOUND 有权用于异源催化气相的方法部分氧化至少一种有机起始化合物公开(公告)号：US20070155988A1
公开(公告)日：2007-07-05
申请号：US11612824
申请日：2006-12-19
IPC分类号： C07C51/16
CPC分类号： C07C51/252 , B01J8/067 , B01J23/002 , B01J23/24 , B01J23/887 , B01J23/92 , B01J35/0006 , B01J2208/00221 , B01J2208/025 , B01J2523/00 , C07C45/35 , C07C51/215 , Y02P20/584 , C07C57/04 , C07C47/22 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/27 , B01J2523/51 , B01J2523/847
摘要： A process for heterogeneously catalyzed gas phase partial oxidation of an organic starting compound over a fixed catalyst bed freshly installed into a reaction chamber, in which the reduction in the quality of the fixed catalyst bed is restored with increasing operating time by replacing a portion of the fixed catalyst bed by a replacement fixed catalyst bed part whose volume-specific activity is lower than the volume-specific activity of the replaced fixed catalyst bed part in its freshly installed state.
摘要翻译： 一种在新鲜安装到反应室中的固定催化剂床上的有机起始化合物的非均相催化气相部分氧化的方法，其中固定催化剂床的质量的降低通过增加操作时间而恢复， 固定催化剂床通过替代的固定催化剂床部分，其体积比活度低于其新安装状态下更换的固定催化剂床部分的体积比活性。
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2.发明申请PROCESS FOR STARTING-UP A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF ACROLEIN TO ACRYLIC ACID OR OF METHACROLEIN TO METHACRYLIC ACID 有权将异丙烯酸异丙酯与甲基丙烯酸异丙酯气相氧化反应进行甲基丙烯酸的方法公开(公告)号：US20080269521A1
公开(公告)日：2008-10-30
申请号：US12107420
申请日：2008-04-22
申请人： Ulrich HAMMON , Thorsten Friese , Jochen Petzoldt , Klaus Joachim Muller-Engel , Ulrich Cremer , Andreas Raichle
发明人： Ulrich HAMMON , Thorsten Friese , Jochen Petzoldt , Klaus Joachim Muller-Engel , Ulrich Cremer , Andreas Raichle
IPC分类号： C07C51/235
CPC分类号： B01J8/067 , B01J23/002 , B01J23/8885 , B01J27/199 , B01J35/0006 , B01J2208/00212 , B01J2208/00221 , B01J2208/00513 , B01J2208/025 , B01J2219/30207 , B01J2219/30215 , B01J2523/00 , C07C51/235 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/17 , B01J2523/55 , B01J2523/15 , B01J2523/51 , B01J2523/53 , B01J2523/62
摘要： A process for starting-up a heterogeneously catalyzed partial gas phase oxidation of acrolein to acrylic acid or of methacrolein to methacrylic acid over a fixed catalyst bed disposed in a tube bundle reactor cooled by a heat exchange medium, wherein the temperature of the heat exchange medium is ≧290° C. and the temperature of that reactor plate surface which faces the reaction gas entry mixture and the temperature of the reaction gas entry mixture itself are ≦285° C.
摘要翻译： 一种在由热交换介质冷却的管束反应器中的固定催化剂床上启动丙烯醛异丙烯醛至丙烯醛或甲基丙烯醛至甲基丙烯酸的非均相催化部分气相氧化方法，其中热交换介质的温度 > 290℃，反应器板表面的面对反应气体进入混合物的温度和反应气体进入混合物本身的温度<285℃。
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3.发明申请APPARATUS FOR LONG-TERM OPERATION OF A HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION OF AT LEAST ONE ORGANIC COMPOUND 审中-公开用于长时间操作异源催化气相的装置相对于至少一种有机化合物的部分氧化公开(公告)号：US20080187467A1
公开(公告)日：2008-08-07
申请号：US12043417
申请日：2008-03-06
IPC分类号： B01J19/24
CPC分类号： B01J8/0285 , B01J2208/00061 , B01J2208/00539 , C07B41/00 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： Apparatus for the long-term operation of a heterogeneously catalyzed gas phase partial oxidation of at least one organic compound over a catalyst bed, in which, in order to counteract the deactivation of the catalyst bed, the working pressure in the gas phase is increased during the operating time of the catalyst bed.
