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1.发明授权Scratch resistant coated glass article including layer(s) resistant to fluoride-based etchant(s), and method of making article using combustion CVD 失效包括耐氟化物蚀刻剂的层的耐划伤涂层玻璃制品以及使用燃烧CVD制备制品的方法公开(公告)号：US07824772B2
公开(公告)日：2010-11-02
申请号：US12149334
申请日：2008-04-30
IPC分类号： B32B9/00
CPC分类号： C23C14/06 , C03C17/22 , C03C17/225 , C03C17/23 , C03C17/245 , C03C17/2453 , C03C17/3417 , C03C17/3435 , C03C17/3441 , C03C17/3452 , C03C2217/215 , C03C2217/218 , C03C2217/228 , C03C2217/281 , C03C2217/282 , C03C2217/285 , C03C2218/15 , C03C2218/154 , C23C14/024 , C23C14/0635 , C23C14/08 , C23C14/086 , C23C14/58 , Y10T428/265 , Y10T428/30 , Y10T428/31612
摘要： A scratch resistant coated article is provided which is also resistant to attacks by at least some fluoride-based etchant(s) for at least a period of time. In certain example embodiments, an anti-etch layer(s) is provided on a glass substrate in order to protect the glass substrate from attacks by fluoride-based etchant(s), and an underlayer(s) deposited by flame pyrolysis may be provided under at least the anti-etch layer(s).
摘要翻译： 提供了耐刮擦涂层制品，其还耐受至少一些基于氟化物的蚀刻剂至少一段时间的攻击。 在某些示例性实施例中，在玻璃基板上提供防蚀刻层，以便保护玻璃基板免受基于氟化物的蚀刻剂的攻击，并且可以提供通过火焰热解沉积的底层 在至少一个或多个抗蚀刻层之下。
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公开(公告)号：US07510786B2
公开(公告)日：2009-03-31
申请号：US11389162
申请日：2006-03-27
IPC分类号： B32B9/04
CPC分类号： C23C14/5833 , C03C17/22 , C03C17/2456 , C03C2217/212 , C03C2217/282 , C03C2218/154 , C03C2218/32 , C23C14/06 , C23C14/083 , C23C14/48 , Y10T428/30 , Y10T428/31
摘要： A coated article is provided which includes a layer including titanium oxycarbide. In order to form the coated article, a layer of titanium oxide is deposited on a substrate by sputtering or the like. After sputtering of the layer including titanium oxide, an ion beam source(s) is used to implant at least carbon ions into the titanium oxide. When implanting, the carbon ions have sufficient ion energy so as to knock off oxygen (0) from TiOx molecules so as to enable a substantially continuous layer comprising titanium oxycarbide to form near a surface of the previously sputtered layer.
摘要翻译： 提供了包括包含碳氧化钛的层的涂覆制品。 为了形成被覆制品，通过溅射等将氧化钛层沉积在基板上。 在溅射包括氧化钛的层之后，使用离子束源至少将碳离子注入到氧化钛中。 当注入时，碳离子具有足够的离子能量，从而从TiOx分子中除去氧（0），以使得能够在先前溅射层的表面附近形成包含碳氧化钛的基本连续的层。
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3.发明授权Method of manufacturing windshield using ion beam milling of glass substrate(s) 失效使用玻璃基板的离子束铣削制造挡风玻璃的方法公开(公告)号：US06740211B2
公开(公告)日：2004-05-25
申请号：US10074685
申请日：2002-02-14
申请人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
发明人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
IPC分类号： C23C1434
CPC分类号： C03C17/3618 , B32B17/10036 , B32B17/10174 , B32B17/10981 , C03C17/22 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C23/006 , C03C2217/282 , C03C2218/31 , C03C2218/32 , C03C2218/36 , C03C2218/365 , Y10T156/1028 , Y10T428/24628 , Y10T428/315 , Y10T428/31623 , Y10T428/3163
摘要： This invention relates to a method of making a laminated window such as a vehicle windshield. At least one of the two glass substrates of the window is ion beam milled prior to heat treatment and lamination. As a result, defects in the resulting window and/or haze may be reduced.
