Method of Preparing Silica Aerogel Granules
    1.
    发明申请
    Method of Preparing Silica Aerogel Granules 有权
    二氧化硅气凝胶颗粒的制备方法

    公开(公告)号:US20130106008A1

    公开(公告)日:2013-05-02

    申请号:US13808673

    申请日:2011-09-28

    IPC分类号: C07F7/12 C09K3/00

    摘要: A method of preparing transparent or nontransparent silica aerogel granules. The method includes forming a granular wet gel by spraying a silica sol into alcohol, the silica sol being prepared by mixing a water glass solution or an opacifier-containing water glass solution with an inorganic acid solution, forming a granular alcohol gel through gelation aging and solvent substitution of the granular wet gel in alcohol, hydrophobically modifying the surface of the granular alcohol gel using an organic silane compound, and drying the surface modified gel at ambient pressure or in a vacuum. The method may prepare silica aerogel granules in a short period of time through heat treatment at a relatively low temperature and at ambient pressure or in a vacuum, thereby ensuring excellent economic feasibility, continuity and reliability, suited for mass production.

    摘要翻译: 制备透明或不透明的二氧化硅气凝胶颗粒的方法。 该方法包括通过将二氧化硅溶胶喷射到醇中形成粒状湿凝胶,该硅溶胶是通过将水玻璃溶液或含有遮光剂的水玻璃溶液与无机酸溶液混合制备的,通过凝胶化老化形成粒状醇凝胶, 在醇中的颗粒状湿凝胶的溶剂置换,使用有机硅烷化合物疏水改性粒状醇凝胶的表面,并在环境压力或真空下干燥表面改性凝胶。 该方法可以在相对较低的温度和环境压力或真空下通过热处理在短时间内制备二氧化硅气凝胶颗粒,从而确保了适合于批量生产的优异的经济可行性,连续性和可靠性。

    Method of preparing silica aerogel granules
    4.
    发明授权
    Method of preparing silica aerogel granules 有权
    制备二氧化硅气凝胶颗粒的方法

    公开(公告)号:US08894893B2

    公开(公告)日:2014-11-25

    申请号:US13808673

    申请日:2011-09-28

    IPC分类号: C01B33/158 B01J2/08 C09K3/00

    摘要: A method of preparing transparent or nontransparent silica aerogel granules. The method includes forming a granular wet gel by spraying a silica sol into alcohol, the silica sol being prepared by mixing a water glass solution or an opacifier-containing water glass solution with an inorganic acid solution, forming a granular alcohol gel through gelation aging and solvent substitution of the granular wet gel in alcohol, hydrophobically modifying the surface of the granular alcohol gel using an organic silane compound, and drying the surface modified gel at ambient pressure or in a vacuum. The method may prepare silica aerogel granules in a short period of time through heat treatment at a relatively low temperature and at ambient pressure or in a vacuum, thereby ensuring excellent economic feasibility, continuity and reliability, suited for mass production.

    摘要翻译: 制备透明或不透明的二氧化硅气凝胶颗粒的方法。 该方法包括通过将二氧化硅溶胶喷射到醇中形成粒状湿凝胶,该硅溶胶是通过将水玻璃溶液或含有遮光剂的水玻璃溶液与无机酸溶液混合制备的,通过凝胶化老化形成粒状醇凝胶, 在醇中的颗粒状湿凝胶的溶剂置换,使用有机硅烷化合物疏水改性粒状醇凝胶的表面,并在环境压力或真空下干燥表面改性凝胶。 该方法可以在相对较低的温度和环境压力或真空下通过热处理在短时间内制备二氧化硅气凝胶颗粒,从而确保了适合于批量生产的优异的经济可行性,连续性和可靠性。

    THERMAL CRACKING RESISTANT ZEOLITE MEMBRANE AND METHOD OF FABRICATING THE SAME
    6.
    发明申请
    THERMAL CRACKING RESISTANT ZEOLITE MEMBRANE AND METHOD OF FABRICATING THE SAME 审中-公开
    热裂化抗沸石薄膜及其制造方法

    公开(公告)号:US20120009120A1

    公开(公告)日:2012-01-12

    申请号:US12843159

    申请日:2010-07-26

    IPC分类号: C01B39/02

    摘要: The present disclosure relates to a thermal cracking resistant zeolite membrane and a method of fabricating the same. The method includes dissolving an alumina-based material, a silica-based material and sodium hydroxide in water to prepare an aqueous solution, stirring the aqueous solution to form a hydrothermal solution, preparing a slurry of zeolite seeds through wet-type vibration pulverization and centrifugal separation of zeolite powder, passing the zeolite seeds through a support by vacuum filtration such that the zeolite seeds can be infiltrated into an inner region of the support ranging from a depth of 3 μm to a depth corresponding to 50% of a total thickness of the support, and immersing the support into the hydrothermal solution for hydrothermal treatment to grow a dense zeolite separation layer not only on the surface of the support but also on the inner region thereof. The zeolite membrane prevents the occurrence of thermal cracking on the zeolite separation layer, thereby providing good thermal stability and separation performance during heating and at a target processing temperature.