摘要翻译： 用于在催化剂床上长期运行至少一种有机化合物的非均相催化气相部分氧化的装置，其中为了抵消催化剂床的失活，气相中的工作压力在 催化剂床的操作时间。
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4.发明申请PROCESS FOR PREPARING AT LEAST ONE ORGANIC TARGET COMPOUND BY HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION 有权通过异源催化气相部分氧化制备至少一种有机靶化合物的方法公开(公告)号：US20080260605A1
公开(公告)日：2008-10-23
申请号：US12146807
申请日：2008-06-26
IPC分类号： B01J19/00
CPC分类号： C07C51/252 , C07C57/04
摘要： A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalysts charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line.
摘要翻译： 通过在两个平行操作的氧化反应器管线中的有机前体化合物与分子氧的非均相催化气相部分氧化来制备有机靶化合物的方法，并且从处理线中的产物气流的混合物中除去目标化合物， 其中氧化线之一的催化剂装料包括一部分催化剂，其上已经进行非均相催化的气相部分氧化比在另一个氧化反应器管线的催化剂装料的催化剂的部分长。
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5.发明申请PROCESS FOR TRANSPORTING IN THE TANK OF A TANK TRUCK OR TANKER SHIP A LIQUID MONOMER PHASE WITHDRAWN FROM A STORAGE VESSEL 有权运输在坦克卡车或坦克的油罐的过程从储存船运送液体单体相公开(公告)号：US20080234446A1
公开(公告)日：2008-09-25
申请号：US12053158
申请日：2008-03-21
CPC分类号： C07C45/79 , C07C45/78 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , C07C67/62 , C07C47/22 , C07C57/04 , C07C69/54
摘要： A process for transporting a liquid monomer phase which has been withdrawn from a storage vessel and comprises methacrylic monomers to an extent of ≧90% by weight, in a tank truck or in a tanker ship, in which the liquid monomer phase is subjected to a separating operation on the route from the storage vessel into the tank of a tank truck or of a tanker ship in order to separate polymer of the monomer present in dissolved form in the liquid monomer phase.
摘要翻译： 运输液体单体相的方法，该液体单体相已经从储存容器中取出并且包含甲基丙烯酸单体至> 90重量％的程度，在油罐车或油罐船中，其中液体单体相经受 在从储存容器进入罐车或油罐船的罐的路线上的分离操作，以分离以溶解形式存在于液体单体相中的单体的聚合物。
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6.发明申请PROCESS FOR PURIFYING REMOVAL OF ACRYLIC ACID, METHACRYLIC ACID, N-VINYLPYRROLIDONE OR P-XYLENE CRYSTALS FROM THEIR SUSPENSION IN MOTHER LIQUOR 有权从母乳中悬浮液中除去丙烯酸，甲基丙烯酸，N-乙烯基吡咯烷酮或对二甲苯晶体的方法公开(公告)号：US20090018347A1
公开(公告)日：2009-01-15
申请号：US12170002
申请日：2008-07-09
IPC分类号： C07C7/14
CPC分类号： C07B63/00 , B01D9/0013 , B01D9/0036 , B01D9/004 , B01D9/0045 , C07C7/14 , C07C51/43 , C07C15/08 , C07C57/04
摘要： A process for purifying removal of acrylic acid, methacrylic acid, N-vinylpyrrolidone or p-xylene crystals from their suspension in mother liquor by means of a wash column with forced transport, whose shell of the process chamber is a metal wall, the wash column additionally being enveloped by a thermal insulation material having a water vapor barrier and a specific heat flow of >0.1 W/m2 and
摘要翻译： 一种通过强制运输的洗涤柱从母液中的悬浮液中除去丙烯酸，甲基丙烯酸，N-乙烯基吡咯烷酮或对二甲苯晶体的方法，其处理室的外壳是金属壁，洗涤柱 另外由具有水蒸气阻挡层和通过洗涤塔的金属壁流入处理室的> 0.1W / m 2和<10W / m 2的比热流的隔热材料包围。
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7.发明授权Process for storing a monomer phase which is liquid under the conditions of storage 有权在储存条件下储存液体的单体相的方法公开(公告)号：US07893178B2
公开(公告)日：2011-02-22
申请号：US12053268
申请日：2008-03-21
IPC分类号： C08F16/34 , C08F20/06 , C08F118/02 , F16K49/00 , F17D1/16 , F04B49/10 , F04B49/00 , C07C45/00 , C07C69/52 , C07C57/02
CPC分类号： C07C67/48 , C07C45/79 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , Y10T137/0391 , Y10T137/6579 , C07C57/04 , C07C69/54 , C07C47/22
摘要： A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed.
