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    Catalyst for the hydrotreating of heavy hydrocarbon oils
    2.
    发明授权
    Catalyst for the hydrotreating of heavy hydrocarbon oils 失效
    用于加氢处理重质烃油的催化剂

    公开(公告)号：US4595667A

    公开(公告)日：1986-06-17

    申请号：US722821

    申请日：1985-04-12

    申请人： Shinji Takase ,  Akira Inoue ,  Tatuo Omata ,  Masao Mori ,  Yoshihiro Yamazaki ,  Tatsuki Kubo

    发明人： Shinji Takase ,  Akira Inoue ,  Tatuo Omata ,  Masao Mori ,  Yoshihiro Yamazaki ,  Tatsuki Kubo

    IPC分类号： B01J21/16 ,  B01J35/10 ,  B01J37/02 ,  C01G45/04 ,  C10G45/04

    CPC分类号： B01J37/024 ,  C10G45/04

    摘要： This invention relates to a catalyst for the hydrotreating of heavy hydrocarbon oils, which catalyst comprises a dual structure including a porous core (1), made chiefly of alumina, which has micropores having an average size smaller than 170 angstrom and to which at least one active metal is applied, and a surface layer (2) comprised mainly of at least one clay mineral selected from the group consisting of sepiolite, halloysite, attapulgite, palygorskite, and asbestos. The active metal may be applied to the surface layer (2) as desired.

    摘要翻译： 本发明涉及一种用于重质烃油加氢处理的催化剂，该催化剂包括双重结构，其包括主要由氧化铝制成的多孔芯（1），其具有平均尺寸小于170埃的微孔，并且至少一个 施加活性金属，以及主要由至少一种选自海泡石，多水高岭土，绿坡缕石，坡缕石和石棉的粘土矿物组成的表层（2）。 可以根据需要将活性金属施加到表面层（2）。

    Hydroconversion process employing catalyst with specified pore size distribution
    5.
    发明授权
    Hydroconversion process employing catalyst with specified pore size distribution 失效
    使用具有规定孔径分布的催化剂的加氢转化方法

    公开(公告)号：US5399259A

    公开(公告)日：1995-03-21

    申请号：US870970

    申请日：1992-04-20

    申请人： Pei-Shing E. Dai ,  Gerald V. Nelson ,  Govanon Nongbri ,  Roy E. Pratt ,  David E. Sherwood, Jr.

    发明人： Pei-Shing E. Dai ,  Gerald V. Nelson ,  Govanon Nongbri ,  Roy E. Pratt ,  David E. Sherwood, Jr.

    IPC分类号： B01J23/85 ,  B01J27/18 ,  B01J27/185 ,  B01J35/10 ,  C07B61/00 ,  C10G45/08 ,  C10G47/12 ,  C10G49/04 ,  C01G45/04 ,  C01G47/12

    CPC分类号： C10G45/08 ,  B01J23/85 ,  B01J27/1853 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/108

    摘要： Heavy oils may be hydrotreated in the presence of a porous alumina support bearing metals of Group VIII and VI-B and optionally phosphorus, the catalyst having a Total Surface Area of 165-230 m.sup.2 /g, a Total Pore Volume of 0.5-0.8 cc.g, and a Pore Diameter Distribution whereby less than about 5% of the Total Pore Volume is present as primary micropores of diameter less than 80.ANG., and secondary micropores of diameter of .+-.20.ANG. of a Pore Mode of 100-135.ANG. are present in amount of at least about 65% of the micropore volume having pores with diameter less than 250.ANG., and 22-29% of the Total Pore Volume is present as macropores of diameter >250.ANG.. The process of the instant invention is particularly effective in achieving desired levels of hydrodemetallation, hydrodesulfurization, and hydrocracking of asphaltenes in the fraction of hydrotreated/hydrocracked petroleum resid product having a boiling point greater than 1000.degree. F.

    摘要翻译： 重油可以在带有VIII族和VI-B族金属和任选的磷的多孔氧化铝载体存在下进行加氢处理，催化剂的总表面积为165-230m2 / g，总孔体积为0.5-0.8cc 孔和直径分布，其中小于总孔体积的约5％作为直径小于80的初级微孔存在，孔径模式的直径为+/- 20的第二微孔为100-135 ANGSTROM以直径小于250的孔的微孔体积的至少约65％的量存在，并且总孔体积的22-29％作为直径大于250的大孔存在。 本发明的方法在沸点高于1000°F的加氢处理/加氢裂化石油渣产品馏分中达到希望水平的加氢脱金属，加氢脱硫和沥青质加氢裂化的水平是特别有效的。

    Formulation of Tc and Re carbonyl complexes using stannous ion as the reductant for pertechnetate and perrhenate
    10.
    发明申请
    Formulation of Tc and Re carbonyl complexes using stannous ion as the reductant for pertechnetate and perrhenate 审中-公开
    使用亚锡离子作为高铼酸盐和高铼酸盐的还原剂制备Tc和Re羰基络合物

    公开(公告)号：US20050276755A1

    公开(公告)日：2005-12-15

    申请号：US11205020

    申请日：2005-08-17

    申请人： David Pipes ,  Mary Dyszlewski ,  Elizabeth Webb

    发明人： David Pipes ,  Mary Dyszlewski ,  Elizabeth Webb

    IPC分类号： G21H5/02 ,  A61K49/08 ,  A61K51/00 ,  A61K51/04 ,  A61P43/00 ,  C01G45/04 ,  C01G47/00 ,  C01G99/00 ,  C07F5/00 ,  C07F13/00

    CPC分类号： A61K51/0476 ,  A61K49/101 ,  A61K51/0474 ,  C07F13/005 ,  Y10S530/811

    摘要： The invention relates to novel aminocarboxylate ligands that are suitable for complexing with a radionuclide, and are useful as therapeutic agents and as imaging agents for diagnostic purposes. In accordance with the present invention, a method of preparing a compound of formula fac-[M(CO)3(OH2)3]+  (I) where M is MN, 99mTc, 186Re or 188Re, involves reacting a metal in permetallate form with carbon monoxide and stannous ion. The compound of formula (I) can be reacted with a ligand Lx to form a compound of the formula fac-[M(CO)3Lx]n  (II) wherein M is as defined above, Lx is a monodentate or multidentate ligand or a mixture of these ligands, and n is a charge of the ligand Lx increased with one+charge. The invention also is directed to novel compounds, and kits for carrying out the disclosed methods.

    摘要翻译： 本发明涉及适用于与放射性核素络合的新型氨基羧酸酯配体，并且可用作诊断目的的治疗剂和成像剂。 根据本发明，制备式<β的化合物的方法在线配方描述=“在线式”中，末端=“铅”→fac- [M（CO）3 < （I 2）（I）<βin-line-formula description =“In-line Formulas”end = “尾”→其中M是MN，99m Tc，186 Re或188 Re，包括使金属元素与一氧化碳反应 和亚锡离子。 式（I）的化合物可以与配位体L x x化合物反应形成下式的化合物：式中：-in-line-formula description =“In-Line Formulas”end =“lead”？ （II）<β-in-line-formula description =“In-line 式“末端=”尾“→其中M如上所定义，L x x是单齿或多齿配体或这些配体的混合物，n是配体L的电荷， x 增加一个+电荷。 本发明还涉及用于实施所公开的方法的新化合物和试剂盒。