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    Process for the preparation of 1-alkyl glycerol ethers
    4.
    发明授权
    Process for the preparation of 1-alkyl glycerol ethers 有权
    制备1-烷基甘油醚的方法

    公开(公告)号：US08877983B2

    公开(公告)日：2014-11-04

    申请号：US12830552

    申请日：2010-07-06

    申请人： Wolfgang Beilfuss ,  Martin Balthasar ,  Ralf Gradtke ,  Klaus Weber ,  Heinz-Georg Steffen

    发明人： Wolfgang Beilfuss ,  Martin Balthasar ,  Ralf Gradtke ,  Klaus Weber ,  Heinz-Georg Steffen

    IPC分类号： C07C41/02 ,  C07C43/10 ,  C07C41/26 ,  C07C67/26

    CPC分类号： C07C41/26 ,  C07C67/26 ,  Y02P20/582 ,  C07C43/13 ,  C07C69/08

    摘要： A process for the preparation of a 1-alkyl glycerol ether of the formula (I) in which: (a) an alkyl glycidyl ether of the formula (II) in which R is an unbranched or branched C1- to C24-alkyl group, where the alkyl group may be substituted with one or more hydroxy and/or C1- to C4-alkoxy group(s) and/or the alkyl chain may be interrupted by up to four oxygen atoms, is added to: (x) a carboxylic acid having 1-10 carbon atoms; (y) an ester of a carboxylic acid having 1-10 carbon atoms; and/or (z) an anhydride of a carboxylic acid having 1-10 carbon atoms. The low-water reaction mixture containing a catalytic amount of a strong acid is reacted at a temperature of more than 40° C. to give an acylated alkyl glycerol ether; and (b) the acylated alkyl glycerol ether is reacted in order to obtain the alkyl glycerol ether of the formula (I).

    摘要翻译： 一种制备式（I）的1-烷基甘油醚的方法，其中：（a）式（II）的烷基缩水甘油醚，其中R是未支链或支链的C 1〜C 24 - 烷基， 其中烷基可以被一个或多个羟基和/或C 1至C 4 - 烷氧基取代，和/或烷基链可以被至多四个氧原子间隔，加入到：（x）羧酸 具有1-10个碳原子的酸; （y）具有1-10个碳原子的羧酸的酯; 和/或（z）具有1-10个碳原子的羧酸的酸酐。 含有催化量的强酸的低水反应混合物在大于40℃的温度下反应，得到酰化烷基甘油醚; 和（b）使酰化烷基甘油醚反应，得到式（I）的烷基甘油醚。