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    Processes for the production of mono- and multifilaments and staple fibers based on kolyarylene sulfides and high-strength polyarylene sulfide fibers
    2.
    发明授权
    Processes for the production of mono- and multifilaments and staple fibers based on kolyarylene sulfides and high-strength polyarylene sulfide fibers 失效

    公开(公告)号：US5215819A

    公开(公告)日：1993-06-01

    申请号：US621403

    申请日：1990-12-03

    申请人： Wolfgang Anderheggen ,  Michael Kraemer ,  Roland Vogelsgesang ,  Wolfram Wagner ,  Wolfgang Olges ,  Thomas Dragovic

    发明人： Wolfgang Anderheggen ,  Michael Kraemer ,  Roland Vogelsgesang ,  Wolfram Wagner ,  Wolfgang Olges ,  Thomas Dragovic

    IPC分类号： D01D5/08 ,  D01F6/76

    CPC分类号： D01D5/08 ,  D01F6/765 ,  Y10T428/2909 ,  Y10T428/2913 ,  Y10T428/2922

    摘要： This invention relates to processes for the production of mono- and multifilaments and also staple fibers of multifilaments based on polyarylene sulfides, preferably substantially linear polyarylene sulfides and, more preferably, substantially linear poly-p-phenylene sulfide by melt spinning, multistage stretching and optionally crimping and setting.As a result of the treatment by blowing of air onto the stabilized spun filaments in the first stretching stages at temperatures .ltoreq.100.degree. C. (preferably in stretching baths, more particularly in boiling water), the chain molecules are oriented; the orientation and crystallinity required for high strengths is achieved by afterstretching (in hot air) at elevated temperature. The residence times in the first stage required for effective stretching in accordance with the invention can only be varied within relatively narrow limits in order subsequently to achieve the calculated orientations and effects, particularly high strengths, crystallinities and densities. Overly long residence times at temperatures above 100.degree. C. result in elongation of the material with no additional orientation and hence with an inadequate increase in strength.To increase crystallinity and strength in the production of mono- and multifilaments, multistage stretching may be followed by a thermal aftertreatment; in the staple fiber process, the material is additionally crimped, set (in the absence of tension) and cut. Where an aerodynamic crimping nozzle is used, as is preferably the case, stretching has to be carried out in accordance with the invention in such a way that the fibers are left with sufficiently high shrinkage which is important for crimping and subsequent processing. Crimping is improved by setting in the absence of tension. Relatively high-tensile fibers with sufficiently high residual crimping for subsequent processing are obtained.Textile-denier fibers (up to about 20 dtex) having hitherto unknown strengths of >6 cN/dtex, preferably >6.2 cN/dtex and, more preferably, >6.4 cN/dtex are claimed.

    Processes for the production of mono- and multifilaments and staple fibers based on polyarylene sulfides
    3.
    发明授权
    Processes for the production of mono- and multifilaments and staple fibers based on polyarylene sulfides 失效
    用于生产基于聚亚芳基硫化物的单丝和复丝和短纤维的方法

    公开(公告)号：US5024797A

    公开(公告)日：1991-06-18

    申请号：US522296

    申请日：1990-05-11

    申请人： Wolfgang Anderheggen ,  Michael Kraemer ,  Roland Vogelsgesang ,  Wolfram Wagner ,  Wolfgang Olges ,  Thomas Dragovic

    发明人： Wolfgang Anderheggen ,  Michael Kraemer ,  Roland Vogelsgesang ,  Wolfram Wagner ,  Wolfgang Olges ,  Thomas Dragovic

    IPC分类号： D01D5/08 ,  D01D5/12 ,  D01F6/76 ,  D02J1/22

    CPC分类号： D01D5/08 ,  D01F6/765

    摘要： Processes for the production of mono- and multifilaments and also staple fibers of multifilaments based on polyarylene sulfides by melt spinning, multistage stretching and setting. As a result of the treatment by blowing of air onto the stabilized spun filaments in the first stretching stages at temperatures .ltoreq.100.degree. C., the chain molecules are oriented; the orientation and crystallinity required for high strengths is achieved by afterstretching at elevated temperature. The residence times in the first stage required for effective stretching can only be varied within relatively narrow limits in order subsequently to achieve the calculated orientations and effects. Overly long residence times at temperatures above 100.degree. C. result in elongation of the material with no additional orientation and hence with an inadequate increase in strength.

