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1.发明授权
公开(公告)号：US4470446A
公开(公告)日：1984-09-11
申请号：US280494
申请日：1981-07-06
CPC分类号： G01F23/242
摘要： A method for detecting a molten metal surface level in a casting mold, comprises inserting an electrode in a slag constituting a layer under a flux floating on the surface of the molten metal, detecting a change of electric resistance due to a temperature gradient of the place at which the electrode is inserted, displacing the electrode to bring the detected value to be always constant within a range of from 5 to 50 .OMEGA., and measuring the degree of the displacement of the electrode thereby detecting the surface level of the molten level. An apparatus for carrying out the method is also disclosed.
摘要翻译： 一种用于检测铸模中的熔融金属表面水平的方法，包括将电极插入构成熔融金属表面上的助熔剂下的层中的渣中，检测由于该位置的温度梯度引起的电阻变化 电极插入其中，使电极移动，使检测值始终保持在5〜50欧姆范围内，并测量电极的位移程度，从而检测熔融水平的表面水平。 还公开了一种用于执行该方法的装置。
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公开(公告)号：US08859700B2
公开(公告)日：2014-10-14
申请号：US13812695
申请日：2011-07-20
申请人： Hideki Yokoyama , Sachi Kikuno , Atsushi Heguri , Nobuhiro Maeda
发明人： Hideki Yokoyama , Sachi Kikuno , Atsushi Heguri , Nobuhiro Maeda
IPC分类号： C08F2/20 , C08F2/32 , A61L15/24 , C08F2/18 , C08F2/00 , C08F220/06 , A61L15/60 , C08F2/10 , C08F2/24 , C08F4/04 , C08L33/08
CPC分类号： C08F2/10 , A61L15/24 , A61L15/60 , C08F2/001 , C08F2/18 , C08F2/20 , C08F2/24 , C08F2/32 , C08F4/04 , C08F220/06 , C08L33/08 , Y10S526/91 , Y10S526/911
摘要： A method for producing a water-absorbent resin having a further reduced odor as compared with a water-absorbent resin obtained by a conventional method as well as a water-absorbent resin produced by the same method, by maintaining the addition rate V from the pouring nozzle for the aqueous solution of the water-soluble ethylenically unsaturated monomer in a polymerization reaction tank not more than 0.30 [min−1], in the first stage polymerization step which is within the step of the conventional method upon performing multi-stages such as two or more stages of reversed-phase suspension polymerizations in a method for producing a water-absorbent resin, and thereby by being able to reduce the amount of the petroleum hydrocarbon dispersion medium remaining in the above water-absorbent resin.
摘要翻译： 与通过常规方法获得的吸水性树脂相比，具有进一步降低气味的吸水性树脂的制造方法以及通过相同方法制备的吸水性树脂，通过保持来自浇注的添加率V 在聚合反应槽中的水溶性烯键式不饱和单体的水溶液的喷嘴在不大于0.30 [min -1]的情况下，在第一阶段聚合步骤中，在进行多阶段的步骤中的第一阶段聚合步骤，例如 在吸水性树脂的制造方法中，由于能够减少残留在上述吸水性树脂中的石油烃分散介质的量，反相悬浮聚合的两个阶段或更多阶段。
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公开(公告)号：US20140179886A1
公开(公告)日：2014-06-26
申请号：US14125818
申请日：2011-07-20
申请人： Hideki Yokoyama , Atsushi Heguri , Nobuhiro Maeda
发明人： Hideki Yokoyama , Atsushi Heguri , Nobuhiro Maeda
IPC分类号： C08F120/06
CPC分类号： C08F120/06 , B01J20/267 , C08F2/18 , C08F2/32 , C08F220/06 , C08F220/10 , C08F220/56
摘要： A method is disclosed for producing a water-absorbent resin by a reversed-phase suspension polymerization method, wherein an odor originating from a raw material component, in particular, a petroleum hydrocarbon dispersion medium, is further reduced as compared with a water-absorbent resin obtained by a conventional method, and a water-absorbent resin obtained by the method. More specifically, a method is disclosed for producing a water-absorbent resin by performing a reversed-phase suspension polymerization of a water-soluble ethylenically unsaturated monomer in a petroleum hydrocarbon dispersion medium, comprising adding and dispersing an aqueous solution of a water-soluble ethylenically unsaturated monomer containing a hydrophilic polymeric dispersion agent to a petroleum hydrocarbon dispersion medium in the presence of a surfactant under stirring, and performing a reversed-phase suspension polymerization using a radical polymerization initiator, and a water-absorbent resin obtained by the method.
