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    Method of forming regenerated carbohydrates with solvent systems based on molten ionic liquids
    1.
    发明授权
    Method of forming regenerated carbohydrates with solvent systems based on molten ionic liquids 有权
    用基于熔融离子液体的溶剂体系形成再生碳水化合物的方法

    公开(公告)号：US08163215B2

    公开(公告)日：2012-04-24

    申请号：US12158869

    申请日：2006-12-22

    申请人： Veit Stegmann ,  Klemens Massonne ,  Matthias Maase ,  Eric Uerdingen ,  Michael Lutz ,  Frank Hermanutz ,  Frank Gaehr

    发明人： Veit Stegmann ,  Klemens Massonne ,  Matthias Maase ,  Eric Uerdingen ,  Michael Lutz ,  Frank Hermanutz ,  Frank Gaehr

    IPC分类号： D01F2/24 ,  D01D5/04 ,  B29C47/00 ,  C08B16/00 ,  C07H1/00 ,  B32B23/00

    CPC分类号： D01F2/02 ,  C08B1/003 ,  C08B16/00 ,  C08J3/096 ,  C08J2301/02 ,  C08L1/02 ,  C08L3/00 ,  C08L3/02 ,  C08L3/12 ,  C08L5/08 ,  Y02P20/542 ,  Y10T428/2965 ,  C08L2666/26

    摘要： A solution system for biopolymers in the form of carbohydrates based on a molten ionic liquid, additives optionally being contained in the solution system, is described. This solution system contains a protic solvent or a mixture of several protic solvents, and in the case where the protic solvent is solely water, this is present in the solution system in an amount of more than about 5 wt. %. Carbohydrates can be incorporated into the solution system, in particular in the form of starch, cellulose and derivatives thereof, and it can then be used for regeneration of the carbohydrates contained therein. A particularly advantageous process for the preparation of the solution system containing the carbohydrates and for the preparation of regenerated carbohydrates, in particular in the form of regenerated cellulose fibers, is moreover described. The invention accordingly also provides such spun fibers as are distinguished in that they are non-fibrillating. The invention offers in particular economic advantages over the systems of the prior art.

    摘要翻译： 描述了基于熔融离子液体的碳水化合物形式的生物聚合物的溶液系统，任选地包含在溶液体系中的添加剂。 该溶液系统含有质子溶剂或几种质子溶剂的混合物，在质子溶剂仅为水的情况下，溶液体系中的溶解体积大于约5wt。 ％ 碳水化合物可以并入溶液体系中，特别是淀粉，纤维素及其衍生物的形式，然后可以用于其中所含的碳水化合物的再生。 此外，还描述了制备含有碳水化合物和用于制备再生碳水化合物，特别是再生纤维素纤维形式的溶液体系的特别有利的方法。 因此，本发明还提供了这样的纺丝纤维，其特征在于它们是非原纤化的。 本发明相对于现有技术的系统提供了特别的经济优势。

    Solvent System Based on Molten Ionic Liquids, Its Production and Use for Producing Regenerated Carbohydrates
    2.
    发明申请
    Solvent System Based on Molten Ionic Liquids, Its Production and Use for Producing Regenerated Carbohydrates 有权
    基于熔融离子液体的溶剂体系，其生产和用于生产再生碳水化合物

    公开(公告)号：US20080269477A1

    公开(公告)日：2008-10-30

    申请号：US12158869

    申请日：2006-12-22

    申请人： Veit Stegmann ,  Klemens Massonne ,  Matthias Maase ,  Eric Uerdingen ,  Michael Lutz ,  Frank Hermanutz ,  Frank Gaehr

    发明人： Veit Stegmann ,  Klemens Massonne ,  Matthias Maase ,  Eric Uerdingen ,  Michael Lutz ,  Frank Hermanutz ,  Frank Gaehr

    IPC分类号： C08B16/00

    CPC分类号： D01F2/02 ,  C08B1/003 ,  C08B16/00 ,  C08J3/096 ,  C08J2301/02 ,  C08L1/02 ,  C08L3/00 ,  C08L3/02 ,  C08L3/12 ,  C08L5/08 ,  Y02P20/542 ,  Y10T428/2965 ,  C08L2666/26

    摘要： A solution system for biopolymers in the form of carbohydrates based on a molten ionic liquid, additives optionally being contained in the solution system, is described. This solution system contains a protic solvent or a mixture of several protic solvents, and in the case where the protic solvent is solely water, this is present in the solution system in an amount of more than about 5 wt. %. Carbohydrates can be incorporated into the solution system, in particular in the form of starch, cellulose and derivatives thereof, and it can then be used for regeneration of the carbohydrates contained therein. A particularly advantageous process for the preparation of the solution system containing the carbohydrates and for the preparation of regenerated carbohydrates, in particular in the form of regenerated cellulose fibers, is moreover described. The invention accordingly also provides such spun fibers as are distinguished in that they are non-fibrillating. The invention offers in particular economic advantages over the systems of the prior art.

