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    Method of Preparing Silica Aerogel Granules
    2.
    发明申请
    Method of Preparing Silica Aerogel Granules 有权
    二氧化硅气凝胶颗粒的制备方法

    公开(公告)号：US20130106008A1

    公开(公告)日：2013-05-02

    申请号：US13808673

    申请日：2011-09-28

    申请人： Young-Soo Ahn ,  Jeong-gu Yeo ,  Churl-Hee Cho

    发明人： Young-Soo Ahn ,  Jeong-gu Yeo ,  Churl-Hee Cho

    IPC分类号： C07F7/12 ,  C09K3/00

    CPC分类号： C08K7/10 ,  B01J2/08 ,  C01B33/1585 ,  C07F7/12 ,  C09K3/00

    摘要： A method of preparing transparent or nontransparent silica aerogel granules. The method includes forming a granular wet gel by spraying a silica sol into alcohol, the silica sol being prepared by mixing a water glass solution or an opacifier-containing water glass solution with an inorganic acid solution, forming a granular alcohol gel through gelation aging and solvent substitution of the granular wet gel in alcohol, hydrophobically modifying the surface of the granular alcohol gel using an organic silane compound, and drying the surface modified gel at ambient pressure or in a vacuum. The method may prepare silica aerogel granules in a short period of time through heat treatment at a relatively low temperature and at ambient pressure or in a vacuum, thereby ensuring excellent economic feasibility, continuity and reliability, suited for mass production.

    摘要翻译： 制备透明或不透明的二氧化硅气凝胶颗粒的方法。 该方法包括通过将二氧化硅溶胶喷射到醇中形成粒状湿凝胶，该硅溶胶是通过将水玻璃溶液或含有遮光剂的水玻璃溶液与无机酸溶液混合制备的，通过凝胶化老化形成粒状醇凝胶， 在醇中的颗粒状湿凝胶的溶剂置换，使用有机硅烷化合物疏水改性粒状醇凝胶的表面，并在环境压力或真空下干燥表面改性凝胶。 该方法可以在相对较低的温度和环境压力或真空下通过热处理在短时间内制备二氧化硅气凝胶颗粒，从而确保了适合于批量生产的优异的经济可行性，连续性和可靠性。

    Method of preparing silica aerogel granules
    4.
    发明授权
    Method of preparing silica aerogel granules 有权
    制备二氧化硅气凝胶颗粒的方法

    公开(公告)号：US08894893B2

    公开(公告)日：2014-11-25

    申请号：US13808673

    申请日：2011-09-28

    申请人： Young-Soo Ahn ,  Jeong-gu Yeo ,  Churl-Hee Cho

    发明人： Young-Soo Ahn ,  Jeong-gu Yeo ,  Churl-Hee Cho

    IPC分类号： C01B33/158 ,  B01J2/08 ,  C09K3/00

    CPC分类号： C08K7/10 ,  B01J2/08 ,  C01B33/1585 ,  C07F7/12 ,  C09K3/00

    摘要： A method of preparing transparent or nontransparent silica aerogel granules. The method includes forming a granular wet gel by spraying a silica sol into alcohol, the silica sol being prepared by mixing a water glass solution or an opacifier-containing water glass solution with an inorganic acid solution, forming a granular alcohol gel through gelation aging and solvent substitution of the granular wet gel in alcohol, hydrophobically modifying the surface of the granular alcohol gel using an organic silane compound, and drying the surface modified gel at ambient pressure or in a vacuum. The method may prepare silica aerogel granules in a short period of time through heat treatment at a relatively low temperature and at ambient pressure or in a vacuum, thereby ensuring excellent economic feasibility, continuity and reliability, suited for mass production.

    摘要翻译： 制备透明或不透明的二氧化硅气凝胶颗粒的方法。 该方法包括通过将二氧化硅溶胶喷射到醇中形成粒状湿凝胶，该硅溶胶是通过将水玻璃溶液或含有遮光剂的水玻璃溶液与无机酸溶液混合制备的，通过凝胶化老化形成粒状醇凝胶， 在醇中的颗粒状湿凝胶的溶剂置换，使用有机硅烷化合物疏水改性粒状醇凝胶的表面，并在环境压力或真空下干燥表面改性凝胶。 该方法可以在相对较低的温度和环境压力或真空下通过热处理在短时间内制备二氧化硅气凝胶颗粒，从而确保了适合于批量生产的优异的经济可行性，连续性和可靠性。

    Aerogel Mat and Manufacturing Method Thereof
    5.
    发明申请
    Aerogel Mat and Manufacturing Method Thereof 有权
    气凝胶垫及其制造方法

    公开(公告)号：US20120025127A1

    公开(公告)日：2012-02-02

    申请号：US13258225

    申请日：2010-06-10

    申请人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    发明人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    IPC分类号： E04B1/82 ,  B01J8/00

    CPC分类号： C01B33/1585 ,  C01B33/155 ,  C01B33/157 ,  Y02P20/544

    摘要： The present invention relates to a method of manufacturing a mat containing aerogel and to a mat manufactured using this method. A method of manufacturing a mat containing silica aerogel according to an aspect of the invention includes: (S1) producing a wet gel by mixing water glass and alcohol in a reactor; (S2) modifying a surface of the wet gel by adding an organic silane compound and an organic solvent to the reactor and mixing; (S3) separating a upper liquid from a solution in the reactor and impregnating a fibrous matrix with the upper liquid; and (S4) drying the fibrous matrix impregnated with the upper liquid. According to an aspect of the invention, a mat containing silica aerogel can be manufactured using only water glass as raw material, even when applying the drying process in an ambient environment, without using expensive materials or supercritical apparatus.