摘要翻译： 公开了通过反相悬浮聚合法制造吸水性树脂的方法，其中与原料成分，特别是石油烃分散介质相比产生的气味与吸水性树脂相比进一步降低 通过常规方法获得的吸水性树脂和通过该方法获得的吸水性树脂。 更具体地，公开了通过在石油烃分散介质中进行水溶性烯键式不饱和单体的反相悬浮聚合来制造吸水性树脂的方法，包括将水溶性烯键式的水溶液 在表面活性剂存在下，在搅拌的同时，将含有亲水性高分子分散剂的亲水性高分子分散剂与不饱和单体反应，使用自由基聚合引发剂进行反相悬浮聚合，得到的吸水性树脂。
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公开(公告)号：US20130123454A1
公开(公告)日：2013-05-16
申请号：US13812612
申请日：2011-07-20
申请人： Hideki Yokoyama , Sachi Kikuno , Atsushi Heguri , Nobuhiro Maeda
发明人： Hideki Yokoyama , Sachi Kikuno , Atsushi Heguri , Nobuhiro Maeda
IPC分类号： C08F2/10
CPC分类号： C08F2/10 , B01J20/261 , C08F2/18 , C08F2/32 , C08F220/06 , C08F222/1006
摘要： The present invention provides a method for producing a water-absorbent resin by a reversed-phase suspension polymerization method, wherein an odor originating from a raw material component, in particular, a petroleum hydrocarbon dispersion medium, was reduced, and a water-absorbent resin obtained by the method. More specifically, the present invention provides a method for producing a water-absorbent resin comprising performing a reversed-phase suspension polymerization of a water-soluble ethylenically unsaturated monomer in a petroleum hydrocarbon dispersion medium by using a surfactant, wherein an aqueous solution of the water-soluble ethylenically unsaturated monomer is dispersed in the dispersion medium at a specific pouring rate to reduce an odor, and a water-absorbent resin obtained by the method, are provided.
摘要翻译： 本发明提供一种通过反相悬浮聚合法制造吸水性树脂的方法，其中来自原料成分，特别是石油烃分散介质的气味被还原，并且吸水性树脂 通过该方法获得。 更具体地说，本发明提供一种吸水性树脂的制造方法，其包括使用表面活性剂在石油烃分散介质中进行水溶性烯属不饱和单体的反相悬浮聚合，其中，水的水溶液 可溶性烯属不饱和单体以特定的浇注速率分散在分散介质中以降低气味，并且提供通过该方法获得的吸水性树脂。
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公开(公告)号：US06329492B1
公开(公告)日：2001-12-11
申请号：US09319487
申请日：1999-08-13
申请人： Haruaki Sue , Shinsuke Hagiwara , Fumio Furusawa , Seiichi Akagi , Akihiro Kobayashi , Hideki Yokoyama
发明人： Haruaki Sue , Shinsuke Hagiwara , Fumio Furusawa , Seiichi Akagi , Akihiro Kobayashi , Hideki Yokoyama
IPC分类号： C08G5906
CPC分类号： C08G59/3218 , C07C39/17 , C07C2601/08 , C08G59/24 , C08L63/00 , H01L23/293 , H01L2224/32245 , H01L2224/45144 , H01L2224/48091 , H01L2224/48247 , H01L2224/73265 , H01L2924/1301 , H01L2924/00014 , H01L2924/00
摘要： This invention provides a compound suitable as an encapsulating material for electronic devices and having a high Tg, low moisture-absorptive, high adhesion and rich fluidity, which is a cyclopentylene compound represented by Formula (I) and its intermediate cyclopentenyl compound represented by Formula (III). In the formula, m is 0 or more, Ar1 and Ar2 are each a phenol residual group, a naphthol residual group or a fluorene derivative residual group, and each contain a hydroxyl group or a glycidyloxyl group.