    摘要翻译： 描述了基于熔融离子液体的碳水化合物形式的生物聚合物的溶液系统，任选地包含在溶液体系中的添加剂。 该溶液系统含有质子溶剂或几种质子溶剂的混合物，在质子溶剂仅为水的情况下，溶液体系中的溶解体积大于约5wt。 ％。 碳水化合物可以并入溶液体系中，特别是淀粉，纤维素及其衍生物的形式，然后可以用于其中所含的碳水化合物的再生。 此外，还描述了制备含有碳水化合物和用于制备再生碳水化合物，特别是再生纤维素纤维形式的溶液体系的特别有利的方法。 因此，本发明还提供了这样的纺丝纤维，其特征在于它们是非原纤化的。 本发明相对于现有技术的系统提供了特别的经济优势。

    Method for producing regenerated biopolymers and regenerated products obtained by said method
    3.
    发明授权
    Method for producing regenerated biopolymers and regenerated products obtained by said method 有权
    通过所述方法制备再生生物聚合物和再生产品的方法

    公开(公告)号：US08841441B2

    公开(公告)日：2014-09-23

    申请号：US12742593

    申请日：2008-11-13

    申请人： Eric Uerdingen ,  Michael Siemer ,  Michael Lutz ,  Thomas Wisniewski ,  Frank Hermanutz ,  Frank Gaehr

    发明人： Eric Uerdingen ,  Michael Siemer ,  Michael Lutz ,  Thomas Wisniewski ,  Frank Hermanutz ,  Frank Gaehr

    IPC分类号： C07H1/06 ,  C07H1/08 ,  C08B31/00 ,  C08B33/00 ,  C08B35/00 ,  C08B1/00

    CPC分类号： D01F2/02 ,  C08B1/003 ,  C08B16/00 ,  C08L1/02 ,  C08L1/08 ,  C08L1/10 ,  C08L1/26 ,  C08L3/02 ,  C08L3/06 ,  C08L3/08 ,  D01D5/06 ,  Y02P20/542

    摘要： The invention relates to a method for producing regenerated biopolymers in the form of carbohydrates, using a solvent system that contains the biopolymers dissolved therein. The solvent system is based on a melted ionic liquid and optionally a protic solvent or a mixture thereof. The biopolymers dissolved in the solvent system are precipitated in a coagulation medium, said medium comprising a protic coagulant or a mixture of protic coagulants. The method according to the invention is characterized in that the surface tension σ of the coagulant or the mixture of coagulants is 99% to 30% of the surface tension σ of water, the surface tension being measured according to ASTM D 1590-60 at a temperature of 50° C. The method according to the invention is economical and flexible and leads to advantageous products, especially in the form of staple fibers which are especially not fibrillated and have an advantageous wet to dry strength ratio.

    摘要翻译： 本发明涉及使用含有溶解于其中的生物聚合物的溶剂系统生产碳水化合物形式的再生生物聚合物的方法。 溶剂体系基于熔融的离子液体和任选的质子溶剂或其混合物。 溶解在溶剂体系中的生物聚合物在凝固介质中沉淀，所述介质包含质子凝结剂或质子凝结剂的混合物。 根据本发明的方法，其特征在于表面张力＆ 的凝结剂或絮凝剂的混合物是表面张力的99％至30％ 的水，表面张力根据ASTM D 1590-60在50℃的温度下测量。根据本发明的方法是经济的和柔性的，并且导致有利的产品，特别是以短纤维的形式，特别是不是 原纤化并且具有有利的湿 - 干强度比。

    METHOD FOR PRODUCING REGENERATED BIOPOLYMERS AND REGENERATED PRODUCTS OBTAINED BY SAID METHOD
    4.
    发明申请
    METHOD FOR PRODUCING REGENERATED BIOPOLYMERS AND REGENERATED PRODUCTS OBTAINED BY SAID METHOD 有权
    生产再生型生物聚合物的方法和由方法获得的再生产品的方法

    公开(公告)号：US20100256352A1

    公开(公告)日：2010-10-07

    申请号：US12742593

    申请日：2008-11-13

    申请人： Eric Uerdingen ,  Michael Siemer ,  Michael Lutz ,  Thomas Wisniewski ,  Frank Hermanutz ,  Frank Gaehr

    发明人： Eric Uerdingen ,  Michael Siemer ,  Michael Lutz ,  Thomas Wisniewski ,  Frank Hermanutz ,  Frank Gaehr

