Regeneration of mixed bed resins
    6.
    发明授权

    公开(公告)号:US10287186B2

    公开(公告)日:2019-05-14

    申请号:US15566652

    申请日:2016-04-13

    申请人: Ovivo Inc.

    摘要: In an ion-exchange separation system, a single regeneration column provides for separation of anion and cation resins and the regeneration of both cation and anion resins with a very low level of cross-contamination. After regeneration most of the anion layer in the column is withdrawn, and most of the cation layer is withdrawn, but a portion of each layer adjacent to the interface between the layers remains in the column, to isolate these cross-contaminated portions from the regenerated resins. The withdrawn, regenerated anion and cation resins are placed back into the working vessel.

    Recovery of fluorinated emulsifying acids from basic anion exchangers
    8.
    发明授权
    Recovery of fluorinated emulsifying acids from basic anion exchangers 失效
    从碱性阴离子交换剂回收氟化乳化酸

    公开(公告)号:US4282162A

    公开(公告)日:1981-08-04

    申请号:US115803

    申请日:1980-01-28

    申请人: Jurgen Kuhls

    发明人: Jurgen Kuhls

    摘要: To elute fluorinated emulsifying acids, especially perfluoro-carboxylic acids, from basic anion exchangers a mixture of dilute mineral acid and polar organic solvents is used. The solvent should be miscible with water preferably to an extent of at least 40%. By this process the required amount of eluent and the time of elution can be reduced while simultaneously the amount of recovered emulsifying acid can be improved. The process is especially suitable for the recovery of fluorinated emulsifiers in the coagulation or concentration of fluoropolymer latices.

    摘要翻译: 为了从碱性阴离子交换剂中洗脱含氟乳化酸,特别是全氟羧酸,使用稀无机酸和极性有机溶剂的混合物。 溶剂应与水混溶,优选至少为40%。 通过该方法,可以减少所需量的洗脱液和洗脱时间,同时可以提高回收的乳化酸的量。 该方法特别适用于在含氟聚合物胶乳的凝结或浓缩中回收氟化乳化剂。

    LOW-SODIUM RESIN
    9.
    发明申请

    公开(公告)号:US20210283593A1

    公开(公告)日:2021-09-16

    申请号:US16321609

    申请日:2017-08-25

    申请人: John C. Rohanna

    发明人: John C. Rohanna

    摘要: Provided is a method of removing sodium from a collection of sodium-laden resin beads comprising the steps of (a) providing the collection of sodium-laden resin beads, wherein the resin beads comprise one or more vinyl polymers having quaternary ammonium groups; wherein cation exchange resin, if present in the collection of resin beads, are present in an amount of 0 to 0.5% by weight based on the weight of the collection of resin beads; wherein 90 mole % or more of the quaternary ammonium groups are each associated with a hydroxide anion; wherein sodium is present in an amount of more than 100 ppb by weight, based on the weight of the collection of sodium-laden resin beads, and (b) bringing the collection of sodium-laden resin beads into contact with aqueous ammonium hydroxide to form a mixture (b).