    摘要翻译： 用于通过熔融纺丝，多段拉伸和定型来生产单丝和多丝以及基于聚亚芳基硫化物的复丝的短纤维的方法。 作为通过在100℃的温度下在第一拉伸阶段中将空气吹到稳定纺丝上进行处理的结果，链分子被取向; 高强度所需的取向和结晶度通过在升高的温度下拉伸来实现。 在有效拉伸所需的第一阶段中的停留时间只能在相对窄的范围内变化，以便随后实现计算的取向和效果。 超过100℃的过长停留时间导致材料的伸长，没有额外的取向，因此强度不足。

    Production of very fine polymer fibres
    5.
    发明授权
    Production of very fine polymer fibres 失效
    生产非常细的聚合物纤维

    公开(公告)号：US4937020A

    公开(公告)日：1990-06-26

    申请号：US292696

    申请日：1989-01-03

    申请人： Wolfram Wagner ,  Peter R. Nyssen ,  Dirk Berkenhaus ,  Hans-Theo van Pey

    发明人： Wolfram Wagner ,  Peter R. Nyssen ,  Dirk Berkenhaus ,  Hans-Theo van Pey

    IPC分类号： D01F6/06 ,  D01D5/08 ,  D01D5/18 ,  D01F6/60

    CPC分类号： D04H3/02 ,  D01D5/18 ,  D04H3/009 ,  D04H3/011 ,  D04H3/16

    摘要： The polymer granular melt (1) is whirled out of a rotating nozzle head (6) through a plurality of exit holes (24) with fibre formation (32) and the fibres formed (9) are deposited on a collecting surface (12) in web form (15). This polymer melt is introduced into the nozzle head (6) under a preliminary pressure of 1 bar to 200 bar, preferably 1 bar to 50 bar. Furthermore, the fibres (32) are deflected by a high-speed gas stream (7, 8) in a radial direction at a radial distance of 10 mm to 200 mm from the exit holes (24) and, in the course of being deflected, are simultaneously drawn and stretched. The melt streams (32) exiting from the exit holes (24) can be additionally drawn by gas streams (26, 34) exiting in the vicinity of the exit holes (24) at the nozzle head (6) with a predominantly radial component before coming under the influence of the axial deflecting gas stream (7, 8).

    摘要翻译： 聚合物颗粒状熔体（1）通过具有纤维形成（32）的多个出口孔（24）从旋转喷嘴头（6）旋转出来并且形成的纤维（9）沉积在收集表面（12）上 网络形式（15）。 该聚合物熔体在1巴至200巴，优选1巴至50巴的预备压力下引入喷嘴头（6）。 此外，纤维（32）在离开孔（24）的径向距离为10mm至200mm的径向方向上被高速气流（7,8）偏转，并且在被偏转的过程中 ，同时拉伸和拉伸。 从出口孔（24）排出的熔体流（32）可以另外由在喷嘴头（6）处的出口孔（24）附近出口的气流（26,34）以主要的径向分量吸引 在轴向偏转气流（7,8）的影响下。

    Apparatus for the production of fine mineral fibres
    6.
    发明授权
    Apparatus for the production of fine mineral fibres 失效
    用于生产细矿物纤维的设备

    公开(公告)号：US4676815A

    公开(公告)日：1987-06-30

    申请号：US847797

    申请日：1986-04-03

    申请人： Wolfram Wagner ,  Peter R. Nyssen ,  Gunter Espanion ,  Dirk Berkenhaus ,  Gunter Haladuda ,  Hans-Theo van Pey ,  Karl-Heinz Schott

    发明人： Wolfram Wagner ,  Peter R. Nyssen ,  Gunter Espanion ,  Dirk Berkenhaus ,  Gunter Haladuda ,  Hans-Theo van Pey ,  Karl-Heinz Schott

    IPC分类号： C03B37/022 ,  C03B37/06 ,  D01D5/14

    CPC分类号： C03B37/06 ,  D01D5/14

    摘要： Filaments of a molten material issue from a plurality of openings in a heated melt crucible and are further fiberized in a draw nozzle by means of a blowing medium. The diameter of the outlet openings (3) at the base of the melt crucible (1) is very small and is 0.2 to 1.5 mm, so that very fine primary filaments (12) are already formed at this point. These primary filaments are grasped by a very turbulent current at the entrance of the draw nozzle (5). The transverse component of the current decreasing in favor of the longitudinal component as the axial distance from the outlet openings (3) increases. The draw nozzle also has an inlet portion, which has a sharp outer edge and widens in the direction of flow, so that air blows against the primary filaments at a high speed and they are exposed to a strong pressure gradient in the longitudinal direction before entering the inlet portion. In the draw nozzle the primary filaments which are themselves already very thin are drawn out further until they have the required final diameter. For this purpose a zone is provided in the interior of the nozzle, following the inlet portion, in which zone the rate of flow of the blowing medium is 400 m/s to 600 m/s at a pressure of between 0.1 and 0.4 bar. By means of this device very fine mineral fibres with a substantially uniform fibre diameter of between 0.1 .mu.m and 5 .mu.m can be produced.