    摘要翻译： 本发明涉及一种制造含有气凝胶的垫的方法和使用该方法制造的垫。 根据本发明的一个方面的制备含有二氧化硅气凝胶的垫的方法包括：（S1）通过在反应器中混合水玻璃和醇来生产湿凝胶; （S2）通过向反应器中加入有机硅烷化合物和有机溶剂并混合来改性湿凝胶的表面; （S3）将上液体与反应器中的溶液分离，并用上液体浸渍纤维基质; 和（S4）干燥浸渍有上层液体的纤维基质。 根据本发明的一个方面，即使在不使用昂贵的材料或超临界设备的情况下在周围环境中进行干燥处理，也可以仅使用水玻璃作为原料来制造含有二氧化硅气凝胶的垫。

    Aerogel mat and manufacturing method thereof
    7.
    发明授权
    Aerogel mat and manufacturing method thereof 有权
    气凝胶垫及其制造方法

    公开(公告)号：US08663739B2

    公开(公告)日：2014-03-04

    申请号：US13258225

    申请日：2010-06-10

    申请人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    发明人： Jeong-Gu Yeo ,  Young-Soo Ahn ,  Churl-Hee Cho ,  Jeong Min Hong

    IPC分类号： B05D3/02

    CPC分类号： C01B33/1585 ,  C01B33/155 ,  C01B33/157 ,  Y02P20/544

    摘要： The present invention relates to a method of manufacturing a mat containing aerogel and to a mat manufactured using this method. A method of manufacturing a mat containing silica aerogel according to an aspect of the invention includes: (S1) producing a wet gel by mixing water glass and alcohol in a reactor; (S2) modifying a surface of the wet gel by adding an organic silane compound and an organic solvent to the reactor and mixing; (S3) separating a upper liquid from a solution in the reactor and impregnating a fibrous matrix with the upper liquid; and (S4) drying the fibrous matrix impregnated with the upper liquid. According to an aspect of the invention, a mat containing silica aerogel can be manufactured using only water glass as raw material, even when applying the drying process in an ambient environment, without using expensive materials or supercritical apparatus.

    摘要翻译： 本发明涉及一种制造含有气凝胶的垫的方法和使用该方法制造的垫。 根据本发明的一个方面的制备含有二氧化硅气凝胶的垫的方法包括：（S1）通过在反应器中混合水玻璃和醇来生产湿凝胶; （S2）通过向反应器中加入有机硅烷化合物和有机溶剂并混合来改性湿凝胶的表面; （S3）将上液体与反应器中的溶液分离，并用上液体浸渍纤维基质; 和（S4）干燥浸渍有上层液体的纤维基质。 根据本发明的一个方面，即使在不使用昂贵的材料或超临界设备的情况下在周围环境中进行干燥处理，也可以仅使用水玻璃作为原料来制造含有二氧化硅气凝胶的垫。

    RAPID PREPARATION PROCESS OF AEROGEL
    8.
    发明申请
    RAPID PREPARATION PROCESS OF AEROGEL 审中-公开
    航空快速准备过程

    公开(公告)号：US20080081014A1

    公开(公告)日：2008-04-03

    申请号：US11737450

    申请日：2007-04-19

    申请人： Yong-Soo AHN ,  Jeong-Gu Yeo ,  Moon-Hee Han ,  Churl-Hee Cho ,  Sharad D. Bhagat ,  Yong-Ha Kim ,  Ho-Sung Park

    发明人： Yong-Soo AHN ,  Jeong-Gu Yeo ,  Moon-Hee Han ,  Churl-Hee Cho ,  Sharad D. Bhagat ,  Yong-Ha Kim ,  Ho-Sung Park

    IPC分类号： C01B33/12

    CPC分类号： C01B33/1585 ,  C01B33/158

    摘要： Disclosed herein is a rapid preparation process of aerogel. More specifically, the present invention relates to a rapid preparation process of aerogel which enables a considerable reduction in preparation time and preparation costs via simultaneous treatment of solvent exchange and surface-modification of hydrophilic-to-hydrophobic transition.The rapid preparation process comprises mixing a cation exchange resin with sodium silicate (water glass) as a starting material, and removing the sodium ion from the sodium silicate, to subject the sodium silicate to ion exchange; adding a base catalyst and an organosilane compound to the sodium silicate to subject the sodium silicate to gelation; aging the gellized silica gel at room temperature for 2 to 4 hours to discharge water from the silica gel and to modify the surface of the silica gel into hydrophobicity; and drying the hydrophobic silica gel at atmospheric pressure for 18 to 27 hours.

    摘要翻译： 本文公开了气凝胶的快速制备方法。 更具体地说，本发明涉及一种气凝胶的快速制备方法，其通过同时处理亲水 - 疏水过渡的溶剂交换和表面改性，能够显着降低制备时间和制备成本。 快速制备方法包括将阳离子交换树脂与硅酸钠（水玻璃）作为起始原料混合，并从硅酸钠中除去钠离子，使硅酸钠进行离子交换; 向硅酸钠中加入碱催化剂和有机硅烷化合物以使硅酸钠发生凝胶化; 将胶凝硅胶在室温下老化2至4小时，以从硅胶中排出水，并将硅胶表面改性为疏水性; 并在大气压下干燥疏水性硅胶18至27小时。