摘要翻译： 一种在储存条件下储存液体的单体相的方法，其包含甲基丙烯酸单体至95重量％的程度，并且通过在气相中冷凝或通过熔化结晶相获得，在储存容器 其中在从其产生到储存容器中的途径中，其中以液态单体相中溶解形式存在的单体的聚合物被从其中除去，以及从存在容器中的单体的聚合物的储存容器中取出液体单体相的方法 在单体相中溶解形式同样被除去。
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8.发明申请PROCESS FOR OPERATING A CONTINUOUS REMOVAL OF A TARGET PRODUCT X IN THE FORM OF FINE CRYSTALS 有权在精细晶体形式下连续移除目标产品X的过程公开(公告)号：US20090076286A1
公开(公告)日：2009-03-19
申请号：US12208737
申请日：2008-09-11
IPC分类号： C07C7/14 , C07C51/43 , C07D207/267
CPC分类号： B01D9/0013 , B01D9/004 , B01D9/005 , B01D9/0063 , C07C7/14 , C07C51/43 , C07C15/08 , C07C57/04
摘要： A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferee, in which the crystal suspension formed is conducted out of the heat transferer first into a mixed buffer tank and, from there, fed to an apparatus for separating the crystal suspension into crystals and liquid phase, and wherein external measures dissipade the oversaturation of the crystal suspension fed to the buffer vessel with target product X.
摘要翻译： 通过在间接热转移体中冷却悬浮液结晶，从包含目标产物X和除了目标产物X的成分的液相P连续除去目标产物X的形式的方法，其中形成的晶体悬浮液为 首先从热转移器中导出到混合缓冲罐中，从那里进料到用于将晶体悬浮液分离成晶体和液相的装置，并且其中外部措施消除了用目标物供给缓冲容器的晶体悬浮液的过饱和 产品X.
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9.发明申请PROCESS FOR OPERATING A CONTINUOUS REMOVAL OF A TARGET PRODUCT X IN THE FORM OF FINE CRYSTALS OF THE TARGET PRODUCT X 有权在目标产品X的精细晶体形式下连续移除目标产品X的过程X公开(公告)号：US20090076232A1
公开(公告)日：2009-03-19
申请号：US12208559
申请日：2008-09-11
IPC分类号： C07C51/43 , C07C7/14 , C07D207/00 , C08F2/00
CPC分类号： B01D9/0009 , B01D9/0013 , B01D9/005 , B01D9/0063 , C07C51/43 , C07C57/04
摘要： A process for operating a continuous removal of a target product X in the form of fine crystals of a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in the secondary chamber of an indirect heat exchanger to which liquid phase P flows continuously with simultaneous continuous flow through the primary chamber of the indirect heat exchanger with a coolant, and continuous withdrawal of a crystal suspension S having a degree of crystallization Y from the secondary chamber in two operating states I and II, wherein the coolant temperature is lower, the mass flow of liquid phase P is greater and the molar proportion of the constituents other than the target product X in the liquid phase P in operating state II is greater than in operating state I.
摘要翻译： 通过在间接热交换器的二次室中冷却悬浮液结晶来操作以含有目标产物X和除了目标产物X的成分的液相P的细晶体的形式连续除去目标产物X的方法， 该液相P以连续的流动方式连续流过间接热交换器的主室，并具有冷却剂，并且在两个操作状态I和II中连续取出具有结晶Y的程度的结晶悬浮液， 冷却剂温度较低，液相P的质量流量较大，并且在运行状态II下的液相P中除目标产物X以外的成分的摩尔比例大于运行状态I.
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10.发明申请PROCESS FOR STORING A MONOMER PHASE WHICH IS LIQUID UNDER THE CONDITIONS OF STORAGE 有权存储根据存储条件液化的单体相的过程公开(公告)号：US20090221780A1
公开(公告)日：2009-09-03
申请号：US12053268
申请日：2008-03-21
CPC分类号： C07C67/48 , C07C45/79 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , Y10T137/0391 , Y10T137/6579 , C07C57/04 , C07C69/54 , C07C47/22
摘要： A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed.
摘要翻译： 一种在储存条件下储存液体的单体相的方法，其包含甲基丙烯酸单体至> 95重量％的程度，并且通过在气相中冷凝或熔融结晶相获得， 容器，其中以其溶解形式存在于液体单体相中的单体的聚合物在其从其产生进入储存容器的路线上被除去，以及从存储容器中抽出液体单体相的方法，其中单体的聚合物 在单体相中以溶解形式存在，同样地被除去。
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