    摘要翻译： 熔融材料的长丝从加热熔融坩埚中的多个开口出现，并通过吹塑介质进一步在牵引喷嘴中纤维化。 在熔融坩埚（1）底部的出口开口（3）的直径非常小，为0.2-1.5mm，从而在这一点上已经形成非常细的一次丝（12）。 这些初级细丝在拉伸喷嘴（5）的入口处被非常湍流的电流所夹持。 随着与出口（3）的轴向距离的增加，电流的横向分量有利于纵向分量。 牵引喷嘴还具有入口部分，其具有尖锐的外边缘并且在流动方向上变宽，使得空气以高速吹向初级细丝，并且在进入之前暴露于纵向方向上的强压力梯度 入口部分。 在拉丝喷嘴中，本身已经非常薄的主丝被进一步拉出，直到它们具有所需的最终直径。 为此，在喷嘴的内部设有一区域，在入口部分之后，在0.1-4.0巴的压力下，吹送介质的流速为400m / s至600m / s。 通过该装置，可以生产出具有0.1μm至5μm之间的基本上均匀的纤维直径的非常细的矿物纤维。

    Process for treatment of filament cable
    9.
    发明授权
    Process for treatment of filament cable 失效
    长丝电缆处理工艺

    公开(公告)号：US4854020A

    公开(公告)日：1989-08-08

    申请号：US145574

    申请日：1988-01-19

    申请人： Wolfram Wagner ,  Dieter Paulini ,  Peter Widder

    发明人： Wolfram Wagner ,  Dieter Paulini ,  Peter Widder

    IPC分类号： D02G1/12 ,  D02G1/20

    CPC分类号： D02G1/205

    摘要： Filament cables are crimped and the crimp cake of the filament cable obtained is passed over a gas permeable screen plate while gas flows to the bottom of the cake from flow through the screen plate so that the cake can be moved over the plate without making contact therewith or with reduced contact force and can be treated during its residence over the screen plate.

    摘要翻译： 丝束电缆被卷曲，并且所获得的细丝电缆的卷边饼通过透气性筛板，同时气体从流过筛板的流动到滤饼的底部，使得滤饼可以在板上移动而不与其接触 或具有降低的接触力并且可以在其在屏板上的居住期间进行处理。

    Process and apparatus for the production of very fine mineral fibers, in particular glass fibers
    10.
    发明授权
    Process and apparatus for the production of very fine mineral fibers, in particular glass fibers 失效
    生产非常细的矿物纤维，特别是玻璃纤维的方法和设备

    公开(公告)号：US4838917A

    公开(公告)日：1989-06-13

    申请号：US150682

    申请日：1988-02-01

    申请人： Wolfram Wagner ,  Roger Nyssen ,  Dirk Berkenhaus ,  Hans-Theo van Pey

    发明人： Wolfram Wagner ,  Roger Nyssen ,  Dirk Berkenhaus ,  Hans-Theo van Pey

    IPC分类号： C03B37/06

    CPC分类号： C03B37/06

    摘要： The streams of melt issuing from the melt outlet apertures (18) at the bottom of a melting crucible (14) are broken up into fibers in a drawing nozzle by means of a blast medium directed substantially parallel to the streams of melt. The blast medium is produced by a pressure gradient in the drawing nozzle and sucked in at the drawing nozzle inlet (7). In the drawing nozzle (16), the flow velocity is reduced in a downstream diffuser after the drawing process. The blast medium is supplied in the form of a hot gas between the underside of the crucible and the top edge (15) of the drawing nozzle from opposite broadsides of the melt distributor (14) in excess to the total quantity of gas stream sucked in at the drawing nozzle inlet (7). The hot gas consists of a mixture of combustion gases and air and is at a temperature from 600.degree. C. to 1500.degree. C., preferably from 800.degree. C. to 1400.degree. C. The flow velocity of the hot gas is adjusted to a value below 100 m/s, preferably 50 m/s, in the region (13) between the drawing nozzle (16) and the melt distributor (14). Gas burners (1) provided for producing the hot gas are arranged with their combustion chambers (3) situated laterally between the melt distributor (14) and the top edge (15) of the debiteuse. The combustion chambers (3) are connected by bores (6) to air chambers which are under an excess pressure. In the combustion chambers (3), the combustion gases are homogeneously mixed with the air introduced.

    摘要翻译： 从熔融坩埚（14）底部的熔体出口孔（18）发出的熔体流通过基本上平行于熔体流定向的鼓风介质在拉丝喷嘴中分解成纤维。 鼓风介质由拉伸喷嘴中的压力梯度产生，并在抽吸喷嘴入口（7）处吸入。 在绘图喷嘴（16）中，拉伸处理后的下游扩散器中的流速减小。 鼓风介质以坩埚的下侧和拉丝喷嘴的顶边（15）之间的热气体的形式从熔体分配器（14）的相对的宽边提供，超过吸入的气流的总量 在绘图喷嘴入口（7）处。 热气体由燃烧气体和空气的混合物组成，温度为600℃至1500℃，优选为800℃至1400℃。将热气体的流速调节至 在拉伸喷嘴（16）和熔体分配器（14）之间的区域（13）中的值低于100m / s，优选为50m / s。 设置用于产生热气体的气体燃烧器（1）被布置成其燃烧室（3）横向位于熔体分配器（14）和脱盐槽的顶部边缘（15）之间。 燃烧室（3）通过孔（6）连接到处于过大压力下的空气室。 在燃烧室（3）中，燃烧气体与引入的空气均匀混合。