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    Method of producing metal particles, and metal oxide obtained from the particles
    1.
    发明申请
    Method of producing metal particles, and metal oxide obtained from the particles 失效
    制备金属颗粒的方法和从颗粒获得的金属氧化物

    公开(公告)号：US20040131538A1

    公开(公告)日：2004-07-08

    申请号：US10670790

    申请日：2003-09-26

    申请人： FUJI PHOTO FILM CO., LTD.

    发明人： Katsuhisa Ohzeki

    IPC分类号： C01G001/02

    CPC分类号： B82Y30/00 ,  B22F1/0022 ,  B22F9/24 ,  B22F2009/088

    摘要： A method of producing (1) metal particles or (2) metal fine-particles, which contains: jetting out two solutions of (1) a metal salt solution and a reducing agent solution, or (2) a metal ion-containing solution and a hydroxide ion-containing solution, from respective nozzles to a mixing chamber, to give a mixed reaction solution; and discharging the mixed reaction solution from a discharging port having a diameter smaller than a diameter of the mixing chamber, wherein one of the two solutions is made into straightly-going flow, which is jetted from a nozzle having a diameter smaller than the diameter of the mixing chamber to the mixing chamber, and the other solution is jetted out, as flow substantially orthogonal to the straightly-going flow, to a position before a position where eddy viscosity generated by the straightly-going flow would be maximum.

    摘要翻译： （1）金属颗粒或（2）金属微粒的制造方法，其特征在于，包括：喷射（1）金属盐溶液和还原剂溶液的两种溶液，或（2）含金属离子的溶液和 含氢氧根离子的溶液，从各个喷嘴到混合室，得到混合的反应溶液; 并且从具有小于混合室直径的直径的排出口排出混合的反应溶液，其中两个溶液中的一个被制成直线流动，其从直径小于 将混合室输送到混合室，将另一溶液作为大致垂直于直线流动的流动被喷射到在直线流动产生的涡流粘度最大的位置之前的位置。

    Method of making oxide particles
    5.
    发明申请
    Method of making oxide particles 失效
    制造氧化物颗粒的方法

    公开(公告)号：US20040253174A1

    公开(公告)日：2004-12-16

    申请号：US10462053

    申请日：2003-06-16

    申请人： General Electric Company

    发明人： Darryl Stephen Williams

    IPC分类号： C01G001/02

    CPC分类号： B82Y30/00 ,  C01B33/145 ,  C01G1/02 ,  C01G23/053 ,  C01G25/02 ,  C01P2004/62 ,  C01P2004/64 ,  Y10S977/773 ,  Y10S977/775 ,  Y10S977/777 ,  Y10S977/811

    摘要： The present invention provides a process for producing particles comprising mixing, in a substantially water-free environment, at least one metal compound of the formula M(O2CR)nX(m-n)Lp wherein M is an electropositive element of Groups 1-15, each X is independently selected from the group consisting of O1/2, F, Cl, Br, I, OR, O2CR, NR2, and R, each R is independently a hydrocarbyl group, each L is independently a Lewis base ligand, n is equal to null the oxidation state of the metal M in the product particle, m is equal to the oxidation state of M in the compound M(O2CR)nX(m-n)Lp and pnull0; at least one surfactant; and at least one solvent wherein the mixture is thermally treated for a time sufficient to convert the at least one metal compound into particles of the corresponding oxide having sizes in a range between about 0.5 nanometers and about 1000 nanometers.

    摘要翻译： 本发明提供了一种生产颗粒的方法，包括在基本无水的环境中混合至少一种式M（O 2 CR）n X（mn）L p的金属化合物，其中M是第1-15族的正电性元素，各自 X独立地选自O1 / 2，F，Cl，Br，I，OR，O2CR，NR2和R，每个R独立地是烃基，每个L独立地是路易斯碱配体，n等于 到产物颗粒中金属M的氧化态的1/2，m等于化合物M（O 2 CR）n X（mn）Lp中的M的氧化态，p> = 0; 至少一种表面活性剂; 和至少一种溶剂，其中将该混合物进行热处理足以将至少一种金属化合物转化成尺寸在约0.5纳米至约1000纳米之间的相应氧化物的颗粒的时间。

    Metal oxide powder for high precision polishing and method of preparation thereof
    6.
    发明申请
    Metal oxide powder for high precision polishing and method of preparation thereof 有权
    用于高精度抛光的金属氧化物粉末及其制备方法

    公开(公告)号：US20030228248A1

    公开(公告)日：2003-12-11

    申请号：US10456685

    申请日：2003-06-05

    发明人： Hyukjin Kwon ,  Myungho Ahn ,  Youngkwon Joung ,  Inyeon Lee

    IPC分类号： C01G001/02

    CPC分类号： B82Y30/00 ,  C01F7/02 ,  C01F17/0043 ,  C01G1/02 ,  C01P2004/04 ,  C01P2004/50 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C09G1/02 ,  C09K3/1409 ,  C09K3/1463

    摘要： The present invention relates to a metal oxide powder for high precision polishing and prepartion thereof, comprising aggregates formed by cohesion of primary particles, which has a cohesive degree (null) of 1.1 to 2.0 and a cohesive scale (null) of 3 to 10, the cohesive degree (null) and the cohesive scale (null) being defined by formula (I) and formula (II), respectively: nullnull6/(Snullnullnulld(XRD))nullnull(I) nullnullweight average particle diameter/d(XRD)nullnull(II) wherein, S is the specific surface area of the powder; null, the density; and d(XRD), the particle diameter of the powder determined by X-ray diffraction analysis. In accordance with the present invention, it is possible to provide a high polishing speed and reduce scratches.