摘要翻译： 本发明涉及一种制造诸如车辆挡风玻璃的层压窗的方法。 在热处理和层压之前，窗口的两个玻璃基板中的至少一个是离子束研磨的。 结果，可能降低所得到的窗口和/或雾度中的缺陷。
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公开(公告)号：US07049003B2
公开(公告)日：2006-05-23
申请号：US10735869
申请日：2003-12-16
申请人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
发明人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
IPC分类号： B32B9/00
CPC分类号： C03C17/3618 , B32B17/10036 , B32B17/10174 , B32B17/10981 , C03C17/22 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C23/006 , C03C2217/282 , C03C2218/31 , C03C2218/32 , C03C2218/36 , C03C2218/365 , Y10T156/1028 , Y10T428/24628 , Y10T428/315 , Y10T428/31623 , Y10T428/3163
摘要： This invention relates to a method of making a laminated window such as a vehicle windshield. At least one of the two glass substrates of the window is ion beam milled prior to heat treatment and lamination. As a result, defects in the resulting window and/or haze may be reduced.
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5.发明授权公开(公告)号：US06808606B2
公开(公告)日：2004-10-26
申请号：US10238052
申请日：2002-09-10
申请人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Vijayen S. Veerasamy , Anthony V. Longobardo , Henry A. Luten , David R. Hall, Jr.
发明人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Vijayen S. Veerasamy , Anthony V. Longobardo , Henry A. Luten , David R. Hall, Jr.
IPC分类号： C23C1434
CPC分类号： C03C17/3618 , B05D5/083 , B08B17/06 , B08B17/065 , B32B17/10036 , B32B17/10174 , B32B17/1033 , B32B17/10761 , B32B17/10981 , B60S1/54 , B60S1/58 , C03C3/076 , C03C15/00 , C03C15/02 , C03C17/22 , C03C17/3441 , C03C17/36 , C03C17/3626 , C03C17/3634 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C17/42 , C03C19/00 , C03C23/0005 , C03C23/006 , C03C23/0075 , C03C2217/282 , C03C2218/151 , C03C2218/31 , C03C2218/32 , C03C2218/36 , C03C2218/365 , C23C16/26 , Y10T428/24612
摘要： This invention relates to a method of making a window (e.g., vehicle windshield, architectural window, etc.), and the resulting window product. At least one glass substrate of the window is ion beam treated and/or milled prior to application of a coating (e.g., sputter coated coating) over the treated/milled substrate surface and/or prior to heat treatment. As a result, defects in the resulting window and/or haze may be reduced. The ion beam used in certain embodiments may be diffused. In certain embodiments, the ion beam treating and/or milling is carried out using a fluorine (F) inclusive gas(es) and/or argon/oxygen gas(es) at the ion source(s). In certain optional embodiments, F may be subimplanted into to treated/milled glass surface for the purpose of reducing Na migration to the glass surface during heat treatment or thereafter, thereby enabling corrosion and/or stains to be reduced for long periods of time.
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6.发明申请Scratch resistant coated glass article including layer(s) resistant to fluoride-based etchant(s), and method of making article using combustion CVD 失效包括耐氟化物蚀刻剂的层的耐划伤涂层玻璃制品以及使用燃烧CVD制备制品的方法公开(公告)号：US20080226926A1
公开(公告)日：2008-09-18
申请号：US12149334
申请日：2008-04-30
IPC分类号： B32B17/06
CPC分类号： C23C14/06 , C03C17/22 , C03C17/225 , C03C17/23 , C03C17/245 , C03C17/2453 , C03C17/3417 , C03C17/3435 , C03C17/3441 , C03C17/3452 , C03C2217/215 , C03C2217/218 , C03C2217/228 , C03C2217/281 , C03C2217/282 , C03C2217/285 , C03C2218/15 , C03C2218/154 , C23C14/024 , C23C14/0635 , C23C14/08 , C23C14/086 , C23C14/58 , Y10T428/265 , Y10T428/30 , Y10T428/31612
摘要： A scratch resistant coated article is provided which is also resistant to attacks by at least some fluoride-based etchant(s) for at least a period of time. In certain example embodiments, an anti-etch layer(s) is provided on a glass substrate in order to protect the glass substrate from attacks by fluoride-based etchant(s), and an underlayer(s) deposited by flame pyrolysis may be provided under at least the anti-etch layer(s).
