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    RAPID PREPARATION PROCESS OF AEROGEL
    1.
    发明申请
    RAPID PREPARATION PROCESS OF AEROGEL 审中-公开
    航空快速准备过程

    公开(公告)号：US20080081014A1

    公开(公告)日：2008-04-03

    申请号：US11737450

    申请日：2007-04-19

    申请人： Yong-Soo AHN ,  Jeong-Gu Yeo ,  Moon-Hee Han ,  Churl-Hee Cho ,  Sharad D. Bhagat ,  Yong-Ha Kim ,  Ho-Sung Park

    发明人： Yong-Soo AHN ,  Jeong-Gu Yeo ,  Moon-Hee Han ,  Churl-Hee Cho ,  Sharad D. Bhagat ,  Yong-Ha Kim ,  Ho-Sung Park

    IPC分类号： C01B33/12

    CPC分类号： C01B33/1585 ,  C01B33/158

    摘要： Disclosed herein is a rapid preparation process of aerogel. More specifically, the present invention relates to a rapid preparation process of aerogel which enables a considerable reduction in preparation time and preparation costs via simultaneous treatment of solvent exchange and surface-modification of hydrophilic-to-hydrophobic transition.The rapid preparation process comprises mixing a cation exchange resin with sodium silicate (water glass) as a starting material, and removing the sodium ion from the sodium silicate, to subject the sodium silicate to ion exchange; adding a base catalyst and an organosilane compound to the sodium silicate to subject the sodium silicate to gelation; aging the gellized silica gel at room temperature for 2 to 4 hours to discharge water from the silica gel and to modify the surface of the silica gel into hydrophobicity; and drying the hydrophobic silica gel at atmospheric pressure for 18 to 27 hours.

    摘要翻译： 本文公开了气凝胶的快速制备方法。 更具体地说，本发明涉及一种气凝胶的快速制备方法，其通过同时处理亲水 - 疏水过渡的溶剂交换和表面改性，能够显着降低制备时间和制备成本。 快速制备方法包括将阳离子交换树脂与硅酸钠（水玻璃）作为起始原料混合，并从硅酸钠中除去钠离子，使硅酸钠进行离子交换; 向硅酸钠中加入碱催化剂和有机硅烷化合物以使硅酸钠发生凝胶化; 将胶凝硅胶在室温下老化2至4小时，以从硅胶中排出水，并将硅胶表面改性为疏水性; 并在大气压下干燥疏水性硅胶18至27小时。

    THERMAL CRACKING RESISTANT ZEOLITE MEMBRANE AND METHOD OF FABRICATING THE SAME
    3.
    发明申请
    THERMAL CRACKING RESISTANT ZEOLITE MEMBRANE AND METHOD OF FABRICATING THE SAME 审中-公开
    热裂化抗沸石薄膜及其制造方法

    公开(公告)号：US20120009120A1

    公开(公告)日：2012-01-12

    申请号：US12843159

    申请日：2010-07-26

    申请人： CHURL-HEE CHO ,  Jeong-Gu Yeo ,  Young-Soo Ahn ,  Si-Kyung Kim ,  Joon-Soo Kim ,  Nam-Jo Jeong ,  Bo-Yun Jang ,  Dong-Kook Kim ,  Hong-Soo Kim

    发明人： CHURL-HEE CHO ,  Jeong-Gu Yeo ,  Young-Soo Ahn ,  Si-Kyung Kim ,  Joon-Soo Kim ,  Nam-Jo Jeong ,  Bo-Yun Jang ,  Dong-Kook Kim ,  Hong-Soo Kim

    IPC分类号： C01B39/02

    CPC分类号： B01D71/028 ,  B01D67/0051 ,  B01D69/10 ,  B01D2323/46

    摘要： The present disclosure relates to a thermal cracking resistant zeolite membrane and a method of fabricating the same. The method includes dissolving an alumina-based material, a silica-based material and sodium hydroxide in water to prepare an aqueous solution, stirring the aqueous solution to form a hydrothermal solution, preparing a slurry of zeolite seeds through wet-type vibration pulverization and centrifugal separation of zeolite powder, passing the zeolite seeds through a support by vacuum filtration such that the zeolite seeds can be infiltrated into an inner region of the support ranging from a depth of 3 μm to a depth corresponding to 50% of a total thickness of the support, and immersing the support into the hydrothermal solution for hydrothermal treatment to grow a dense zeolite separation layer not only on the surface of the support but also on the inner region thereof. The zeolite membrane prevents the occurrence of thermal cracking on the zeolite separation layer, thereby providing good thermal stability and separation performance during heating and at a target processing temperature.