    摘要翻译： 本发明涉及一种用于高精度抛光及其制备的金属氧化物粉末，其包含通过粘结度（α）为1.1〜2.0，凝聚度（β）为3〜10的一次粒子凝聚而形成的聚集体， 分别由式（I）和式（II）定义的内聚度（α）和粘结度（β）：α= 6 /（Sxrhoxd（XRD））（I）β=重均粒径/ d XRD）（II）其中，S为粉末的比表面积; 密度; 和d（XRD），通过X射线衍射分析确定粉末的粒径。 根据本发明，可以提供高抛光速度并减少划痕。

    Method of producing fine particles of metal oxide
    7.
    发明申请
    Method of producing fine particles of metal oxide 有权
    生产金属氧化物细颗粒的方法

    公开(公告)号：US20020119093A1

    公开(公告)日：2002-08-29

    申请号：US10014558

    申请日：2001-12-14

    申请人： NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY

    发明人： Norimitsu Murayama ,  Woosuck Shin ,  Sumihito Sago ,  Makiko Hayashi

    IPC分类号： C01G001/02

    CPC分类号： B82Y30/00 ,  C01B13/14 ,  C01F17/0043 ,  C01G1/02 ,  C01G19/02 ,  C01P2004/64

    摘要： A method of producing fine particles of an oxide of a metal, comprising the steps of: preparing an acidic solution which contains ions of the metal; precipitating fine particles of a hydroxide of the metal by adding an alkaline solution to the acidic solution; collecting the fine particles of the hydroxide of the metal precipitated in a mixed solution of the acidic solution and the alkaline solution; mixing fine particles of a carbon with the collected fine particles of the hydroxide of the metal; and heat-treating a mixture of the fine particles of the hydroxide of the metal and the fine particles of the carbon at a predetermined temperature in a non-reducing atmosphere, whereby the fine particles of the oxide of the metal are produced.

    摘要翻译： 一种生产金属氧化物微粒的方法，包括以下步骤：制备含有金属离子的酸性溶液; 通过向酸性溶液中加入碱性溶液来沉淀金属氢氧化物的细颗粒; 收集在酸性溶液和碱性溶液的混合溶液中沉淀的金属氢氧化物的细颗粒; 将碳的细颗粒与收集的金属氢氧化物的细颗粒混合; 在非还原性气氛中，将规定温度的金属的氢氧化物的微粒与碳的微粒的混合物进行热处理，由此制造金属氧化物的微粒。

    Cathode material for lithium battery
    8.
    发明申请
    Cathode material for lithium battery 有权
    锂电池阴极材料

    公开(公告)号：US20040265216A1

    公开(公告)日：2004-12-30

    申请号：US10603910

    申请日：2003-06-25

    发明人： Gholam-Abbas Nazri ,  Gregory Charles Garabedian

    IPC分类号： C01G001/02

    CPC分类号： C01G53/42 ,  C01P2002/52 ,  C01P2002/54 ,  C01P2002/72 ,  C01P2002/74 ,  C01P2002/76 ,  C01P2002/88 ,  C01P2006/12 ,  C01P2006/40

    摘要： A method is disclosed for synthesizing a crystalline metal oxide powder material containing two or more uniformly distributed metal elements. Crystalline, water containing, oxygen containing inorganic acid salts of the metals are heated to liquefy the salts. The apparent solution contains a uniform mixture of the metal elements. The water is removed from the liquid and the resulting powder calcined in air to decompose the acid salts to a mixed metal crystalline oxide. The method is particularly useful to make doped LiNiO2 type crystals using hydrated nitrate or nitrite salts of Li, Ni and the dopant elements. Examples of useful salts are LiNO3.H2O, Ni(NO3)2.6H2O, Co(NO3)2.6H2O, Al(NO3)3.9H2O, and Mg(NO3)2.6H2O.

    Metal compound microparitcles and ultra-microparticle powders
    10.
    发明申请
    Metal compound microparitcles and ultra-microparticle powders 审中-公开
    金属复合微晶片和超微粒粉末

    公开(公告)号：US20040052673A1

    公开(公告)日：2004-03-18

    申请号：US10466490

    申请日：2003-07-17

    发明人： Fukuo Huang

    IPC分类号： C01G001/02 ,  B22F003/23

    CPC分类号： C01G1/02

    摘要： A method for producing fine or ultra fine powder particles comprising mixing a metal alkoxide with a non-metallic hydride in an organic solvent, agitating the mixed solution, and then burning the mixed solution. The burning process comprises igniting the solution directly or burning the solution in situ. A self-sustaining flame will result. When the precursor solution burns, the metallic compound will be co-fired with the organic solvent. As a result, fine or ultra fine particles of mixed metal will burst from the flame, or thrust through the flame and be synthesized.

    摘要翻译： 一种生产精细或超细粉末颗粒的方法，包括在有机溶剂中混合金属醇盐与非金属氢化物，搅拌混合溶液，然后燃烧混合溶液。 燃烧过程包括直接点燃溶液或原位燃烧溶液。 会导致自我维持的火焰。 当前体溶液燃烧时，金属化合物将与有机溶剂共烧。 结果，混合金属的细或超细颗粒将从火焰中爆裂，或者通过火焰推出并被合成。