    IPC分类号： C08B1/00 ,  C08B30/04 ,  D01F2/02

    CPC分类号： D01F2/02 ,  C08B1/003 ,  C08B16/00 ,  C08L1/02 ,  C08L1/08 ,  C08L1/10 ,  C08L1/26 ,  C08L3/02 ,  C08L3/06 ,  C08L3/08 ,  D01D5/06 ,  Y02P20/542

    摘要： The invention relates to a method for producing regenerated biopolymers in the form of carbohydrates, using a solvent system that contains the biopolymers dissolved therein. The solvent system is based on a melted ionic liquid and optionally a protic solvent or a mixture thereof. The biopolymers dissolved in the solvent system are precipitated in a coagulation medium, said medium comprising a protic coagulant or a mixture of protic coagulants. The method according to the invention is characterized in that the surface tension a of the coagulant or the mixture of coagulants is 99% to 30% of the surface tension a of water, the surface tension being measured according to ASTM D 1590-60 at a temperature of 50° C. The method according to the invention is economical and flexible and leads to advantageous products, especially in the form of staple fibers which are especially not fibrillated and have an advantageous wet to dry strength ratio.

    摘要翻译： 本发明涉及使用含有溶解于其中的生物聚合物的溶剂系统生产碳水化合物形式的再生生物聚合物的方法。 溶剂系统基于熔融的离子液体和任选的质子溶剂或其混合物。 溶解在溶剂体系中的生物聚合物在凝固介质中沉淀，所述介质包含质子凝结剂或质子凝结剂的混合物。 根据本发明的方法的特征在于，凝结剂或凝结剂混合物的表面张力a为水的表面张力a的99％至30％，表面张力根据ASTM D 1590-60测量， 温度为50℃。根据本发明的方法是经济和灵活的，并且导致有利的产品，特别是以特别不原纤化并且具有有利的湿干比强度的短纤维的形式。

    PRODUCTION OF SPHERICAL PARTICLES FROM SOLUTIONS COMPRISING A WATER-MISCIBLE SOLVENT BY THE METHOD OF UNDERWATER PELLETIZATION
    5.
    发明申请
    PRODUCTION OF SPHERICAL PARTICLES FROM SOLUTIONS COMPRISING A WATER-MISCIBLE SOLVENT BY THE METHOD OF UNDERWATER PELLETIZATION 审中-公开
    通过水下释放方法生产包含水不溶性溶剂的溶液的球形颗粒

    公开(公告)号：US20100297445A1

    公开(公告)日：2010-11-25

    申请号：US12744265

    申请日：2008-11-20

    申请人： Norbert Guentherberg ,  Karl-Peter Farwerck ,  Armin Kurps ,  Daniel Barrera-Medrano ,  Eric Uerdingen ,  Veit Stegmann ,  Michael Lutz

    发明人： Norbert Guentherberg ,  Karl-Peter Farwerck ,  Armin Kurps ,  Daniel Barrera-Medrano ,  Eric Uerdingen ,  Veit Stegmann ,  Michael Lutz

    IPC分类号： C08G75/20 ,  C08B1/00 ,  B29C47/00

    CPC分类号： C08J3/09 ,  C08J3/12 ,  C08J2301/02 ,  Y10T428/2982

    摘要： The present invention relates to a process for producing spherical particles of at least one material, which comprises the steps: (A) preparation of a solution or dispersion of the at least one material in at least one water-miscible solvent or dispersion medium, (B) conversion of the solution or dispersion obtained in step (A) into individual portions comprising an amount of the at least one material corresponding to the amount present in the spherical particles by underwater pelletization and (C) introduction of the portions obtained in step (B) into a medium which is miscible with the solvent or dispersion medium from step (A) and in which the material used in step (A) is insoluble so that the solvent or dispersion medium used in step (A) is replaced by the medium which is miscible with the solvent or dispersion medium from step (A) and the material solidifies to form the spherical particle.

    摘要翻译： 本发明涉及一种制备至少一种材料的球形颗粒的方法，其包括以下步骤：（A）在至少一种水混溶性溶剂或分散介质中制备所述至少一种材料的溶液或分散体（ B）将步骤（A）中获得的溶液或分散体转化成包含一定量的至少一种与球形颗粒中存在的量相对应的材料的水溶液造粒和（C）将步骤 B）进入与步骤（A）的溶剂或分散介质混溶的介质，其中步骤（A）中使用的材料是不溶的，使得步骤（A）中使用的溶剂或分散介质被介质 其与来自步骤（A）的溶剂或分散介质混溶，并且材料固化以形成球形颗粒。