摘要翻译： 本发明提供一种适合作为电子器件的封装材料的化合物，其具有高Tg，低吸水性，高粘附性和较高的流动性，其为由式（I）表示的环戊烯化合物及其由式（I）表示的中间体环戊烯基化合物 III）。 在该式中，m为0以上，Ar 1和Ar 2分别为酚残基，萘酚残基或芴衍生物残基，各自含有羟基或缩水甘油氧基。
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公开(公告)号：US5067747A
公开(公告)日：1991-11-26
申请号：US546319
申请日：1990-07-02
申请人： Hideki Yokoyama
发明人： Hideki Yokoyama
摘要： An instrument panel of a vehicle mounts a cluster gauge and is formed with an opening through which a collapsible steering shaft projects. A steering end cover, formed as a hollow shell, is generally cylindrically shaped and covers an end portion of the collapsible steering shaft projecting above the instrument panel. A guide member, provided so as to overlap the opening, has a surface for guiding the hollow shell to sink or telescope into the opening when the collapsible steering shaft axially collapses during a front end, head-on collision.
摘要翻译： 车辆的仪表板安装了一个集群计量器，并形成有可折叠转向轴通过该开口突出的开口。 形成为中空壳的转向端盖通常为圆柱形并且覆盖突出在仪表板上方的可折叠转向轴的端部。 设置成与开口重叠的引导构件具有用于当可折叠的转向轴在前端，正面碰撞期间轴向塌陷时，引导中空壳向凹槽或望远镜入口的表面。
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公开(公告)号：US09132413B2
公开(公告)日：2015-09-15
申请号：US13812650
申请日：2011-07-20
申请人： Sachi Kikuno , Atsushi Heguri , Hideki Yokoyama , Nobuhiro Maeda
发明人： Sachi Kikuno , Atsushi Heguri , Hideki Yokoyama , Nobuhiro Maeda
IPC分类号： C08F2/18 , B01J20/30 , C08F2/32 , C08F220/06 , C08F220/56
CPC分类号： B01J20/30 , C08F2/18 , C08F2/32 , C08F220/06 , C08F220/56
摘要： A method for producing a water-absorbent resin comprising at least two stages of reversed-phase suspension polymerization, wherein the first stage of the at least two stages of reversed-phase suspension polymerization comprises the following steps of: (A) performing a primary dispersion by stirring to mix in the absence of surfactants an aqueous solution of a water-soluble ethylenically unsaturated monomer containing a hydrophilic polymeric dispersion agent with a petroleum hydrocarbon dispersion medium in which a hydrophobic polymeric dispersion agent dissolves or disperses; (B) further performing a secondary dispersion by adding a surfactant to the resultant dispersion liquid; and (C) performing a polymerization by using a water-soluble radical polymerization initiator to obtain a water-absorbent resin as particles in a hydrous gel state which disperse in the petroleum hydrocarbon dispersion medium, and a water-absorbent resin obtained by the method.
摘要翻译： 一种制备吸水性树脂的方法，其包含至少两个阶段的反相悬浮聚合，其中所述至少两个阶段的反相悬浮聚合的第一阶段包括以下步骤：（A）进行一次分散 通过搅拌在不存在表面活性剂的情况下将含有亲水性聚合物分散剂的水溶性烯属不饱和单体的水溶液与疏水性聚合物分散剂溶解或分散的石油烃分散介质混合; （B）通过向所得分散液中加入表面活性剂进一步进行二次分散; 和（C）通过使用水溶性自由基聚合引发剂进行聚合，得到作为分散在石油烃分散介质中的含水凝胶状态的颗粒的吸水性树脂和通过该方法获得的吸水性树脂。
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公开(公告)号：US09074022B2
公开(公告)日：2015-07-07
申请号：US12298195
申请日：2007-04-26
申请人： Hideki Yokoyama , Yasuhiro Nawata
发明人： Hideki Yokoyama , Yasuhiro Nawata
IPC分类号： C08F2/18 , C08F2/32 , C08F220/06
CPC分类号： C08F2/18 , C08F2/32 , C08F220/06
摘要： A purpose of the present invention is to reduce odor of a water-absorbent resin during absorption of water. Such the invention is attained by a process for production of a water-absorbent resin by subjecting a water-soluble ethylenically unsaturated monomer to reversed-phase suspension polymerization. The process comprises the following steps (A) to (C): (A) adding an aqueous solution of water-soluble ethylenically unsaturated monomer to a petroleum hydrocarbon dispersion medium to disperse the aqueous solution in the dispersion medium; (B) adding a surfactant to the emulsion to further disperse the emulsion; and (C) performing the reversed-phase suspension polymerization using a water-soluble radical polymerization initiator, optionally in the presence of an internal-crosslinking agent.