    摘要翻译: 本发明涉及耐热裂解沸石膜及其制造方法。 该方法包括将氧化铝基材料,二氧化硅基材料和氢氧化钠溶解在水中以制备水溶液,搅拌该水溶液以形成水热溶液,通过湿式振动粉碎和离心制备沸石种子的浆料 分离沸石粉末,通过真空过滤将沸石种子通过支持物,使得沸石种子可以渗透到载体的内部区域中,范围从3μm的深度到相当于总厚度的50%的深度 支撑并将载体浸入用于水热处理的水热溶液中,不仅在支撑体的表面上而且在其内部区域上生长致密的沸石分离层。 沸石膜防止沸石分离层发生热裂解,从而在加热和目标加工温度下提供良好的热稳定性和分离性能。

    Aerogel mat and manufacturing method thereof
    8.
    发明授权
    Aerogel mat and manufacturing method thereof 有权
    气凝胶垫及其制造方法

    公开(公告)号:US08663739B2

    公开(公告)日:2014-03-04

    申请号:US13258225

    申请日:2010-06-10

    IPC分类号: B05D3/02

    摘要: The present invention relates to a method of manufacturing a mat containing aerogel and to a mat manufactured using this method. A method of manufacturing a mat containing silica aerogel according to an aspect of the invention includes: (S1) producing a wet gel by mixing water glass and alcohol in a reactor; (S2) modifying a surface of the wet gel by adding an organic silane compound and an organic solvent to the reactor and mixing; (S3) separating a upper liquid from a solution in the reactor and impregnating a fibrous matrix with the upper liquid; and (S4) drying the fibrous matrix impregnated with the upper liquid. According to an aspect of the invention, a mat containing silica aerogel can be manufactured using only water glass as raw material, even when applying the drying process in an ambient environment, without using expensive materials or supercritical apparatus.

    摘要翻译: 本发明涉及一种制造含有气凝胶的垫的方法和使用该方法制造的垫。 根据本发明的一个方面的制备含有二氧化硅气凝胶的垫的方法包括:(S1)通过在反应器中混合水玻璃和醇来生产湿凝胶; (S2)通过向反应器中加入有机硅烷化合物和有机溶剂并混合来改性湿凝胶的表面; (S3)将上液体与反应器中的溶液分离,并用上液体浸渍纤维基质; 和(S4)干燥浸渍有上层液体的纤维基质。 根据本发明的一个方面,即使在不使用昂贵的材料或超临界设备的情况下在周围环境中进行干燥处理,也可以仅使用水玻璃作为原料来制造含有二氧化硅气凝胶的垫。

    POLYMER COMPOSITE MATERIALS FOR BUILDING AIR CONDITIONING OR DEHUMIDIFICATION AND PREPARATION METHOD THEREOF
    9.
    发明申请
    POLYMER COMPOSITE MATERIALS FOR BUILDING AIR CONDITIONING OR DEHUMIDIFICATION AND PREPARATION METHOD THEREOF 审中-公开
    用于建筑空调或除湿的聚合物复合材料及其制备方法

    公开(公告)号:US20130299121A1

    公开(公告)日:2013-11-14

    申请号:US13994320

    申请日:2010-12-15

    IPC分类号: F28D19/04

    摘要: The present disclosure relates to the preparation of a polymer composite material for building air conditioning or dehumidification having superior water-adsorbing ability, durability and antibacterial properties by electro spinning. Specifically, the disclosed method for preparing a polymer composite material for building air conditioning or dehumidification includes: (S1) adding a crosslinking agent or a crosslinking agent and a porous filler for conferring durability and antibacterial properties into a hydrophilic polymer solution antibacterial properties to prepare a polymer composite material solution; (S2) electrospinning the polymer composite material solution to prepare a nanofiber sheet; and (S3) crosslinking the nanofiber sheet by heat-treatment. Since the disclosed polymer composite material for building air conditioning or dehumidification has superior antibacterial properties and excellent water-adsorbing ability and durability, the polymer composite material can perform dehumidification when used for air conditioning of a building, thereby reducing air conditioning load and improving energy efficiency. Further, through dehumidifying cooling, the high-efficiency polymer composite material can remove moisture from the hot and humid air in the summer, thus reducing air conditioning load by decreasing latent heat load and saving energy. In addition, the polymer composite material can be used in moisture-sensitive production processes, industrial applications requiring moisture control or protection from damage or corrosion by moisture to reduce moisture and provide dry air.

    摘要翻译: 本公开内容涉及通过电纺法制备具有优异的吸水能力,耐久性和抗菌性的建筑空调或除湿用聚合物复合材料。 具体地,所公开的制造用于建筑空调或除湿的聚合物复合材料的方法包括:(S1)添加交联剂或交联剂和多孔填料以​​赋予亲水性聚合物溶液抗菌性能的耐久性和抗菌性,以制备 聚合物复合材料溶液; (S2)静电纺丝聚合物复合材料溶液以制备纳米纤维片; 和(S3)通过热处理使纳米纤维片交联。 由于所公开的用于建筑空调或除湿的聚合物复合材料具有优异的抗菌性能和优异的吸水能力和耐久性,所以当用于建筑物的空调时,聚合物复合材料可以进行除湿,从而降低空调负荷并提高能量效率 。 此外,通过除湿冷却,高效聚合物复合材料可以在夏季从潮湿的空气中除去水分,从而通过减少潜热负荷并节约能源来减少空调负荷。 此外,聚合物复合材料可用于湿度敏感的生产工艺,工业应用中需要水分控制或防止水分损坏或腐蚀以减少水分并提供干燥空气。