摘要翻译： 提供了耐刮擦涂层制品，其还耐受至少一些基于氟化物的蚀刻剂至少一段时间的攻击。 在某些示例性实施例中，在玻璃基板上提供防蚀刻层，以便保护玻璃基板免受基于氟化物的蚀刻剂的攻击，并且可以提供通过火焰热解沉积的底层 在至少一个或多个抗蚀刻层之下。
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公开(公告)号：US07052585B2
公开(公告)日：2006-05-30
申请号：US10384797
申请日：2003-03-11
CPC分类号： C23C14/5833 , C03C17/22 , C03C17/2456 , C03C2217/212 , C03C2217/282 , C03C2218/154 , C03C2218/32 , C23C14/06 , C23C14/083 , C23C14/48 , Y10T428/30 , Y10T428/31
摘要： A coated article is provided which includes a layer including titanium oxycarbide. In order to form the coated article, a layer of titanium oxide is deposited on a substrate by sputtering or the like. After sputtering of the layer including titanium oxide, an ion beam source(s) is used to implant at least carbon ions into the titanium oxide. When implanting, the carbon ions have sufficient ion energy so as to knock off oxygen (O) from TiOx molecules so as to enable a substantially continuous layer comprising titanium oxycarbide to form near a surface of the previously sputtered layer.
摘要翻译： 提供了包括包含碳氧化钛的层的涂覆制品。 为了形成被覆制品，通过溅射等将氧化钛层沉积在基板上。 在溅射包括氧化钛的层之后，使用离子束源至少将碳离子注入到氧化钛中。 当注入时，碳离子具有足够的离子能量以从TiO 2分子中分离出氧（O），从而使包含碳氧化钛的基本上连续的层能够形成在先前溅射的表面附近 层。
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公开(公告)号：US06764579B2
公开(公告)日：2004-07-20
申请号：US10242438
申请日：2002-09-13
IPC分类号： C23C1434
CPC分类号： C03C17/3618 , B05D5/083 , B08B17/06 , B08B17/065 , B32B17/1033 , B60S1/54 , B60S1/58 , C03C3/076 , C03C17/22 , C03C17/3441 , C03C17/3482 , C03C17/36 , C03C17/3621 , C03C17/3626 , C03C17/3634 , C03C17/3636 , C03C17/3644 , C03C17/3649 , C03C17/3652 , C03C17/3655 , C03C17/366 , C03C17/3681 , C03C17/42 , C03C23/0075 , C03C2217/282 , C03C2217/75 , C03C2217/76 , C03C2217/78 , C03C2218/151 , C03C2218/31 , C23C16/26 , G02B5/208 , Y10T428/30 , Y10T428/31504
摘要： A substrate is coated with a solar management coating system including at least one infrared (IR) reflective layer. A diamond-like carbon (DLC) inclusive protective coating system (e.g., including at least one highly tetrahedral amorphous carbon (ta-C) inclusive layer having sp3 carbon—carbon bonds) is provided on the substrate over at least the IR reflective layer in order to make the coating system scratch resistant, abrasion resistant, and generally mechanically durable. The DLC inclusive protective coating system may be hydrophobic, hydrophillic, or neutral in different embodiments of the invention. Optionally, at least one fluoro-alkyl silane (FAS) compound inclusive layer may be provided on the substrate over at least one of the DLC inclusive layer(s) in hydrophobic embodiments in order to increase contact angle &thgr; of the coated article.