    摘要翻译： 本发明涉及耐热裂解沸石膜及其制造方法。 该方法包括将氧化铝基材料，二氧化硅基材料和氢氧化钠溶解在水中以制备水溶液，搅拌该水溶液以形成水热溶液，通过湿式振动粉碎和离心制备沸石种子的浆料 分离沸石粉末，通过真空过滤将沸石种子通过支持物，使得沸石种子可以渗透到载体的内部区域中，范围从3μm的深度到相当于总厚度的50％的深度 支撑并将载体浸入用于水热处理的水热溶液中，不仅在支撑体的表面上而且在其内部区域上生长致密的沸石分离层。 沸石膜防止沸石分离层发生热裂解，从而在加热和目标加工温度下提供良好的热稳定性和分离性能。

    Aerogel Mat and Manufacturing Method Thereof
    4.
    发明申请
    Aerogel Mat and Manufacturing Method Thereof 有权
    气凝胶垫及其制造方法

    公开(公告)号：US20120025127A1

    公开(公告)日：2012-02-02

    申请号：US13258225

    申请日：2010-06-10

    申请人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    发明人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    IPC分类号： E04B1/82 ,  B01J8/00

    CPC分类号： C01B33/1585 ,  C01B33/155 ,  C01B33/157 ,  Y02P20/544

    摘要： The present invention relates to a method of manufacturing a mat containing aerogel and to a mat manufactured using this method. A method of manufacturing a mat containing silica aerogel according to an aspect of the invention includes: (S1) producing a wet gel by mixing water glass and alcohol in a reactor; (S2) modifying a surface of the wet gel by adding an organic silane compound and an organic solvent to the reactor and mixing; (S3) separating a upper liquid from a solution in the reactor and impregnating a fibrous matrix with the upper liquid; and (S4) drying the fibrous matrix impregnated with the upper liquid. According to an aspect of the invention, a mat containing silica aerogel can be manufactured using only water glass as raw material, even when applying the drying process in an ambient environment, without using expensive materials or supercritical apparatus.

    摘要翻译： 本发明涉及一种制造含有气凝胶的垫的方法和使用该方法制造的垫。 根据本发明的一个方面的制备含有二氧化硅气凝胶的垫的方法包括：（S1）通过在反应器中混合水玻璃和醇来生产湿凝胶; （S2）通过向反应器中加入有机硅烷化合物和有机溶剂并混合来改性湿凝胶的表面; （S3）将上液体与反应器中的溶液分离，并用上液体浸渍纤维基质; 和（S4）干燥浸渍有上层液体的纤维基质。 根据本发明的一个方面，即使在不使用昂贵的材料或超临界设备的情况下在周围环境中进行干燥处理，也可以仅使用水玻璃作为原料来制造含有二氧化硅气凝胶的垫。

    Aerogel mat and manufacturing method thereof
    5.
    发明授权
    Aerogel mat and manufacturing method thereof 有权
    气凝胶垫及其制造方法

    公开(公告)号：US08663739B2

    公开(公告)日：2014-03-04

    申请号：US13258225

    申请日：2010-06-10

    申请人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    发明人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    IPC分类号： B05D3/02

    CPC分类号： C01B33/1585 ,  C01B33/155 ,  C01B33/157 ,  Y02P20/544

    摘要： The present invention relates to a method of manufacturing a mat containing aerogel and to a mat manufactured using this method. A method of manufacturing a mat containing silica aerogel according to an aspect of the invention includes: (S1) producing a wet gel by mixing water glass and alcohol in a reactor; (S2) modifying a surface of the wet gel by adding an organic silane compound and an organic solvent to the reactor and mixing; (S3) separating a upper liquid from a solution in the reactor and impregnating a fibrous matrix with the upper liquid; and (S4) drying the fibrous matrix impregnated with the upper liquid. According to an aspect of the invention, a mat containing silica aerogel can be manufactured using only water glass as raw material, even when applying the drying process in an ambient environment, without using expensive materials or supercritical apparatus.

    摘要翻译： 本发明涉及一种制造含有气凝胶的垫的方法和使用该方法制造的垫。 根据本发明的一个方面的制备含有二氧化硅气凝胶的垫的方法包括：（S1）通过在反应器中混合水玻璃和醇来生产湿凝胶; （S2）通过向反应器中加入有机硅烷化合物和有机溶剂并混合来改性湿凝胶的表面; （S3）将上液体与反应器中的溶液分离，并用上液体浸渍纤维基质; 和（S4）干燥浸渍有上层液体的纤维基质。 根据本发明的一个方面，即使在不使用昂贵的材料或超临界设备的情况下在周围环境中进行干燥处理，也可以仅使用水玻璃作为原料来制造含有二氧化硅气凝胶的垫。