摘要翻译： 本发明的目的是减少吸水性树脂在吸水期间的气味。 通过使水溶性烯属不饱和单体进行反相悬浮聚合，通过吸水性树脂的制造方法实现本发明。 该方法包括以下步骤（A）至（C）：（A）将水溶性烯属不饱和单体的水溶液加入到石油烃分散介质中以将水溶液分散在分散介质中; （B）向乳液中加入表面活性剂以进一步分散乳液; 和（C）任选地在内部交联剂的存在下，使用水溶性自由基聚合引发剂进行反相悬浮聚合。
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公开(公告)号：US20130123445A1
公开(公告)日：2013-05-16
申请号：US13812753
申请日：2011-07-20
申请人： Atsushi Heguri , Sachi Kikuno , Hideki Yokoyama , Nobuhiro Maeda
发明人： Atsushi Heguri , Sachi Kikuno , Hideki Yokoyama , Nobuhiro Maeda
IPC分类号： C08F2/10
CPC分类号： C08F2/10 , C08F2/32 , C08F220/06 , C08F220/56
摘要： A method for producing a water-absorbent resin by performing a reversed-phase suspension polymerization of a water-soluble ethylenically unsaturated monomer in a petroleum hydrocarbon dispersion medium, comprising the following steps of: (A) performing a primary dispersion in the absence of surfactants by adding an aqueous solution of a water-soluble ethylenically unsaturated monomer containing a hydrophilic polymeric dispersion agent to a petroleum hydrocarbon dispersion medium in which a hydrophobic polymeric dispersion agent was heat-dispersed or heat-dissolved, under stirring; (B) further performing a secondary dispersion by adding a surfactant to a dispersion liquid obtained after the primary dispersion; and (C) performing the reversed-phase suspension polymerization by using a radical polymerization initiator; and the water-absorbent resin obtained by the method.
摘要翻译： 一种通过在石油烃分散介质中进行水溶性烯键式不饱和单体的反相悬浮聚合制备吸水性树脂的方法，包括以下步骤：（A）在不存在表面活性剂的情况下进行一次分散 通过在搅拌下将含有亲水性高分子分散剂的水溶性烯属不饱和单体的水溶液加入其中疏水聚合物分散剂被热分散或热溶解的石油烃分散介质中; （B）通过向在一次分散后得到的分散液中添加表面活性剂进一步进行二次分散; 和（C）使用自由基聚合引发剂进行反相悬浮聚合; 和通过该方法获得的吸水性树脂。
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公开(公告)号：US20100331802A1
公开(公告)日：2010-12-30
申请号：US12673924
申请日：2008-08-14
申请人： Hideki Yokoyama , Yasuhiro Nawata
发明人： Hideki Yokoyama , Yasuhiro Nawata
CPC分类号： B01J20/267 , A61L15/60 , B01J20/261 , C08F2/14 , C08F2/32 , C08F20/06
摘要： The present invention provides a water-absorbent resin produced by a reversed-phase suspension polymerization method, which contains a small amount of a petroleum hydrocarbon dispersion medium remaining therein used in reversed-phase suspension polymerization, and thus reducing an odor originating from the petroleum hydrocarbon dispersion medium, when the water-absorbent resin absorbs water, and also which is suitable for use in hygienic materials; an absorbent material and an absorbent article. More particularly, the present invention provides a water-absorbent resin obtained by subjecting an aqueous solution of a water-soluble ethylenically unsaturated monomer to reversed-phase suspension polymerization in a petroleum hydrocarbon dispersion medium in the presence of a surfactant, wherein the amount of the petroleum hydrocarbon dispersion medium remaining in the water-absorbent resin is 2,000 ppm or less; and an absorbent material and an absorbent article using the same.
摘要翻译： 本发明提供一种通过反相悬浮聚合法制备的吸水性树脂，其中含有少量其中残留在反相悬浮聚合中的石油烃分散体，从而减少源自石油烃的气味 分散介质，当吸水性树脂吸水时，也适用于卫生材料; 吸收材料和吸收制品。 更具体地说，本发明提供一种吸水性树脂，其通过在表面活性剂的存在下，在石油烃分散介质中使水溶性烯属不饱和单体的水溶液进行反相悬浮聚合，其中， 残留在吸水性树脂中的石油烃分散介质为2000ppm以下， 以及使用其的吸收性材料和吸收性物品。
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