摘要翻译： 衬底涂覆有包括至少一个红外（IR）反射层的太阳能管理涂层系统。 至少在IR上提供了包含金刚石碳（DLC）的保护涂层系统（例如，包括至少一个具有sp 3碳 - 碳键的高度四面体无定形碳（ta-C））层） 反射层，以使涂层体系耐划伤，耐磨损，并且通常机械耐久。 在本发明的不同实施方案中，含DLC的保护涂层体系可以是疏水的，亲水的或中性的。 任选地，在疏水性实施方案中，至少一种含氟烷基硅烷（FAS）化合物的层可以在至少一种含DLC的层中在衬底上提供，以增加涂覆制品的接触角θ。
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9.发明授权Method of making coated article including DLC inclusive layer over low-E coating 失效在低E涂层上制造包含DLC的层的涂层制品的方法公开(公告)号：US06663753B2
公开(公告)日：2003-12-16
申请号：US10175083
申请日：2002-06-20
IPC分类号： C23C1400
CPC分类号： C03C17/3618 , B05D5/083 , B08B17/06 , B08B17/065 , B32B17/1033 , B60S1/54 , B60S1/58 , C03C3/076 , C03C17/22 , C03C17/3441 , C03C17/3482 , C03C17/36 , C03C17/3621 , C03C17/3626 , C03C17/3634 , C03C17/3636 , C03C17/3644 , C03C17/3652 , C03C17/3655 , C03C17/366 , C03C17/3681 , C03C17/42 , C03C23/0075 , C03C2217/282 , C03C2217/75 , C03C2217/76 , C03C2217/78 , C03C2218/151 , C03C2218/31 , C23C16/26 , G02B5/208 , Y10T428/24975 , Y10T428/265 , Y10T428/30
摘要： A substrate is coated with a low-E coating system including at least one infrared (IR) reflective layer. A diamond-like carbon (DLC) inclusive protective coating system (e.g., including at least one highly tetrahedral amorphous carbon (ta-C) inclusive layer having sp3 carbon—carbon bonds) is provided on the substrate over at least the IR reflective layer in order to make the low-E coating system scratch resistant, abrasion resistant, and generally mechanically durable. The DLC inclusive protective coating system may be hydrophobic, hydrophillic, or neutral in different embodiments of the invention. Optionally, at least one fluoro-alkyl silane (FAS) compound inclusive layer may be provided on the substrate over at least one of the DLC inclusive layer(s) in hydrophobic embodiments in order to increase contact angle &thgr; of the coated article.
摘要翻译： 衬底被涂覆有包括至少一个红外（IR）反射层的低E涂层系统。 至少在IR上提供了包含金刚石碳（DLC）的保护涂层系统（例如，包括至少一个具有sp 3碳 - 碳键的高度四面体无定形碳（ta-C））层） 反射层，以使低E涂层系统耐划伤，耐磨损，并且通常机械耐用。 在本发明的不同实施方案中，含DLC的保护涂层体系可以是疏水的，亲水的或中性的。 任选地，在疏水性实施方案中，至少一种含氟烷基硅烷（FAS）化合物的层可以在至少一种含DLC的层中在衬底上提供，以增加涂覆制品的接触角θ。
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10.发明授权Method of making coated article including diamond-like carbon (DLC) and FAS 失效制造包括类金刚石碳（DLC）和FAS的涂层制品的方法公开(公告)号：US06472017B2
公开(公告)日：2002-10-29
申请号：US09877099
申请日：2001-06-11
IPC分类号： C23C1626
CPC分类号： C03C17/3634 , B05D5/083 , B08B17/06 , B08B17/065 , B32B17/1033 , B60S1/54 , B60S1/58 , C03C3/076 , C03C17/22 , C03C17/3441 , C03C17/3482 , C03C17/36 , C03C17/3644 , C03C17/3652 , C03C17/42 , C03C23/0075 , C03C2217/282 , C03C2217/76 , C03C2217/78 , C03C2218/151 , C03C2218/31 , C23C16/0272 , C23C16/26 , G02B5/208 , Y10T428/24942 , Y10T428/24983 , Y10T428/30 , Y10T428/31663
摘要： A substrate is coated with a hydrophobic coating system including diamond-like carbon (DLC) and at least one fluoro-alkyl silane (FAS) compound. In certain embodiments, the coating system includes an FAS inclusive layer provided over at least one DLC inclusive layer in order to increase the initial contact angle of the coated article. At least the FAS inclusive layer may be heated (i.e., thermally cured) to an extent sufficient to at least one of: (a) improve the initial contact angle &thgr; of the resulting coated article, (b) render the hydrophobic nature of the resulting coated article more stable when exposed to solution(s)/material(s) such as hexane and/or isopropyl alcohol, and/or (c) improve bonding characteristics of the FAS inclusive layer within itself and/or between the FAS inclusive layer and a layer immediately beneath it.
摘要翻译： 用包括类金刚石碳（DLC）和至少一种氟烷基硅烷（FAS）化合物的疏水涂层体系涂覆基材。 在某些实施方案中，涂层系统包括在至少一个含DLC层上提供的包含FAS的层，以便增加涂覆制品的初始接触角。 至少包含FAS的层可以被加热（即，热固化）至足以至少一个程度的程度：（a）改善所得涂层制品的初始接触角θ，（b）使所得到的涂层制品的疏水性质 涂覆制品当暴露于溶液/材料如己烷和/或异丙醇时更稳定，和/或（c）改善其本身和/或FAS包含层之间和/或包含FAS的层之间的粘合特性和 在它下面的一层。
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